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An enzymatic route to a benzocarbazole framework using bacterial CotA laccase

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Detalhes bibliográficos
Resumo:The CotA laccase-catalysed oxidation of the meta, para-disubstituted arylamine 2,4-diaminophenyldiamine delivers, under mild reaction conditions, a benzocarbazole derivative (1) (74% yield), a key structural motif of a diverse range of applications. This work extends the scope of aromatic frameworks obtained using these enzymes and represents a new efficient and clean method to construct in one step C-C and C-N bonds.
Autores principais:Sousa, Ana Catarina
Outros Autores:Piedade, Maria de Fátima M. M.; Martins, Lígia O.; Robalo, Maria Paula
Assunto:Active carbazole alkaloids Transition-Metal-Complexes Organic-Synthesis Fungal laccases Antimicrobial activity Biological evaluation Coupling reactions Bacillus-subtilis Domino reactions Green chemistry
Ano:2015
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso restrito
Instituição associada:Instituto Politécnico de Lisboa
Idioma:inglês
Origem:Repositório Científico do Instituto Politécnico de Lisboa
Descrição
Resumo:The CotA laccase-catalysed oxidation of the meta, para-disubstituted arylamine 2,4-diaminophenyldiamine delivers, under mild reaction conditions, a benzocarbazole derivative (1) (74% yield), a key structural motif of a diverse range of applications. This work extends the scope of aromatic frameworks obtained using these enzymes and represents a new efficient and clean method to construct in one step C-C and C-N bonds.