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Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue

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Summary:This study successfully applied a potentiometric E-tongue with 20 cross-selectivity lipidic polymeric membranes in the discrimination of three semi-quantitative groups, that represented the following intervals of honey adulteration percentage with cane sugar: 0 %; [0, 10]%; [10, 20]% of adulteration. We analysed five different types of Portuguese honey; five brands of cane sugar were added to the adulterated samples; a comparative analysis was then performed. Linear discriminant analysis coupled with a tabu search algorithm for feature selection was applied to the ETongue's analytical data to select the best model. A discriminant model with 12 sensors was obtained. This model classified correctly all samples in both in internal (train data, 15 samples) and external validation (test data,10 samples). Also, multiple linear regression with tabu search was applied to verify if ETongue's data would allow quantifying the honey's adulteration level. The results showed that it was possible to obtain a quantitative model but with unsatisfactory predictive performance in the test data group (external validation), giving, in general, values below the expected concentrations. E-tongue is a real-time green, flexible and low-cost analytical tool that requires minimum sample preparation and no special technical skills, being a promising tool for everyday application.
Main Authors:Dias, L.G.
Other Authors:Bruni, Andressa R.S.; Anizelli, Camilla P.; Zangirolami, Marcela de Souza; Lima, Patrícia C.; Estevinho, Leticia M.; Bona, Evandro
Subject:Adulterated honey Linear discriminant analysis Multiple linear regression Potentiometric E-Tongue Tabu search
Year:2022
Country:Portugal
Document type:article
Access type:open access
Associated institution:Instituto Politécnico de Bragança
Language:English
Origin:Biblioteca Digital do IPB
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author Dias, L.G.
author2 Bruni, Andressa R.S.
Anizelli, Camilla P.
Zangirolami, Marcela de Souza
Lima, Patrícia C.
Estevinho, Leticia M.
Bona, Evandro
author2_role author
author
author
author
author
author
author_facet Dias, L.G.
Bruni, Andressa R.S.
Anizelli, Camilla P.
Zangirolami, Marcela de Souza
Lima, Patrícia C.
Estevinho, Leticia M.
Bona, Evandro
author_role author
contributor_name_str_mv Biblioteca Digital do IPB
country_str PT
creators_json_txt [{\"Person.name\":\"Dias, L.G.\",\"Person.identifier.orcid\":\"0000-0002-1210-4259\"},{\"Person.name\":\"Bruni, Andressa R.S.\"},{\"Person.name\":\"Anizelli, Camilla P.\"},{\"Person.name\":\"Zangirolami, Marcela de Souza\"},{\"Person.name\":\"Lima, Patrícia C.\"},{\"Person.name\":\"Estevinho, Leticia M.\",\"Person.identifier.orcid\":\"0000-0002-9249-1948\"},{\"Person.name\":\"Bona, Evandro\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Biblioteca Digital do IPB
datacite.creators.creator.creatorName.fl_str_mv Dias, L.G.
Bruni, Andressa R.S.
Anizelli, Camilla P.
Zangirolami, Marcela de Souza
Lima, Patrícia C.
Estevinho, Leticia M.
Bona, Evandro
datacite.date.Accepted.fl_str_mv 2022-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2023-08-03T10:48:25Z
datacite.date.embargoed.fl_str_mv 2023-08-03T10:48:25Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Adulterated honey
Linear discriminant analysis
Multiple linear regression
Potentiometric E-Tongue
Tabu search
datacite.titles.title.fl_str_mv Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
dc.contributor.none.fl_str_mv Biblioteca Digital do IPB
dc.creator.none.fl_str_mv Dias, L.G.
Bruni, Andressa R.S.
Anizelli, Camilla P.
Zangirolami, Marcela de Souza
Lima, Patrícia C.
Estevinho, Leticia M.
Bona, Evandro
dc.date.Accepted.fl_str_mv 2022-01-01T00:00:00Z
dc.date.available.fl_str_mv 2023-08-03T10:48:25Z
dc.date.embargoed.fl_str_mv 2023-08-03T10:48:25Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10198/28671
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv John Wiley & Sons
dc.rights.cclincense.fl_str_mv http://creativecommons.org/licenses/by/4.0/
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Adulterated honey
Linear discriminant analysis
Multiple linear regression
Potentiometric E-Tongue
Tabu search
dc.title.fl_str_mv Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description This study successfully applied a potentiometric E-tongue with 20 cross-selectivity lipidic polymeric membranes in the discrimination of three semi-quantitative groups, that represented the following intervals of honey adulteration percentage with cane sugar: 0 %; [0, 10]%; [10, 20]% of adulteration. We analysed five different types of Portuguese honey; five brands of cane sugar were added to the adulterated samples; a comparative analysis was then performed. Linear discriminant analysis coupled with a tabu search algorithm for feature selection was applied to the ETongue's analytical data to select the best model. A discriminant model with 12 sensors was obtained. This model classified correctly all samples in both in internal (train data, 15 samples) and external validation (test data,10 samples). Also, multiple linear regression with tabu search was applied to verify if ETongue's data would allow quantifying the honey's adulteration level. The results showed that it was possible to obtain a quantitative model but with unsatisfactory predictive performance in the test data group (external validation), giving, in general, values below the expected concentrations. E-tongue is a real-time green, flexible and low-cost analytical tool that requires minimum sample preparation and no special technical skills, being a promising tool for everyday application.
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eu_rights_str_mv openAccess
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fulltext.url.fl_str_mv https://bibliotecadigital.ipb.pt/bitstreams/5ada2b73-1817-4788-a150-61be72cac99d/download
funding.funder.alternateName_str_mv FCT
FCT
funding.funder.identifier_str_mv http://doi.org/10.13039/501100001871
http://doi.org/10.13039/501100001871
funding.funder.name_str_mv Fundação para a Ciência e a Tecnologia
Fundação para a Ciência e a Tecnologia
funding.name_str_mv 6817 - DCRRNI ID
6817 - DCRRNI ID
id ipb_4920329eef3e962fed14074cebe23ebd
identifier.url.fl_str_mv http://hdl.handle.net/10198/28671
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institution Instituto Politécnico de Bragança
instname_str Instituto Politécnico de Bragança
language eng
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network_name_str Biblioteca Digital do IPB
oai_identifier_str oai:bibliotecadigital.ipb.pt:10198/28671
organization_str_mv urn:organizationAcronym:ipb
person_str_mv Dias, L.G.
Dias, L.G.
https://www.ciencia-id.pt/2F11-9092-FAAF
2F11-9092-FAAF
http://orcid.org/0000-0002-1210-4259
0000-0002-1210-4259
Bruni, Andressa R.S.
Anizelli, Camilla P.
Zangirolami, Marcela de Souza
Lima, Patrícia C.
Estevinho, Leticia M.
Estevinho, Leticia M.
https://www.ciencia-id.pt/BA14-09D6-A406
BA14-09D6-A406
http://orcid.org/0000-0002-9249-1948
0000-0002-9249-1948
Bona, Evandro
publishDate 2022
publisher.none.fl_str_mv John Wiley & Sons
reponame_str Biblioteca Digital do IPB
repository_id_str urn:repositoryAcronym:ipb
service_str_mv urn:repositoryAcronym:ipb
spelling engJohn Wiley & Sonspt_PTThis study successfully applied a potentiometric E-tongue with 20 cross-selectivity lipidic polymeric membranes in the discrimination of three semi-quantitative groups, that represented the following intervals of honey adulteration percentage with cane sugar: 0 %; [0, 10]%; [10, 20]% of adulteration. We analysed five different types of Portuguese honey; five brands of cane sugar were added to the adulterated samples; a comparative analysis was then performed. Linear discriminant analysis coupled with a tabu search algorithm for feature selection was applied to the ETongue's analytical data to select the best model. A discriminant model with 12 sensors was obtained. This model classified correctly all samples in both in internal (train data, 15 samples) and external validation (test data,10 samples). Also, multiple linear regression with tabu search was applied to verify if ETongue's data would allow quantifying the honey's adulteration level. The results showed that it was possible to obtain a quantitative model but with unsatisfactory predictive performance in the test data group (external validation), giving, in general, values below the expected concentrations. E-tongue is a real-time green, flexible and low-cost analytical tool that requires minimum sample preparation and no special technical skills, being a promising tool for everyday application.application/pdfpt_PTSemi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETonguePersonalDias, L.G.DSpacehttp://dspace.org/items/eac8c166-4056-4ed0-8d8d-7ecb2c4481a5DSpacehttp://dspace.org/items/eac8c166-4056-4ed0-8d8d-7ecb2c4481a5DiasLuís G.Ciência IDhttps://www.ciencia-id.pt2F11-9092-FAAFORCIDhttp://orcid.org0000-0002-1210-4259Scopus Author IDhttps://www.scopus.com23569169900Bruni, Andressa R.S.Anizelli, Camilla P.Zangirolami, Marcela de SouzaLima, Patrícia C.PersonalEstevinho, Leticia M.DSpacehttp://dspace.org/items/4a1d5ba2-1854-4ca5-89a4-73f35e964df9DSpacehttp://dspace.org/items/4a1d5ba2-1854-4ca5-89a4-73f35e964df9EstevinhoLetícia M.Ciência IDhttps://www.ciencia-id.ptBA14-09D6-A406ORCIDhttp://orcid.org0000-0002-9249-1948Scopus Author IDhttps://www.scopus.com6506577664Scopus Author IDhttps://www.scopus.com57211945650Bona, EvandroHostingInstitutionOrganizationalBiblioteca Digital do IPBe-mailmailto:dspace@ipb.ptdspace@ipb.ptISSNIsPartOf1612-1872DOIIsPartOf10.1002/cbdv.2022006982023-08-03T10:48:25Z20222022-01-01T00:00:00ZHandlehttp://hdl.handle.net/10198/28671http://purl.org/coar/access_right/c_abf2open accessAdulterated honeyLinear discriminant analysisMultiple linear regressionPotentiometric E-TongueTabu search3753936 bytesFundação para a Ciência e a TecnologiaMountain Research Center6817 - DCRRNI IDCrossref Funder IDhttp://doi.org/10.13039/501100001871Fundação para a Ciência e a TecnologiaMountain Research Center6817 - DCRRNI IDCrossref Funder IDhttp://doi.org/10.13039/501100001871literaturehttp://purl.org/coar/resource_type/c_6501journal article2022http://creativecommons.org/licenses/by/4.0/http://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://bibliotecadigital.ipb.pt/bitstreams/5ada2b73-1817-4788-a150-61be72cac99d/downloadChemistry & Biodiversity1911
spellingShingle Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
Dias, L.G.
Adulterated honey
Linear discriminant analysis
Multiple linear regression
Potentiometric E-Tongue
Tabu search
status SINGLETON
subject.fl_str_mv Adulterated honey
Linear discriminant analysis
Multiple linear regression
Potentiometric E-Tongue
Tabu search
title Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
title_full Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
title_fullStr Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
title_full_unstemmed Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
title_short Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
title_sort Semi‐quantitative discrimination of honey adulterated with cane sugar solution by an ETongue
topic Adulterated honey
Linear discriminant analysis
Multiple linear regression
Potentiometric E-Tongue
Tabu search
topic_facet Adulterated honey
Linear discriminant analysis
Multiple linear regression
Potentiometric E-Tongue
Tabu search
url http://hdl.handle.net/10198/28671
visible 1