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Physical characterization of rice starch spherical aggregates produced by spray-drying

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Resumo:The effect of solids content and the presence of bonding agents (CMC and/or gelatin) on the physical characteristics of rice starch spherical aggregates were investigated. Rice starch spherules were produced by spray-drying at 120 °C according to a 2(k − p) Fractional Factorial Designs at 2 Levels. Particle size analysis, spherules’ morphology, porosity and crystallinity determination were obtained for the aggregates produced. Results showed that the size of spherules is significantly affected by starch concentration while the presence of bonding agents seems not to have a direct influence in particle size. The drying process did not yield a change in crystal type but the presence of gelatin leads to a decrease in crystalline regions. Starch and bonding agents’ concentrations did not significantly affect neither the total porosity of the samples nor the average pore diameter. Intra-particle porosity is mainly dependent on starch and gelatin concentrations. This study would be helpful in establishing the more adequate conditions useful in an industrial application on encapsulating bioactive compounds.
Autores principais:Costa, Sara Beirão da
Outros Autores:Duarte, Cláudia; Martins, Margarida Moldão; Costa, M. Luísa Beirão da
Assunto:Starch Spherules Morphology Porosity Spray-drying
Ano:2011
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso restrito
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Costa, Sara Beirão da
author2 Duarte, Cláudia
Martins, Margarida Moldão
Costa, M. Luísa Beirão da
author2_role author
author
author
author_facet Costa, Sara Beirão da
Duarte, Cláudia
Martins, Margarida Moldão
Costa, M. Luísa Beirão da
author_role author
contributor_name_str_mv RepositóriUM - Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Costa, Sara Beirão da\"},{\"Person.name\":\"Duarte, Cláudia\"},{\"Person.name\":\"Martins, Margarida Moldão\"},{\"Person.name\":\"Costa, M. Luísa Beirão da\"}]
datacite.contributors.contributor.contributorName.fl_str_mv RepositóriUM - Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Costa, Sara Beirão da
Duarte, Cláudia
Martins, Margarida Moldão
Costa, M. Luísa Beirão da
datacite.date.Accepted.fl_str_mv 2011-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2012-02-03T14:57:55Z
datacite.date.embargoed.fl_str_mv 2012-02-03T14:57:55Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_16ec
datacite.subjects.subject.fl_str_mv Starch
Spherules
Morphology
Porosity
Spray-drying
datacite.titles.title.fl_str_mv Physical characterization of rice starch spherical aggregates produced by spray-drying
dc.contributor.none.fl_str_mv RepositóriUM - Universidade do Minho
dc.creator.none.fl_str_mv Costa, Sara Beirão da
Duarte, Cláudia
Martins, Margarida Moldão
Costa, M. Luísa Beirão da
dc.date.Accepted.fl_str_mv 2011-01-01T00:00:00Z
dc.date.available.fl_str_mv 2012-02-03T14:57:55Z
dc.date.embargoed.fl_str_mv 2012-02-03T14:57:55Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/16789
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Elsevier
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_16ec
dc.subject.none.fl_str_mv Starch
Spherules
Morphology
Porosity
Spray-drying
dc.title.fl_str_mv Physical characterization of rice starch spherical aggregates produced by spray-drying
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description The effect of solids content and the presence of bonding agents (CMC and/or gelatin) on the physical characteristics of rice starch spherical aggregates were investigated. Rice starch spherules were produced by spray-drying at 120 °C according to a 2(k − p) Fractional Factorial Designs at 2 Levels. Particle size analysis, spherules’ morphology, porosity and crystallinity determination were obtained for the aggregates produced. Results showed that the size of spherules is significantly affected by starch concentration while the presence of bonding agents seems not to have a direct influence in particle size. The drying process did not yield a change in crystal type but the presence of gelatin leads to a decrease in crystalline regions. Starch and bonding agents’ concentrations did not significantly affect neither the total porosity of the samples nor the average pore diameter. Intra-particle porosity is mainly dependent on starch and gelatin concentrations. This study would be helpful in establishing the more adequate conditions useful in an industrial application on encapsulating bioactive compounds.
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eu_rights_str_mv restrictedAccess
format article
fulltext.url.fl_str_mv https://repositorium.uminho.pt/bitstreams/a617df31-fc5c-4a87-bb4e-a511f305a0f0/download
id rum_1bb3f240b13bd4fb19acdf5cd0bb481f
identifier.url.fl_str_mv https://hdl.handle.net/1822/16789
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/16789
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Costa, Sara Beirão da
Duarte, Cláudia
Martins, Margarida Moldão
Costa, M. Luísa Beirão da
publishDate 2011
publisher.none.fl_str_mv Elsevier
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engElsevierporThe effect of solids content and the presence of bonding agents (CMC and/or gelatin) on the physical characteristics of rice starch spherical aggregates were investigated. Rice starch spherules were produced by spray-drying at 120 °C according to a 2(k − p) Fractional Factorial Designs at 2 Levels. Particle size analysis, spherules’ morphology, porosity and crystallinity determination were obtained for the aggregates produced. Results showed that the size of spherules is significantly affected by starch concentration while the presence of bonding agents seems not to have a direct influence in particle size. The drying process did not yield a change in crystal type but the presence of gelatin leads to a decrease in crystalline regions. Starch and bonding agents’ concentrations did not significantly affect neither the total porosity of the samples nor the average pore diameter. Intra-particle porosity is mainly dependent on starch and gelatin concentrations. This study would be helpful in establishing the more adequate conditions useful in an industrial application on encapsulating bioactive compounds.application/pdfporPhysical characterization of rice starch spherical aggregates produced by spray-dryingCosta, Sara Beirão daDuarte, CláudiaMartins, Margarida MoldãoCosta, M. Luísa Beirão daHostingInstitutionOrganizationalRepositóriUM - Universidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptISSNIsPartOf0260-8774DOIIsPartOf10.1016/j.jfoodeng.2010.11.0242012-02-03T14:57:55Z201120102011-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/16789http://purl.org/coar/access_right/c_16ecrestricted accessStarchSpherulesMorphologyPorositySpray-drying1972268 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_16ecapplication/pdffulltexthttps://repositorium.uminho.pt/bitstreams/a617df31-fc5c-4a87-bb4e-a511f305a0f0/download
spellingShingle Physical characterization of rice starch spherical aggregates produced by spray-drying
Costa, Sara Beirão da
Starch
Spherules
Morphology
Porosity
Spray-drying
status SINGLETON
subject.fl_str_mv Starch
Spherules
Morphology
Porosity
Spray-drying
title Physical characterization of rice starch spherical aggregates produced by spray-drying
title_full Physical characterization of rice starch spherical aggregates produced by spray-drying
title_fullStr Physical characterization of rice starch spherical aggregates produced by spray-drying
title_full_unstemmed Physical characterization of rice starch spherical aggregates produced by spray-drying
title_short Physical characterization of rice starch spherical aggregates produced by spray-drying
title_sort Physical characterization of rice starch spherical aggregates produced by spray-drying
topic Starch
Spherules
Morphology
Porosity
Spray-drying
topic_facet Starch
Spherules
Morphology
Porosity
Spray-drying
url https://hdl.handle.net/1822/16789
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