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Greener terpene-terpene eutectic mixtures as hydrophobic solvents

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Resumo:Natural products can be the basis for the development of green solvents, relevant for the advancement of new, more sustainable processes and products. In this work, 10 binary mixtures constituted by terpenes are prepared and characterized. Their solid−liquid phase diagrams show that room-temperature solvents can be prepared from solid terpenes in a wide composition range. These diagrams are accurately described by the conductor-like screening model for real solvents, showing it to be a useful predictive tool for the design of novel natural solvents. At the eutectic point, these mixtures possess low viscosities, densities lower than water, and high boiling temperatures. The low water solubility in the eutectic solvents together with its negligible impact on the properties measured is a strong indicator of the hydrophobic character of these mixtures. The tunable character of these mixtures is demonstrated by studying the solvatochromic parameters in the entire concentration region, the properties of the final solvents being tuned by simply varying the mole fraction of the terpenes. The high potential of this tunable character is shown in the selective extraction of dyes from their aqueous solutions. This work is expected to devise new insights concerning these solvents as well as to boost their application in green industrial processes.
Autores principais:Martins, Mónia A.R.
Outros Autores:Silva, Liliana P.; Schaeffer, Nicolas; Abranches, Dinis O.; Maximo, Guilherme J.; Pinho, Simão; Coutinho, João A.P.
Assunto:COSMO-RS Eutectic mixtures Physicochemical properties SLE Terpenes Tunable
Ano:2019
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Instituto Politécnico de Bragança
Idioma:inglês
Origem:Biblioteca Digital do IPB
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author Martins, Mónia A.R.
author2 Silva, Liliana P.
Schaeffer, Nicolas
Abranches, Dinis O.
Maximo, Guilherme J.
Pinho, Simão
Coutinho, João A.P.
author2_role author
author
author
author
author
author
author_facet Martins, Mónia A.R.
Silva, Liliana P.
Schaeffer, Nicolas
Abranches, Dinis O.
Maximo, Guilherme J.
Pinho, Simão
Coutinho, João A.P.
author_role author
contributor_name_str_mv Biblioteca Digital do IPB
country_str PT
creators_json_str [{\"Person.name\":\"Martins, Mónia A.R.\"},{\"Person.name\":\"Silva, Liliana P.\"},{\"Person.name\":\"Schaeffer, Nicolas\"},{\"Person.name\":\"Abranches, Dinis O.\"},{\"Person.name\":\"Maximo, Guilherme J.\"},{\"Person.name\":\"Pinho, Simão\",\"Person.identifier.orcid\":\"0000-0002-9211-857X\"},{\"Person.name\":\"Coutinho, João A.P.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Biblioteca Digital do IPB
datacite.creators.creator.creatorName.fl_str_mv Martins, Mónia A.R.
Silva, Liliana P.
Schaeffer, Nicolas
Abranches, Dinis O.
Maximo, Guilherme J.
Pinho, Simão
Coutinho, João A.P.
datacite.date.Accepted.fl_str_mv 2019-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2018-01-19T10:00:00Z
datacite.date.embargoed.fl_str_mv 2018-01-19T10:00:00Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv COSMO-RS
Eutectic mixtures
Physicochemical properties
SLE
Terpenes
Tunable
datacite.titles.title.fl_str_mv Greener terpene-terpene eutectic mixtures as hydrophobic solvents
dc.contributor.none.fl_str_mv Biblioteca Digital do IPB
dc.creator.none.fl_str_mv Martins, Mónia A.R.
Silva, Liliana P.
Schaeffer, Nicolas
Abranches, Dinis O.
Maximo, Guilherme J.
Pinho, Simão
Coutinho, João A.P.
dc.date.Accepted.fl_str_mv 2019-01-01T00:00:00Z
dc.date.available.fl_str_mv 2018-01-19T10:00:00Z
dc.date.embargoed.fl_str_mv 2018-01-19T10:00:00Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10198/20237
dc.language.none.fl_str_mv eng
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv COSMO-RS
Eutectic mixtures
Physicochemical properties
SLE
Terpenes
Tunable
dc.title.fl_str_mv Greener terpene-terpene eutectic mixtures as hydrophobic solvents
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description Natural products can be the basis for the development of green solvents, relevant for the advancement of new, more sustainable processes and products. In this work, 10 binary mixtures constituted by terpenes are prepared and characterized. Their solid−liquid phase diagrams show that room-temperature solvents can be prepared from solid terpenes in a wide composition range. These diagrams are accurately described by the conductor-like screening model for real solvents, showing it to be a useful predictive tool for the design of novel natural solvents. At the eutectic point, these mixtures possess low viscosities, densities lower than water, and high boiling temperatures. The low water solubility in the eutectic solvents together with its negligible impact on the properties measured is a strong indicator of the hydrophobic character of these mixtures. The tunable character of these mixtures is demonstrated by studying the solvatochromic parameters in the entire concentration region, the properties of the final solvents being tuned by simply varying the mole fraction of the terpenes. The high potential of this tunable character is shown in the selective extraction of dyes from their aqueous solutions. This work is expected to devise new insights concerning these solvents as well as to boost their application in green industrial processes.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://bibliotecadigital.ipb.pt/bitstreams/3dfc9ea5-250f-4276-89bd-0357bdc6089b/download
id ipb_5470d0e1dd94d042caa176b41ec7bf0e
identifier.url.fl_str_mv http://hdl.handle.net/10198/20237
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instname_str Instituto Politécnico de Bragança
language eng
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network_name_str Biblioteca Digital do IPB
oai_identifier_str oai:bibliotecadigital.ipb.pt:10198/20237
organization_str_mv urn:organizationAcronym:ipb
person_str_mv Martins, Mónia A.R.
Silva, Liliana P.
Schaeffer, Nicolas
Abranches, Dinis O.
Maximo, Guilherme J.
Pinho, Simão
Pinho, Simão
https://www.ciencia-id.pt/481D-73AD-8D0F
481D-73AD-8D0F
http://orcid.org/0000-0002-9211-857X
0000-0002-9211-857X
Coutinho, João A.P.
publishDate 2019
reponame_str Biblioteca Digital do IPB
repository_id_str urn:repositoryAcronym:ipb
service_str_mv urn:repositoryAcronym:ipb
spelling engNatural products can be the basis for the development of green solvents, relevant for the advancement of new, more sustainable processes and products. In this work, 10 binary mixtures constituted by terpenes are prepared and characterized. Their solid−liquid phase diagrams show that room-temperature solvents can be prepared from solid terpenes in a wide composition range. These diagrams are accurately described by the conductor-like screening model for real solvents, showing it to be a useful predictive tool for the design of novel natural solvents. At the eutectic point, these mixtures possess low viscosities, densities lower than water, and high boiling temperatures. The low water solubility in the eutectic solvents together with its negligible impact on the properties measured is a strong indicator of the hydrophobic character of these mixtures. The tunable character of these mixtures is demonstrated by studying the solvatochromic parameters in the entire concentration region, the properties of the final solvents being tuned by simply varying the mole fraction of the terpenes. The high potential of this tunable character is shown in the selective extraction of dyes from their aqueous solutions. This work is expected to devise new insights concerning these solvents as well as to boost their application in green industrial processes.application/pdfen_ENGreener terpene-terpene eutectic mixtures as hydrophobic solventsMartins, Mónia A.R.Silva, Liliana P.Schaeffer, NicolasAbranches, Dinis O.Maximo, Guilherme J.PersonalPinho, SimãoDSpacehttp://dspace.org/items/8ef7789a-34f3-4915-a666-4efe26272a30DSpacehttp://dspace.org/items/8ef7789a-34f3-4915-a666-4efe26272a30PinhoSimãoCiência IDhttps://www.ciencia-id.pt481D-73AD-8D0FORCIDhttp://orcid.org0000-0002-9211-857XResearcher IDhttps://www.researcherid.comD-4148-2013Scopus Author IDhttps://www.scopus.com7003570175Coutinho, João A.P.HostingInstitutionOrganizationalBiblioteca Digital do IPBe-mailmailto:dspace@ipb.ptdspace@ipb.ptDOIIsPartOf10.1021/acssuschemeng.9b046142018-01-19T10:00:00Z20192019-01-01T00:00:00ZHandlehttp://hdl.handle.net/10198/20237http://purl.org/coar/access_right/c_abf2open accessCOSMO-RSEutectic mixturesPhysicochemical propertiesSLETerpenesTunable3985502 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://bibliotecadigital.ipb.pt/bitstreams/3dfc9ea5-250f-4276-89bd-0357bdc6089b/download
spellingShingle Greener terpene-terpene eutectic mixtures as hydrophobic solvents
Martins, Mónia A.R.
COSMO-RS
Eutectic mixtures
Physicochemical properties
SLE
Terpenes
Tunable
subject.fl_str_mv COSMO-RS
Eutectic mixtures
Physicochemical properties
SLE
Terpenes
Tunable
title Greener terpene-terpene eutectic mixtures as hydrophobic solvents
title_full Greener terpene-terpene eutectic mixtures as hydrophobic solvents
title_fullStr Greener terpene-terpene eutectic mixtures as hydrophobic solvents
title_full_unstemmed Greener terpene-terpene eutectic mixtures as hydrophobic solvents
title_short Greener terpene-terpene eutectic mixtures as hydrophobic solvents
title_sort Greener terpene-terpene eutectic mixtures as hydrophobic solvents
topic COSMO-RS
Eutectic mixtures
Physicochemical properties
SLE
Terpenes
Tunable
topic_facet COSMO-RS
Eutectic mixtures
Physicochemical properties
SLE
Terpenes
Tunable
url http://hdl.handle.net/10198/20237
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