Project/scholarship details


This project is concerned with the development of functionally graded materials and structures through the development of a multi-material laser sintering equipment. Once this is achieved this would represent a substantial progress in materials/structures processing when compared to existing man-made materials and equipments. Bio-inspired materials are becoming of increasing interest in many fields of practical applications. In contrast to man-made materials natural materials such as wood, bone, teeth, and shell are composed of materials chemical gradations and hierarchical structuring. This allows them to fulfil and to combine a variety of mechanical and additional functions e.g. combining high stiffness and toughness, benign fracture behaviour, self-adaptability, optical functions, thermal functions, etc. New simulation and production methods intend to allow to structure technical materials similar to the biological templates. Combining the knowledge of natural materials with a newly proposed technique of fabrication of technical materials is the aim of this project. In order to give a step forward in bio-inspired materials/structures development this project intends to design and process: · Multi-material components of metals/alloys and ceramics; · Components with 3D degrees of freedom of chemical composition gradation along its volume; · Hierarquical and cellular structure materials with closed and/or open cells. Although the outputs of the project will cover a wide range of industrial applications such as moulds industry, automotive and aeronautic structural components, electronic devices, etc, this project will focus on development of bio-medical applications namely on dental and hip implants. These would serve as demonstrators of the technological capabilities of the proposed equipment/process. The most important issues to be solved for metallic implant materials are osteolysis and aseptic loosening [1], lack of bioactivity [2], mismatch of the Young's modulus between bone (10–30 GPa) and metallic implant materials (110 GPa for Ti and 248 GPa for CoCrMo alloy) [3], and metallic ion releasing [4]. On the other hand, the real bone cross-section is composed of periosteum, compact bone and spongy bone regions, from outer part to the inner part, respectively. Therefore, in this project, we focused on the requirements on the current implant materials while we inspired from the structure of the real bone. In this context, the main innovative points of the project regarding the design of the components are: · Create an external porosity for osseo-integration (hierarchically cellular open cells) · Create an internal porosity for lower weight (hierarquically celular closed cells) · Create a compositional gradient in longitudinal and radial directions (materials with different functions in different regions) In order to fulfill the previous components/materials requirements the equipment that will be developed to perform it will be a Multi-material Laser Sintering System (MmLSS). New hardware and software systems will be developed to enable both the production of multi-material components or functionally graded components and closed and open cells. The hardware system will comprise a multi-material vat supply system that enables the fabrication of multi-material structures, a dynamic laser processing system and a dynamic building chamber atmosphere. The proposed multi-vat system will be comprised of 5 different material supply vats enabling the material variation during the production of multi-material components. Due to the high variety of powder materials available for laser sintering systems, the building chamber will also be able to vary its controllable sintering atmosphere for each material during production. The fabrication process is based on the projection of an infrared radiation with a wavelength of 1.06 µm with the aid of a scanning system that adjusts its scanning speed according to each powder material specification. The adjustable scanning speed allows adjusting the proper scanning energy depending on each materials characteristic (melting point). The MmLSS system works in an ascendant method sintering the powder from below through a glass window building plate within the building chamber. This process will allow perform hollow cells since the material would remain in the window (see graphical abstract (attach). The system will also involve the development of software to control the apparatus, which works with 3D standard industrial CAD files with appropriate modifications for the production of components of multiple materials or functionally graded. The software will also enable tagging of each building region a specific material for the multi-material production, control the multi-material vat supply system and laser scanning speed for each material.

  • Funder

    FCT - Fundação para a Ciência e a Tecnologia, I.P.

  • Funder's country

    Portugal

  • Funding program

    5876-PPCDTI

  • Funding amount

    453,999.00 €

  • Start date

    2013-01-01

  • End date

    2015-12-31

Documents


Processamento e caracterização mecânica e metalográfica de compósitos adiamanta...

Ferreira, Pedro Alexandre Monteiro

Dissertação de mestrado em Engenharia de Materiais; No mercado da prospeção de rochas existe uma grande procura por ferramentas que possuam características e propriedades adequadas às rochas onde são aplicadas, nomeadamente com resistência mecânica e comportamento ao desgaste adequados. Neste contexto é fundamental um estudo contínuo para encontrar os melhores materiais que possam ser utilizados na produção des...


Wear of PEEK-Ti6Al4V systems under micro-abrasion and linear sliding conditions

Sampaio, Miguel Ângelo Guimarães

Dissertação de mestrado integrado em Engenharia Biomédica; In dentistry, prosthetic structures must be able to support masticatory loads combined with a high biocompatibility and wear resistance in the presence of a corrosive environment. Also, abrasive wear is inevitable at exposed tooth or restorative surfaces, during mastication and tooth brushing. Thus, this work is dedicated to the tribological characteriz...


Improvement on sliding wear behavior of Al/Cast iron tribopair by CNT’s reinfor...

Carvalho, Óscar Samuel Novais; Buciumeanu, Mihaela; Soares, Delfim; Gomes, J. R.; Silva, Filipe Samuel

The results presented in this work show the wear characterization of Al-Si matrix composites reinforced by multiwall carbon nanotubes (MWCNTs) under dry reciprocating sliding conditions against a grey cast iron (GCI). The wear resistance is investigated as a function of the carbon nanotube (CNT) content that varied from 2 to 6 wt%. The results demonstrated that the CNT content plays a relevant role in the wear ...


Functionalizing machinable glass-ceramic for jewellery items produced by hot pr...

Castro, Sara; Guedes, A.; Silva, Filipe Samuel

The present work is centred on the development of a novel technique, tailored to enable chemical bonding between the ceramic and metal parts of jewels produced by hot pressing. The process involves the functionalization of the ceramic part in order to induce the formation of a metallic multi-layered coating, with a global chemical composition similar to that of an active brazing alloy (ABA). In the course of ho...


Processamento e caracterização de compósitos de Ti-HAP para aplicações biomédicas

Araújo, Andreia Sofia Sá

Dissertação de mestrado integrado em Engenharia de Materiais; Este estudo partiu da necessidade de desenvolver materiais com propriedades mais adequadas a uma utilização em aplicações biomédicas em geral e em implantes em particular. Capacidade de osseintegração, alta biocompatibilidade e propriedades mecânicas adequadas são os aspetos mais relevantes em materiais para implantes. O objetivo desta dissertação fo...


Mechanical, fatigue and wear properties of sintered Carbon Nanotube-based funct...

Carvalho, Óscar Samuel Novais de

Tese de Doutoramento Engenharia Mecânica; This PhD thesis is concerned with the development of nickel coated carbon nanotubes (CNTs) functionally graded metal matrix composites, based on an aluminium-silicon alloy matrix, obtained by powder metallurgy. Besides their development and production, this thesis focus on these composites characterization when regarding metallurgical, mechanical, fatigue and wear behav...


Microstructural characterization of biofunctionalized titanium foams

Teixeira, M.; Alves, Alexandra Manuela Vieira Cruz Pinto; Silva, Filipe Samuel; Pinto, A. M. P.; Toptan, Fatih

This study was supported by The Calouste Gulbenkian Foundation through “Programa de Mobilidade Académica para Professores”, “Ações Integradas Luso-Francesas 2014 - ref.ª: TC-12_14”, and the Portuguese Foundation for Science and Technology (FCT–Portugal), under the project EXCL/EMS-TEC/0460/2012.; info:eu-repo/semantics/publishedVersion


Dry sliding wear behaviour of Ti-TiB-TiNx in-situ composite synthesised by reac...

Silva, J. I.; Alves, Alexandra Manuela Vieira Cruz Pinto; Pinto, A. M. P.; Silva, Filipe Samuel; Toptan, Fatih

Ti and its alloys are attractive materials for a variety of fields; however, a major problem of Ti and its alloys is their poor wear resistance. It is known that reinforcing Ti with hard ceramic phases can substantially improve the wear resistance. Thus, Ti-TiB-TiNx in-situ metal matrix composites were synthesised by reactive hot pressing utilising Ti/BN powder blends with 23:1 Ti:BN weight ratio. Ball-on-plate...


Corrosion and tribocorrosion behaviour of Ti−B4C composite intended for orthopa...

Toptan, Fatih; Rego, Alberto; Alves, Alexandra Manuela Vieira Cruz Pinto; Guedes, A.

Poor wear resistance of titanium is a major concern since relative movements due to the cyclic loads in body environment cause wear between the bone and the implant material leading to detachment of the wear debris and release of metal ions due to the simultaneous action of corrosion and wear, defined as tribocorrosion. In order to increase the tribocorrosion resistance, Grade 2 Ti matrix 24 vol.% B4C particle ...


Predictive models for physical and mechanical properties of 316L stainless stee...

Miranda, Maria Georgina Macedo; Faria, Susana; Bartolomeu, F.; Pinto, E.; Madeira, S.; Mateus, A.; Carreira, P.; Alves, N.; Silva, F. S.

Selective Laser Melting (SLM) processing parameters are known to greatly influence 316L stainless steel final properties. A simple energy density calculation is insufficient for explaining mechanical and physical properties as well as microstructural characteristics, which are known to significantly influence these parts performance. In fact, parts produced by using different combinations of processing paramete...

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