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Application of the QuEChERS method for the determination of organochlorine pest...

Paz, Mário; Correia-Sá, Luísa; Vidal, Carla B.; Becker, Helena; Longhinotti, Elisane; Domingues, Valentina F.; Delerue-Matos, Cristina

The Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method was applied to the extraction of 14 organochlorine pesticides (OCPs) residues from commercial fruit pulps available in supermarkets in Fortaleza, Northeastern Brazil. The analyses were carried out by gas chromatography (GC), coupled to an electron-capture detector (ECD), and were confirmed by GC-tandem mass spectrometry (MS). The parameters o...


Brazilian fruit pulps as functional foods and additives: evaluation of bioactiv...

Paz, Mário; Gúllon, Patricia; Barroso, M. Fátima; Carvalho, Ana P.; Domingues, Valentina F.; Gomes, Ana M.; Becker, Helena; Longhinotti, Elisane

Eight tropical fruit pulps from Brazil were simultaneously characterised in terms of their antioxidant and antimicrobial properties. Antioxidant activity was screened by DPPH radical scavenging activity (126-3987 mg TE/100 g DW) and ferric reduction activity power (368-20819 mg AAE/100 g DW), and complemented with total phenolic content (329-12466 mg GAE/100 g DW) and total flavonoid content measurements (46-67...


Brazilian fruit pulps as functional foods and additives: Evaluation of bioactiv...

Paz, Mário; Gúllon, Patricia; Barroso, M. Fátima; Carvalho, Ana P.; Domingues, Valentina F.; Gomes, Ana M.; Becker, Helena; Longhinotti, Elisane

Eight tropical fruit pulps from Brazil were simultaneously characterised in terms of their antioxidant and antimicrobial properties. Antioxidant activity was screened by DPPH radical scavenging activity (126–3987 mg TE/100 g DW) and ferric reduction activity power (368–20819 mg AAE/100 g DW), and complemented with total phenolic content (329–12466 mg GAE/100 g DW) and total flavonoid content measurements (46–67...


Validation of QuEChERS method for organochlorine pesticides analysis in tamarin...

Paz, Mário; Correia-Sá, Luísa; Becker, Helena; Longhinotti, Elisane; Domingues, Valentina F.; Delerue-Matos, Cristina

In this study a citrate-buffered version of QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) method for determination of 14 organochlorine pesticides (OCPs) residues in tamarind peel, fruit and commercial pulp was optimized using gas chromatography (GC) coupled with electron-capture detector (ECD) and confirmation by GC tandem mass spectrometry (GC–MS/MS). Five procedures were tested based on the origi...


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