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Structure and rheological properties of a xyloglucan extracted from Hymenaea co...

Arruda, Isabel R. S.; Albuquerque, Priscilla B. S.; Santos, Gustavo R. C.; Silva, Alexandre G.; Mourão, Paulo A. S.; Correia, Maria T. S.

Hymenaea courbaril var courbaril seed xyloglucan was efficiently extracted with 0.1 M NaCl, followed by ethanol precipitation (yield = 72 ± 5% w/w). Its amorphous structure was identified by the pattern of X-ray diffraction. The monosaccharide composition was determined by GC/MS analysis of the alditol acetates and showed the occurrence of glucose:xylose:galactose:arabinose (40:34:20:6). One-(1D) and two-dimens...



Quercetin-loaded lecithin/chitosan nanoparticles for functional food applications

Souza, Marthyna P.; Vaz, Antônio Fernando; Correia, M. T. S.; Cerqueira, M. A.; Vicente, A. A.; Cunha, Maria G. Carneiro da

This study aimed at the encapsulation of quercetin into lecithin/chitosan nanoparticles using the electrostatic self-assembly technique, followed by evaluation of their functionality (antioxidant activity) and stability at different environmental conditions. These nanoparticles were characterized in terms of: average size, morphology, zeta potential, encapsulation efficiency, loading, and spectroscopic characte...


Development and characterization of hydrogels based on natural polysaccharides ...

Soares, Paulo A. G.; Bourbon, A. I.; Vicente, A. A.; Andrade, Cesar A. S.; Barros Junior, Wilson; Correia, Maria T. S.; Pessoa Júnior, Adalberto

The development of hydrogels based on natural polysaccharides was investigated by preparing mixtures of policaju/chitosan at weight ratios of 1:4 and 2:3. Utilizing dynamic light scattering (DLS) techniques for these mixtures, an increase on the hydrodynamic particle radius was observed varying their pH from 3.0 to 12.0. Furthermore, a reduction of ζ-potential was also observed for the same pH interval. Followi...


Development and characterization of a nanomultilayer coating of pectin and chit...

Medeiros, Bartolomeu G. de S.; Pinheiro, A. C.; Cunha, Maria G. Carneiro da; Vicente, A. A.

A nanomultilayer coating made of food-grade, bio-based materials (consisting of five nanolayers of pectin and chitosan) was produced. This coating was firstly characterized in terms of the water vapor, oxygen and carbon dioxide permeabilities; these parameters exhibited values of 0.019 ± 0.005 × 10−11, 0.069 ± 0.066 × 10−14 and 44.8 ± 32 × 10−14 g m/(Pa s m2), respectively, and are of the same order of magnitud...


Nanostructured films developed through layer-by-layer assembly of k-carrageenan...

Pinheiro, A. C.; Medeiros, Bartolomeu G. de S.; Cunha, Maria G. Carneiro da; Coimbra, Manuel A.; Vicente, A. A.


Production and characterization of protease from Penicillium aurantiogriseum UR...

Rodrigues, Priscila M. B.; Lima, Carolina A.; Filho, José Luiz L.; Teixeira, J. A.; Porto, Ana L. F.; Cunha, Maria G. Carneiro da

Proteases with new properties are required due to their increasing industrial importance. In this work, the optimal fermentation conditions for the production of a protease from Penicillium aurantiogriseum dierchx (URM-4622) are presented together with partial characterization of the protease catalytic properties. The batch fermentation conditions that allow for the highest specific proteolytic activity are 26 ...


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