Autor(es): Rotta, Maycon [UNESP] ; Motta, Maycon ; Pessoa, Alexsander Lourenço [UNESP] ; Carvalho, Claudio Luiz [UNESP] ; Deimling, Cesar Vanderlei ; Lisboa-Filho, Paulo Noronha [UNESP] ; Ortiz, Wilson Aires ; Zadorosny, Rafael [UNESP]
Data: 2020
Identificador Persistente: http://hdl.handle.net/11449/199900
Origem: Oasisbr
Assunto(s): Acetates; Ceramic; One-pot; Sol-gel; Superconductor; Acetates; Acetates; Ceramic; Ceramic; One-pot; One-pot; Sol-gel; Sol-gel; Superconductor; Superconductor
Made available in DSpace on 2020-12-12T01:52:21Z (GMT). No. of bitstreams: 0 Previous issue date: 2020-03-01
Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
ASCRS Research Foundation
Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
There are a variety of chemical routes used to produce advanced ceramic materials. The sol-gel-like methods are widely applied since the final samples present high stoichiometric and grain size homogeneity. However, with the search for sustainable practices, researchers have been worked in the so-called one-pot synthesis, where all the chemical reactions occur in a single vessel with low residue production. Thus, in this work, we used a one-pot-like synthesis adapted to produce YBa2Cu3O7-δ superconducting ceramic samples. One shows that, in two main steps, a polymer solution is prepared in a few hours, and after heat treatments, a single-phase material is obtained. It is shown that the one-pot-like samples can present a higher diamagnetic signal in comparison with specimens prepared by the well-known Pechini Method. With this work, we show that there are alternative routes to produce advanced ceramics with simple and secure methods, if we compare, e.g., with trifluoroacetate routes.
Departamento de Física e Química Universidade Estadual Paulista (UNESP) Faculdade de Engenharia, Caixa Postal 31, Ilha Solteira
Instituto Federal de Educação Ciência e Tecnologia de Mato Grosso do Sul (IFMS) Campus Três Lagoas, Três Lagoas
Departamento de Física Universidade Federal de São Carlos - UFSCar, São Carlos
Departamento Acadêmico de Física Universidade Tecnológica Federal do Paraná - UTFPR, Campo Mourão
Departamento de Física Universidade Estadual Paulista (UNESP) Faculdade de Ciências, Caixa Postal 473, Bauru
Departamento de Física e Química Universidade Estadual Paulista (UNESP) Faculdade de Engenharia, Caixa Postal 31, Ilha Solteira
Departamento de Física Universidade Estadual Paulista (UNESP) Faculdade de Ciências, Caixa Postal 473, Bauru
FAPESP: 2016/12390-6
CNPq: 302564/2018-7
