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COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey

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Resumo:Honey is a widely consumed food product frequently subjected to adulteration, with the mislabeling of its botanical or geographical origin being one of the most common practices. Determining the entomological origin of honey is particularly challenging but of high relevance for ensuring its authenticity, especially for products with protected designation of origin (PDO) labels. This study presents a novel DNA metabarcoding approach targeting a highly informative 406 bp fragment of the cytochrome c oxidase I (COI) gene to differentiate among the three major mitochondrial lineages (A, M, and C) of honey bees (Apis mellifera L.) native to Europe. The target region was selected based on the calculated fixation index (FST), which is frequently used in Population Genetics as a measure of differentiation between populations. The approach was validated with 11 honey samples of known entomological origin and applied to 44 commercial honeys from 13 countries. The approach demonstrated high sensitivity, accurately identifying the entomological origin of honey, including samples produced by honey bees of varying ancestries, which could not be resolved by previous methods based on real-time PCR coupled with high-resolution melting (PCR-HRM) analysis. The results demonstrate the effectiveness of COI metabarcoding in verifying honey authenticity and highlight the predominance of C-lineage honey bees in the production of commercial honeys from northwestern Europe. This finding suggests a limited presence of the native M-lineage ancestry, underscoring the need for conservation efforts.
Autores principais:Honrado, Mónica
Outros Autores:Quaresma, Andreia; Henriques, Dora; Pinto, M. Alice; Amaral, Joana S.
Assunto:Entomologic origin Apis mellifera MtDNA NA metabarcoding Honey COI gene
Ano:2025
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Instituto Politécnico de Bragança
Idioma:inglês
Origem:Biblioteca Digital do IPB
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author Honrado, Mónica
author2 Quaresma, Andreia
Henriques, Dora
Pinto, M. Alice
Amaral, Joana S.
author2_role author
author
author
author
author_facet Honrado, Mónica
Quaresma, Andreia
Henriques, Dora
Pinto, M. Alice
Amaral, Joana S.
author_role author
contributor_name_str_mv Biblioteca Digital do IPB
country_str PT
creators_json_txt [{\"Person.name\":\"Honrado, Mónica\",\"Person.identifier.orcid\":\"0000-0002-5126-4693\"},{\"Person.name\":\"Quaresma, Andreia\",\"Person.identifier.orcid\":\"0000-0002-8678-5800\"},{\"Person.name\":\"Henriques, Dora\",\"Person.identifier.orcid\":\"0000-0001-7530-682X\"},{\"Person.name\":\"Pinto, M. Alice\",\"Person.identifier.orcid\":\"0000-0001-9663-8399\"},{\"Person.name\":\"Amaral, Joana S.\",\"Person.identifier.orcid\":\"0000-0002-3648-7303\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Biblioteca Digital do IPB
datacite.creators.creator.creatorName.fl_str_mv Honrado, Mónica
Quaresma, Andreia
Henriques, Dora
Pinto, M. Alice
Amaral, Joana S.
datacite.date.Accepted.fl_str_mv 2025-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2025-04-07T14:18:15Z
datacite.date.embargoed.fl_str_mv 2025-04-07T14:18:15Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Entomologic origin
Apis mellifera
MtDNA
NA metabarcoding
Honey
COI gene
datacite.titles.title.fl_str_mv COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
dc.contributor.none.fl_str_mv Biblioteca Digital do IPB
dc.creator.none.fl_str_mv Honrado, Mónica
Quaresma, Andreia
Henriques, Dora
Pinto, M. Alice
Amaral, Joana S.
dc.date.Accepted.fl_str_mv 2025-01-01T00:00:00Z
dc.date.available.fl_str_mv 2025-04-07T14:18:15Z
dc.date.embargoed.fl_str_mv 2025-04-07T14:18:15Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10198/34399
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv MDPI
dc.rights.cclincense.fl_str_mv http://creativecommons.org/licenses/by/4.0/
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Entomologic origin
Apis mellifera
MtDNA
NA metabarcoding
Honey
COI gene
dc.title.fl_str_mv COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description Honey is a widely consumed food product frequently subjected to adulteration, with the mislabeling of its botanical or geographical origin being one of the most common practices. Determining the entomological origin of honey is particularly challenging but of high relevance for ensuring its authenticity, especially for products with protected designation of origin (PDO) labels. This study presents a novel DNA metabarcoding approach targeting a highly informative 406 bp fragment of the cytochrome c oxidase I (COI) gene to differentiate among the three major mitochondrial lineages (A, M, and C) of honey bees (Apis mellifera L.) native to Europe. The target region was selected based on the calculated fixation index (FST), which is frequently used in Population Genetics as a measure of differentiation between populations. The approach was validated with 11 honey samples of known entomological origin and applied to 44 commercial honeys from 13 countries. The approach demonstrated high sensitivity, accurately identifying the entomological origin of honey, including samples produced by honey bees of varying ancestries, which could not be resolved by previous methods based on real-time PCR coupled with high-resolution melting (PCR-HRM) analysis. The results demonstrate the effectiveness of COI metabarcoding in verifying honey authenticity and highlight the predominance of C-lineage honey bees in the production of commercial honeys from northwestern Europe. This finding suggests a limited presence of the native M-lineage ancestry, underscoring the need for conservation efforts.
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eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://bibliotecadigital.ipb.pt/bitstreams/85092375-38c6-4166-aba3-e24c736976c9/download
id ipb_28fcab2aeb903eda097ca30a1e5a53a4
identifier.url.fl_str_mv http://hdl.handle.net/10198/34399
instacron_str ipb
institution Instituto Politécnico de Bragança
instname_str Instituto Politécnico de Bragança
language eng
network_acronym_str ipb
network_name_str Biblioteca Digital do IPB
oai_identifier_str oai:bibliotecadigital.ipb.pt:10198/34399
organization_str_mv urn:organizationAcronym:ipb
person_str_mv Honrado, Mónica
Honrado, Mónica
https://www.ciencia-id.pt/4712-B40B-4B0E
4712-B40B-4B0E
http://orcid.org/0000-0002-5126-4693
0000-0002-5126-4693
Quaresma, Andreia
Quaresma, Andreia
https://www.ciencia-id.pt/4F1A-4E4A-3F23
4F1A-4E4A-3F23
http://orcid.org/0000-0002-8678-5800
0000-0002-8678-5800
Henriques, Dora
Henriques, Dora
https://www.ciencia-id.pt/291F-986F-07DA
291F-986F-07DA
http://orcid.org/0000-0001-7530-682X
0000-0001-7530-682X
Pinto, M. Alice
Pinto, M. Alice
https://www.ciencia-id.pt/F814-A1D0-8318
F814-A1D0-8318
http://orcid.org/0000-0001-9663-8399
0000-0001-9663-8399
Amaral, Joana S.
Amaral, Joana S.
https://www.ciencia-id.pt/5319-7DE8-BEDA
5319-7DE8-BEDA
http://orcid.org/0000-0002-3648-7303
0000-0002-3648-7303
publishDate 2025
publisher.none.fl_str_mv MDPI
reponame_str Biblioteca Digital do IPB
repository_id_str urn:repositoryAcronym:ipb
service_str_mv urn:repositoryAcronym:ipb
spelling engMDPIengHoney is a widely consumed food product frequently subjected to adulteration, with the mislabeling of its botanical or geographical origin being one of the most common practices. Determining the entomological origin of honey is particularly challenging but of high relevance for ensuring its authenticity, especially for products with protected designation of origin (PDO) labels. This study presents a novel DNA metabarcoding approach targeting a highly informative 406 bp fragment of the cytochrome c oxidase I (COI) gene to differentiate among the three major mitochondrial lineages (A, M, and C) of honey bees (Apis mellifera L.) native to Europe. The target region was selected based on the calculated fixation index (FST), which is frequently used in Population Genetics as a measure of differentiation between populations. The approach was validated with 11 honey samples of known entomological origin and applied to 44 commercial honeys from 13 countries. The approach demonstrated high sensitivity, accurately identifying the entomological origin of honey, including samples produced by honey bees of varying ancestries, which could not be resolved by previous methods based on real-time PCR coupled with high-resolution melting (PCR-HRM) analysis. The results demonstrate the effectiveness of COI metabarcoding in verifying honey authenticity and highlight the predominance of C-lineage honey bees in the production of commercial honeys from northwestern Europe. This finding suggests a limited presence of the native M-lineage ancestry, underscoring the need for conservation efforts.application/pdfengCOI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European HoneyPersonalHonrado, MónicaDSpacehttp://dspace.org/items/87f8840d-04b1-427a-bca9-d37eadfc0e9bDSpacehttp://dspace.org/items/87f8840d-04b1-427a-bca9-d37eadfc0e9bHonradoMónicaCiência IDhttps://www.ciencia-id.pt4712-B40B-4B0EORCIDhttp://orcid.org0000-0002-5126-4693PersonalQuaresma, AndreiaDSpacehttp://dspace.org/items/d417b0ac-c8ee-473a-a355-820b5b9a3f55DSpacehttp://dspace.org/items/d417b0ac-c8ee-473a-a355-820b5b9a3f55QuaresmaAndreiaCiência IDhttps://www.ciencia-id.pt4F1A-4E4A-3F23ORCIDhttp://orcid.org0000-0002-8678-5800Scopus Author IDhttps://www.scopus.com57119742600PersonalHenriques, DoraDSpacehttp://dspace.org/items/d2abd09f-a90c-4cfb-9a60-7fc32f56184dDSpacehttp://dspace.org/items/d2abd09f-a90c-4cfb-9a60-7fc32f56184dHenriquesDoraCiência IDhttps://www.ciencia-id.pt291F-986F-07DAORCIDhttp://orcid.org0000-0001-7530-682XScopus Author IDhttps://www.scopus.com55761737300PersonalPinto, M. AliceDSpacehttp://dspace.org/items/0667fe04-7078-483d-9198-56d167b19bc5DSpacehttp://dspace.org/items/0667fe04-7078-483d-9198-56d167b19bc5PintoM. AliceCiência IDhttps://www.ciencia-id.ptF814-A1D0-8318ORCIDhttp://orcid.org0000-0001-9663-8399Scopus Author IDhttps://www.scopus.com8085507800PersonalAmaral, Joana S.DSpacehttp://dspace.org/items/42be2cf4-adc4-4e7f-ac60-7aab515b38cdDSpacehttp://dspace.org/items/42be2cf4-adc4-4e7f-ac60-7aab515b38cdAmaralJoana S.Ciência IDhttps://www.ciencia-id.pt5319-7DE8-BEDAORCIDhttp://orcid.org0000-0002-3648-7303HostingInstitutionOrganizationalBiblioteca Digital do IPBe-mailmailto:dspace@ipb.ptdspace@ipb.ptISSNIsPartOf2304-8158DOIIsPartOf10.3390/foods140304192025-04-07T14:18:15Z20252025-01-01T00:00:00ZHandlehttp://hdl.handle.net/10198/34399http://purl.org/coar/access_right/c_abf2open accessEntomologic originApis melliferaMtDNANA metabarcodingHoneyCOI gene756595 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal article2025http://creativecommons.org/licenses/by/4.0/http://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://bibliotecadigital.ipb.pt/bitstreams/85092375-38c6-4166-aba3-e24c736976c9/downloadFoods143115
spellingShingle COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
Honrado, Mónica
Entomologic origin
Apis mellifera
MtDNA
NA metabarcoding
Honey
COI gene
status SINGLETON
subject.fl_str_mv Entomologic origin
Apis mellifera
MtDNA
NA metabarcoding
Honey
COI gene
title COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
title_full COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
title_fullStr COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
title_full_unstemmed COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
title_short COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
title_sort COI Metabarcoding as a Novel Approach for Assessing the Honey Bee Source of European Honey
topic Entomologic origin
Apis mellifera
MtDNA
NA metabarcoding
Honey
COI gene
topic_facet Entomologic origin
Apis mellifera
MtDNA
NA metabarcoding
Honey
COI gene
url http://hdl.handle.net/10198/34399
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