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Assessment of the Prediction Power of Forced Ageing Methodology on Lager Beer A...

Aguiar, Dayana; Pereira, Ana C.; Marques, José C.

The globalisation of the beer market forces brewers to have methodologies that rapidly evaluate the evolution of beer flavour stability. Commonly used forced ageing methods have limitations since temperature and transportation conditions (temperature, vibrations, long-distance travel, and other factors) impact beer quality. This study assessed the prediction power of a forced ageing methodology on the evolution...


Assessment of the prediction power of forced ageing methodology on lager beer a...

Aguiar, Dayana; Pereira, Ana C.; Marques, José C.

The globalisation of the beer market forces brewers to have methodologies that rapidly evaluate the evolution of beer flavour stability. Commonly used forced ageing methods have limitations since temperature and transportation conditions (temperature, vibrations, long-distance travel, and other factors) impact beer quality. This study assessed the prediction power of a forced ageing methodology on the evolution...


Assessment of Staling Aldehydes in Lager Beer under Maritime Transport and Stor...

Aguiar, Dayana; Pereira, Ana C.; Marques, José C.

Beer flavor stability is greatly influenced by external temperature, vibrations, and longer delivery times. The present study assessed the impact of transport and storage conditions on staling aldehyde evolution in lager beers across five sample groups (fresh, transport, and storage simulation, and their controls), which differed in their bottle opening system (either crown cap or ring pull cap). Maritime trans...


Assessment of Staling Aldehydes in Lager Beer under Maritime Transport and Stor...

Aguiar, Dayana; Pereira, Ana C.; Marques, José C.

: Beer flavor stability is greatly influenced by external temperature, vibrations, and longer delivery times. The present study assessed the impact of transport and storage conditions on staling aldehyde evolution in lager beers across five sample groups (fresh, transport, and storage simulation, and their controls), which differed in their bottle opening system (either crown cap or ring pull cap). Maritime tra...


Unveiling the evolution of Madeira Wine key metabolites: a three-year follow-up...

Pereira, Vanda; Leça, João M.; Freitas, Ana I.; Pereira, Ana C.; Pontes, Marisela; Albuquerque, Francisco; Marques, José C.

Madeira wine (MW) encompasses an unusual oxidative ageing process that makes it distinc tive. Several metabolites have been related to its quality and safety, such as 5-hydroxymethylfurfural (HMF), furfural, sotolon, and ethyl carbamate (EC). These compounds were quantified over a three year period to assess their formation rate according to the ageing procedure used: canteiro vs. estufagem. Estufagem, which in...


New insights into ethyl carbamate occurrence in fortified wines

Leça, João M.; Pereira, Vanda; Miranda, Andreia; Vilchez, José Luis; Marques, José C.

The occurrence of ethyl carbamate (EC) in fortified wines was studied testing different model wines under accelerated ageing (45 °C for 4 months and 70 °C for 1 month), to investigate the possibility of arginine (Arg) being a direct precursor of EC in fortified wines, comparing it with known major precursors, urea and citrulline (Cit). Wine main sugars were appraised as possible catalysts, as previously pointed...


Influence of crop system fruit quality, carotenoids, fatty acids and phenolic c...

Fernandes, Igor; Leça, João M.; Aguiar, Roberto; Fernandes, Tomásia; Marques, José C.; Cordeiro, Nereida

Tomato is one of the most consumed vegetables in the world, and its intake is known to be beneficial for human health. The nutritional quality of tomato is connected with numerous factors namely the cultivation system. To achieve the highest fruit quality and yield, the cherry tomato (Lycopersicon esculentum Mill. var. Moscatel RZ) was cultivated in three cultivation systems and its nutritional quality was eval...


Multi-target optimization of solid phase microextraction to analyse key flavour...

Vieira, Ana C.; Pereira, Ana C.; Marques, José C.; Reis, Marco S.

Despite the literature comprises numerous studies dealing with the analysis of wort and beer flavour-related compounds by HS-SPME followed by GC-MS quantification, no generalized consensus exists regarding the optimal conditions for the extraction procedure. The complex chemistry nature of these matrices, the number of analytes, as well as the number and interactions among parameters affecting the extraction pe...


Is sotolon relevant to the aroma of Madeira Wine blends?

Gaspar, João M.; Freitas, Ana I.; Zhao, Qianzhu; Leça, João M.; Pereira, Vanda; Marques, José C.

Madeira wine (MW) oxidative aging results in the formation of several key aromas. Little is still known about their odor relevance to the aroma of the most commercialized MWs. This report presents an in-depth study of the odor impact of sotolon in MW blends. First, its odor perception was estimated in MWs according to ASTM E679, testing different 3-year-old (3-yo) commercial blends. The odor relevance of sotolo...


Evaluation of fucoxanthin contents in seaweed biomass by vortex-assisted solid-...

Nunes, N.; Leça, João M.; Pereira, Ana C.; Pereira, Vanda; Ferraz, S.; Barreto, Maria Carmo; Marques, José C.; Carvalho, M.A.A. Pinheiro de

Fucoxanthin is considered an important marine bioactive compound with biological properties with promising effects, namely on health. A simple and efficient analytical methodology is proposed for its quantification in seaweed biomass by using vortex-assisted solid-liquid microextraction (VASLME) followed by reversed phase high-performance liquid chromatography (RP-HPLC) photodiode array detection (PDA) analysis...


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