The present work concerns the preparation of SAPO-11 materials using microwave (MW) heating during the crystallization process. Different experimental conditions such as crystallization temperature and time were explored, together with different Si sources. The final materials were fully characterized using chemical analysis, XRD diffraction, pyridine adsorption followed by FTIR, nitrogen sorption and NMR spect...
FCHL is a complex disorder with a highly atherogenic profile. The aim of this study is the biochemical/molecular characterization of FCHL patients. Molecular study of LPL, APOAIV, APOAV, APOCIII and USF1 (s1,s2) was performed in 35 index patients by PCR amplification and sequencing. Total cholesterol (TC), HDL-c, sdLDL, triglycerides (TG), apoB and apoCIII were measured in automated analysers. sdLDL was also an...
A Dislipidemia Familiar Combinada (FCHL) é uma doença poligénica caracterizada por hiperlipidemia simples ou combinada, variabilidade intra-individual e intra-familiar do perfil lipídico, ApoB elevada (> 120 mg/dL) e risco elevado de doença cardiovascular (DCV). A sua causa é desconhecida mas alterações nos genes LPL, APOAIV, APOAV, APOCIII e USF1 parecem contribuir para o seu fenótipo. O objectivo deste estudo...
In order to evaluate the performance of several chemicals to control the citrus leprosis mite on orange-trees a test was performed in Rio das Pedras, State of São Paulo, Brazil. The treatments were as follows: A) control; B) fenpropathrin, 13.5g; C) clofentezine, 20.0g; D) biphenthrin, 5.6g: E) binapacryl, 50.0g; F) flubenzimine 60,0g; G) ciexathin, 20.0g. The amounts above are in active ingredients per 100 lit...
In order to control the citrus mite of leprosis, orange trees were sprayed. The following treatments and quantities of active ingredients per hectare were sprayed: A - check; B - hexythiazox, 59. 4g; C - hexythiazox, 89.1g; D - hexythiazox, 118.8 g; E - hexythiazox, 59.4 g+cyhexatin, 123.75g; F-bromopropilate, 371.25g. Each tree received in coverage 3.33 liters of water plus pesticide. Eight evaluations were ma...
Five different insecticides were applied into the mounds of a termite C. cumulans. Fifty mounds were measured, divided in 5 groups (10 nests each) and had pesticide applied. Insecticides were introduced into the center of the nests through a 50-60 cm long canal made from the top to the nucleus with a steel bar. The treatments were as follows: A) 5% granular aldoxicarb (1g); B) 10% EC biphenthrin (0.2g); C) 50% ...
This paper deals with chemical control of the citrus leprosis mite on nature orange trees. The test was carried out in Tietê, State of São Paulo, Brazil (november 1985 - january 1986). The seven treatments were evaluated using plots, with four repetitions (three plants per repetition). Treatments were as follows: A) cyhexatin; B) cyhexatin; C) quinometionate; D) flubenzimine; E) clofentezine; F) clofentezine; G...