Author(s): Stella, Giuseppe ; Almeida, Luis ; Basílio, Lilia ; Pasquale, Stefania ; Dinis, Jorge ; Almeida, Miguel ; Gueli, Anna M.
Date: 2018
Persistent ID: https://hdl.handle.net/10316/101861
Origin: Estudo Geral - Universidade de Coimbra
Subject(s): brick dating; mortar dating; XRD; colorimetry; characterization; archaeological stratigraphy
Cross-dating of bricks and mortars from historical building, through thermal (TL) and optically stimulated (OSL) luminescence have achieved good accuracy and precision. However this approach is, in many cases, not exhaustive especially for buildings with different construction phases closely temporally spaced to each other. The uncertainties of experimental data added to the reuse of old bricks and/or the presence of mortars applied on restorations represent the main limits to obtain the complete chronology. In the case of the Convento de S. Francisco (Coimbra, Portugal), the dating results were crossed with the stratigraphic study of the building, mineralogical characterization by XRD and colorimetric data of the mortar samples. Thanks to luminescence ages, mineralogical composition and color specification, two phases of construction were identified: the first from the 17th century and the first half of the 18th century and the second from the second half of the 18th century to the first half of the 19th century. These results were confirmed by mineralogical characterization and colorimetric measurements of mortars that identify two different types of materials in aggregate/binder ratio terms and superficial optical characteristics.
