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Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives

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Resumo:Consumer demand for natural and healthier products has led to an increasing interest in the bioactive and therapeutic properties of plant extracts. In this study, we evaluated the phenolic compounds profile, bioactivities, and toxicities of plant extracts from eight European flora species, including Calendula officinalis L., Calluna vulgaris (L.) Hull, Hippophae rhamnoides L., Juglans regia L., Mentha cervina L., Rubus idaeus L., Sambucus nigra L., and Vitis vinifera L. The aim was to identify potential preservatives of natural origin. Phenolic compounds were identified by HPLC-DAD-ESI-MS. Caffeic acid derivatives, ellagitannins, flavonols, and flavones were the major phenolic compounds identified. The total phenolic content varied from 16.0 & PLUSMN; 0.2 (V. vinifera) to 123 & PLUSMN; 2 mg/g (H. rhamnoides) of dry extract. All extracts showed antioxidant potential and exhibited activity against some of the microorganisms tested. S. nigra showed the highest activity in the inhibition of oxidative hemolysis (OxHLIA) assay and H. rhamnoides, notably, had the lowest IC50 values in TBARS and DPPH assays, as well as the lowest minimum inhibitory concentration (MIC) values. Regarding in vitro cytotoxicity, in tumor and non-tumor cell lines, although some extracts revealed toxicity against normal cells, it was found that the samples C. vulgaris, V. vinifera and R. idaeus might be used against tumor cells since the active concentration is much lower than the one causing toxicity. In vivo acute toxicity tests using Artemia franciscana suggest low toxicity for most extracts, with LC50 > 400 mg/L. These results showed the potential of the studied extracts as natural preservatives, given their richness in compounds with bioactive properties, highlight their potential value to the production chain.
Autores principais:Deus, Breno Martins de
Outros Autores:Fernandes, Conceição; Molina, Adriana K.; Xavier, Virginie; Pires, Tânia C.S.P.; Mandim, Filipa; Heleno, Sandrina A.; Finimundy, Tiane C.; Barros, Lillian
Assunto:Phenolic compounds Plant extracts Natural preservatives Bioactivity Toxicity Artemia franciscana European flora
Ano:2023
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Instituto Politécnico de Bragança
Idioma:inglês
Origem:Biblioteca Digital do IPB
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author Deus, Breno Martins de
author2 Fernandes, Conceição
Molina, Adriana K.
Xavier, Virginie
Pires, Tânia C.S.P.
Mandim, Filipa
Heleno, Sandrina A.
Finimundy, Tiane C.
Barros, Lillian
author2_role author
author
author
author
author
author
author
author
author_facet Deus, Breno Martins de
Fernandes, Conceição
Molina, Adriana K.
Xavier, Virginie
Pires, Tânia C.S.P.
Mandim, Filipa
Heleno, Sandrina A.
Finimundy, Tiane C.
Barros, Lillian
author_role author
contributor_name_str_mv Biblioteca Digital do IPB
country_str PT
creators_json_txt [{\"Person.name\":\"Deus, Breno Martins de\"},{\"Person.name\":\"Fernandes, Conceição\",\"Person.identifier.orcid\":\"0000-0003-2873-501X\"},{\"Person.name\":\"Molina, Adriana K.\",\"Person.identifier.orcid\":\"0000-0002-6234-2212\"},{\"Person.name\":\"Xavier, Virginie\",\"Person.identifier.orcid\":\"0000-0001-7508-1245\"},{\"Person.name\":\"Pires, Tânia C.S.P.\",\"Person.identifier.orcid\":\"0000-0002-3954-3833\"},{\"Person.name\":\"Mandim, Filipa\",\"Person.identifier.orcid\":\"0000-0002-6494-2326\"},{\"Person.name\":\"Heleno, Sandrina A.\",\"Person.identifier.orcid\":\"0000-0001-7224-1098\"},{\"Person.name\":\"Finimundy, Tiane C.\",\"Person.identifier.orcid\":\"0000-0003-3516-0795\"},{\"Person.name\":\"Barros, Lillian\",\"Person.identifier.orcid\":\"0000-0002-9050-5189\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Biblioteca Digital do IPB
datacite.creators.creator.creatorName.fl_str_mv Deus, Breno Martins de
Fernandes, Conceição
Molina, Adriana K.
Xavier, Virginie
Pires, Tânia C.S.P.
Mandim, Filipa
Heleno, Sandrina A.
Finimundy, Tiane C.
Barros, Lillian
datacite.date.Accepted.fl_str_mv 2023-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2023-05-10T09:16:39Z
datacite.date.embargoed.fl_str_mv 2023-05-10T09:16:39Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Phenolic compounds
Plant extracts
Natural preservatives
Bioactivity
Toxicity
Artemia franciscana
European flora
datacite.titles.title.fl_str_mv Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
dc.contributor.none.fl_str_mv Biblioteca Digital do IPB
dc.creator.none.fl_str_mv Deus, Breno Martins de
Fernandes, Conceição
Molina, Adriana K.
Xavier, Virginie
Pires, Tânia C.S.P.
Mandim, Filipa
Heleno, Sandrina A.
Finimundy, Tiane C.
Barros, Lillian
dc.date.Accepted.fl_str_mv 2023-01-01T00:00:00Z
dc.date.available.fl_str_mv 2023-05-10T09:16:39Z
dc.date.embargoed.fl_str_mv 2023-05-10T09:16:39Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10198/28263
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv MDPI
dc.rights.cclincense.fl_str_mv http://creativecommons.org/licenses/by/4.0/
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Phenolic compounds
Plant extracts
Natural preservatives
Bioactivity
Toxicity
Artemia franciscana
European flora
dc.title.fl_str_mv Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description Consumer demand for natural and healthier products has led to an increasing interest in the bioactive and therapeutic properties of plant extracts. In this study, we evaluated the phenolic compounds profile, bioactivities, and toxicities of plant extracts from eight European flora species, including Calendula officinalis L., Calluna vulgaris (L.) Hull, Hippophae rhamnoides L., Juglans regia L., Mentha cervina L., Rubus idaeus L., Sambucus nigra L., and Vitis vinifera L. The aim was to identify potential preservatives of natural origin. Phenolic compounds were identified by HPLC-DAD-ESI-MS. Caffeic acid derivatives, ellagitannins, flavonols, and flavones were the major phenolic compounds identified. The total phenolic content varied from 16.0 & PLUSMN; 0.2 (V. vinifera) to 123 & PLUSMN; 2 mg/g (H. rhamnoides) of dry extract. All extracts showed antioxidant potential and exhibited activity against some of the microorganisms tested. S. nigra showed the highest activity in the inhibition of oxidative hemolysis (OxHLIA) assay and H. rhamnoides, notably, had the lowest IC50 values in TBARS and DPPH assays, as well as the lowest minimum inhibitory concentration (MIC) values. Regarding in vitro cytotoxicity, in tumor and non-tumor cell lines, although some extracts revealed toxicity against normal cells, it was found that the samples C. vulgaris, V. vinifera and R. idaeus might be used against tumor cells since the active concentration is much lower than the one causing toxicity. In vivo acute toxicity tests using Artemia franciscana suggest low toxicity for most extracts, with LC50 > 400 mg/L. These results showed the potential of the studied extracts as natural preservatives, given their richness in compounds with bioactive properties, highlight their potential value to the production chain.
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eu_rights_str_mv openAccess
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oai_identifier_str oai:bibliotecadigital.ipb.pt:10198/28263
organization_str_mv urn:organizationAcronym:ipb
person_str_mv Deus, Breno Martins de
Fernandes, Conceição
Fernandes, Conceição
https://www.ciencia-id.pt/6514-3D41-4534
6514-3D41-4534
http://orcid.org/0000-0003-2873-501X
0000-0003-2873-501X
Molina, Adriana K.
Molina, Adriana K.
https://www.ciencia-id.pt/C110-0167-E58D
C110-0167-E58D
http://orcid.org/0000-0002-6234-2212
0000-0002-6234-2212
Xavier, Virginie
Xavier, Virginie
https://www.ciencia-id.pt/B212-37BC-7FB4
B212-37BC-7FB4
http://orcid.org/0000-0001-7508-1245
0000-0001-7508-1245
Pires, Tânia C.S.P.
Pires, Tânia C.S.P.
https://www.ciencia-id.pt/321E-2D96-00CA
321E-2D96-00CA
http://orcid.org/0000-0002-3954-3833
0000-0002-3954-3833
Mandim, Filipa
Mandim, Filipa
https://www.ciencia-id.pt/F318-9049-EB99
F318-9049-EB99
http://orcid.org/0000-0002-6494-2326
0000-0002-6494-2326
Heleno, Sandrina A.
Heleno, Sandrina A.
https://www.ciencia-id.pt/8B18-3095-6FC9
8B18-3095-6FC9
http://orcid.org/0000-0001-7224-1098
0000-0001-7224-1098
Finimundy, Tiane C.
Finimundy, Tiane C.
https://www.ciencia-id.pt/2F18-67B1-776A
2F18-67B1-776A
http://orcid.org/0000-0003-3516-0795
0000-0003-3516-0795
Barros, Lillian
Barros, Lillian
https://www.ciencia-id.pt/9616-35CB-D001
9616-35CB-D001
http://orcid.org/0000-0002-9050-5189
0000-0002-9050-5189
publishDate 2023
publisher.none.fl_str_mv MDPI
reponame_str Biblioteca Digital do IPB
repository_id_str urn:repositoryAcronym:ipb
service_str_mv urn:repositoryAcronym:ipb
spelling engMDPIpt_PTConsumer demand for natural and healthier products has led to an increasing interest in the bioactive and therapeutic properties of plant extracts. In this study, we evaluated the phenolic compounds profile, bioactivities, and toxicities of plant extracts from eight European flora species, including Calendula officinalis L., Calluna vulgaris (L.) Hull, Hippophae rhamnoides L., Juglans regia L., Mentha cervina L., Rubus idaeus L., Sambucus nigra L., and Vitis vinifera L. The aim was to identify potential preservatives of natural origin. Phenolic compounds were identified by HPLC-DAD-ESI-MS. Caffeic acid derivatives, ellagitannins, flavonols, and flavones were the major phenolic compounds identified. The total phenolic content varied from 16.0 & PLUSMN; 0.2 (V. vinifera) to 123 & PLUSMN; 2 mg/g (H. rhamnoides) of dry extract. All extracts showed antioxidant potential and exhibited activity against some of the microorganisms tested. S. nigra showed the highest activity in the inhibition of oxidative hemolysis (OxHLIA) assay and H. rhamnoides, notably, had the lowest IC50 values in TBARS and DPPH assays, as well as the lowest minimum inhibitory concentration (MIC) values. Regarding in vitro cytotoxicity, in tumor and non-tumor cell lines, although some extracts revealed toxicity against normal cells, it was found that the samples C. vulgaris, V. vinifera and R. idaeus might be used against tumor cells since the active concentration is much lower than the one causing toxicity. In vivo acute toxicity tests using Artemia franciscana suggest low toxicity for most extracts, with LC50 > 400 mg/L. These results showed the potential of the studied extracts as natural preservatives, given their richness in compounds with bioactive properties, highlight their potential value to the production chain.application/pdfpt_PTChemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservativesDeus, Breno Martins dePersonalFernandes, ConceiçãoDSpacehttp://dspace.org/items/d9c26c54-5e10-4ccb-b7f7-528af9eb9950DSpacehttp://dspace.org/items/d9c26c54-5e10-4ccb-b7f7-528af9eb9950FernandesConceiçãoCiência IDhttps://www.ciencia-id.pt6514-3D41-4534ORCIDhttp://orcid.org0000-0003-2873-501XScopus Author IDhttps://www.scopus.com23018336600PersonalMolina, Adriana K.DSpacehttp://dspace.org/items/dc9b5b67-c45e-4fbe-8af1-8cec9adb5cd9DSpacehttp://dspace.org/items/dc9b5b67-c45e-4fbe-8af1-8cec9adb5cd9MolinaAdriana K.Ciência IDhttps://www.ciencia-id.ptC110-0167-E58DORCIDhttp://orcid.org0000-0002-6234-2212PersonalXavier, VirginieDSpacehttp://dspace.org/items/e11787fd-f254-4635-a4c3-c56e829f614eDSpacehttp://dspace.org/items/e11787fd-f254-4635-a4c3-c56e829f614eXavierVirginieCiência IDhttps://www.ciencia-id.ptB212-37BC-7FB4ORCIDhttp://orcid.org0000-0001-7508-1245PersonalPires, Tânia C.S.P.DSpacehttp://dspace.org/items/34af4d18-b8ae-4329-9450-69dc35ed448fDSpacehttp://dspace.org/items/34af4d18-b8ae-4329-9450-69dc35ed448fPiresTânia C.S.P.Ciência IDhttps://www.ciencia-id.pt321E-2D96-00CAORCIDhttp://orcid.org0000-0002-3954-3833Researcher IDhttps://www.researcherid.comQ-2842-2018Scopus Author IDhttps://www.scopus.com57057440000PersonalMandim, FilipaDSpacehttp://dspace.org/items/bcc274d4-7e6c-46a8-8e49-2752f9dbfbcdDSpacehttp://dspace.org/items/bcc274d4-7e6c-46a8-8e49-2752f9dbfbcdMandimFilipaCiência IDhttps://www.ciencia-id.ptF318-9049-EB99ORCIDhttp://orcid.org0000-0002-6494-2326PersonalHeleno, Sandrina A.DSpacehttp://dspace.org/items/e89b5bf5-d315-49b6-871e-fa8eb6030676DSpacehttp://dspace.org/items/e89b5bf5-d315-49b6-871e-fa8eb6030676HelenoSandrina A.Ciência IDhttps://www.ciencia-id.pt8B18-3095-6FC9ORCIDhttp://orcid.org0000-0001-7224-1098Researcher IDhttps://www.researcherid.comL-5951-2014Scopus Author IDhttps://www.scopus.com30067731800PersonalFinimundy, Tiane C.DSpacehttp://dspace.org/items/4f8767d4-4e62-4550-9b35-740cb2f672daDSpacehttp://dspace.org/items/4f8767d4-4e62-4550-9b35-740cb2f672daFinimundyTiane C.Ciência IDhttps://www.ciencia-id.pt2F18-67B1-776AORCIDhttp://orcid.org0000-0003-3516-0795PersonalBarros, LillianDSpacehttp://dspace.org/items/3af07ffe-f914-48ba-a5d5-efcf70fdce01DSpacehttp://dspace.org/items/3af07ffe-f914-48ba-a5d5-efcf70fdce01BarrosLillianCiência IDhttps://www.ciencia-id.pt9616-35CB-D001ORCIDhttp://orcid.org0000-0002-9050-5189Researcher IDhttps://www.researcherid.comJ-3600-2013Researcher IDhttps://www.researcherid.comJ-3600-2013Scopus Author IDhttps://www.scopus.com35236343600Scopus Author IDhttps://www.scopus.com57194900801HostingInstitutionOrganizationalBiblioteca Digital do IPBe-mailmailto:dspace@ipb.ptdspace@ipb.ptDOIIsPartOf10.3390/plants121527842023-05-10T09:16:39Z20232023-01-01T00:00:00ZHandlehttp://hdl.handle.net/10198/28263http://purl.org/coar/access_right/c_abf2open accessPhenolic compoundsPlant extractsNatural preservativesBioactivityToxicityArtemia franciscanaEuropean flora560625 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal article2023http://creativecommons.org/licenses/by/4.0/http://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://bibliotecadigital.ipb.pt/bitstreams/20394d1d-36ea-4e73-b3fe-14ec6691f431/downloadPlants
spellingShingle Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
Deus, Breno Martins de
Phenolic compounds
Plant extracts
Natural preservatives
Bioactivity
Toxicity
Artemia franciscana
European flora
status SINGLETON
subject.fl_str_mv Phenolic compounds
Plant extracts
Natural preservatives
Bioactivity
Toxicity
Artemia franciscana
European flora
title Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
title_full Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
title_fullStr Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
title_full_unstemmed Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
title_short Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
title_sort Chemical characterization, bioactivity and toxicity of european flora plant extracts in search for potential natural origin preservatives
topic Phenolic compounds
Plant extracts
Natural preservatives
Bioactivity
Toxicity
Artemia franciscana
European flora
topic_facet Phenolic compounds
Plant extracts
Natural preservatives
Bioactivity
Toxicity
Artemia franciscana
European flora
url http://hdl.handle.net/10198/28263
visible 1