Publicação
Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor
| Resumo: | The synthesis of 1,1-Dibutoxyethane was carried out in a Simulated Moving Bed pilot unit LICOSEP 12-26 (Novasep, France) with 12 columns packed with the commercial ionexchange resin Amberlyst 15 (Rohm & Haas, France). Experimentally it was obtained a raffinate purity of 85% with a productivity of 5,04 Kg.L-1.d-1 and a desorbent consumption of 15, 5 L.Kg-1. The influence of the different operation parameters was studied by simulation. The results showed that the SMBR process presents a potential to be a competitive, efficient and environmentally friendly way to produce 1,1- Dibutoxyethane and other acetals. |
|---|---|
| Autores principais: | Graça, Nuno S. |
| Outros Autores: | Pais, Luís S.; Silva, Viviana M.T.M.; Rodrigues, Alírio |
| Assunto: | Multifunctional reactors Simulated moving bed Acetals Amberlyst 15 |
| Ano: | 2012 |
| País: | Portugal |
| Tipo de documento: | documento de conferência |
| Tipo de acesso: | acesso aberto |
| Instituição associada: | Instituto Politécnico de Bragança |
| Idioma: | inglês |
| Origem: | Biblioteca Digital do IPB |
| _version_ | 1867173244628369408 |
|---|---|
| author | Graça, Nuno S. |
| author2 | Pais, Luís S. Silva, Viviana M.T.M. Rodrigues, Alírio |
| author2_role | author author author |
| author_facet | Graça, Nuno S. Pais, Luís S. Silva, Viviana M.T.M. Rodrigues, Alírio |
| author_role | author |
| contributor_name_str_mv | Biblioteca Digital do IPB |
| country_str | PT |
| creators_json_txt | [{\"Person.name\":\"Graça, Nuno S.\"},{\"Person.name\":\"Pais, Luís S.\",\"Person.identifier.orcid\":\"0000-0002-3000-2862\"},{\"Person.name\":\"Silva, Viviana M.T.M.\"},{\"Person.name\":\"Rodrigues, Alírio\"}] |
| datacite.contributors.contributor.contributorName.fl_str_mv | Biblioteca Digital do IPB |
| datacite.creators.creator.creatorName.fl_str_mv | Graça, Nuno S. Pais, Luís S. Silva, Viviana M.T.M. Rodrigues, Alírio |
| datacite.date.Accepted.fl_str_mv | 2012-01-01T00:00:00Z |
| datacite.date.available.fl_str_mv | 2014-01-14T09:38:39Z |
| datacite.date.embargoed.fl_str_mv | 2014-01-14T09:38:39Z |
| datacite.rights.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| datacite.subjects.subject.fl_str_mv | Multifunctional reactors Simulated moving bed Acetals Amberlyst 15 |
| datacite.titles.title.fl_str_mv | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| dc.contributor.none.fl_str_mv | Biblioteca Digital do IPB |
| dc.creator.none.fl_str_mv | Graça, Nuno S. Pais, Luís S. Silva, Viviana M.T.M. Rodrigues, Alírio |
| dc.date.Accepted.fl_str_mv | 2012-01-01T00:00:00Z |
| dc.date.available.fl_str_mv | 2014-01-14T09:38:39Z |
| dc.date.embargoed.fl_str_mv | 2014-01-14T09:38:39Z |
| dc.format.none.fl_str_mv | application/pdf |
| dc.identifier.none.fl_str_mv | http://hdl.handle.net/10198/9146 |
| dc.language.none.fl_str_mv | eng |
| dc.rights.none.fl_str_mv | http://purl.org/coar/access_right/c_abf2 |
| dc.subject.none.fl_str_mv | Multifunctional reactors Simulated moving bed Acetals Amberlyst 15 |
| dc.title.fl_str_mv | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| dc.type.none.fl_str_mv | http://purl.org/coar/resource_type/c_c94f |
| description | The synthesis of 1,1-Dibutoxyethane was carried out in a Simulated Moving Bed pilot unit LICOSEP 12-26 (Novasep, France) with 12 columns packed with the commercial ionexchange resin Amberlyst 15 (Rohm & Haas, France). Experimentally it was obtained a raffinate purity of 85% with a productivity of 5,04 Kg.L-1.d-1 and a desorbent consumption of 15, 5 L.Kg-1. The influence of the different operation parameters was studied by simulation. The results showed that the SMBR process presents a potential to be a competitive, efficient and environmentally friendly way to produce 1,1- Dibutoxyethane and other acetals. |
| dirty | 0 |
| eu_rights_str_mv | openAccess |
| format | conferenceObject |
| fulltext.url.fl_str_mv | https://bibliotecadigital.ipb.pt/bitstreams/70742822-f158-4c86-89ab-350fabd58024/download |
| id | ipb_e3d29d3bfddfc1445aa09c49bda85f74 |
| identifier.url.fl_str_mv | http://hdl.handle.net/10198/9146 |
| instacron_str | ipb |
| institution | Instituto Politécnico de Bragança |
| instname_str | Instituto Politécnico de Bragança |
| language | eng |
| network_acronym_str | ipb |
| network_name_str | Biblioteca Digital do IPB |
| oai_identifier_str | oai:bibliotecadigital.ipb.pt:10198/9146 |
| organization_str_mv | urn:organizationAcronym:ipb |
| person_str_mv | Graça, Nuno S. Pais, Luís S. Pais, Luís S. https://www.ciencia-id.pt/421E-0CCD-A84F 421E-0CCD-A84F http://orcid.org/0000-0002-3000-2862 0000-0002-3000-2862 Silva, Viviana M.T.M. Rodrigues, Alírio |
| publishDate | 2012 |
| reponame_str | Biblioteca Digital do IPB |
| repository_id_str | urn:repositoryAcronym:ipb |
| service_str_mv | urn:repositoryAcronym:ipb |
| spelling | engporThe synthesis of 1,1-Dibutoxyethane was carried out in a Simulated Moving Bed pilot unit LICOSEP 12-26 (Novasep, France) with 12 columns packed with the commercial ionexchange resin Amberlyst 15 (Rohm & Haas, France). Experimentally it was obtained a raffinate purity of 85% with a productivity of 5,04 Kg.L-1.d-1 and a desorbent consumption of 15, 5 L.Kg-1. The influence of the different operation parameters was studied by simulation. The results showed that the SMBR process presents a potential to be a competitive, efficient and environmentally friendly way to produce 1,1- Dibutoxyethane and other acetals.application/pdfporSynthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactorGraça, Nuno S.PersonalPais, Luís S.DSpacehttp://dspace.org/items/c6d25534-8487-45b1-90af-d350f4e3ac55DSpacehttp://dspace.org/items/c6d25534-8487-45b1-90af-d350f4e3ac55PaisLuís S.Ciência IDhttps://www.ciencia-id.pt421E-0CCD-A84FORCIDhttp://orcid.org0000-0002-3000-2862Scopus Author IDhttps://www.scopus.com6603930478Silva, Viviana M.T.M.Rodrigues, AlírioHostingInstitutionOrganizationalBiblioteca Digital do IPBe-mailmailto:dspace@ipb.ptdspace@ipb.pt2014-01-14T09:38:39Z20122012-01-01T00:00:00ZHandlehttp://hdl.handle.net/10198/9146http://purl.org/coar/access_right/c_abf2open accessMultifunctional reactorsSimulated moving bedAcetalsAmberlyst 15151553 bytesother research producthttp://purl.org/coar/resource_type/c_c94fconference objecthttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://bibliotecadigital.ipb.pt/bitstreams/70742822-f158-4c86-89ab-350fabd58024/download22nd International Symposium on Chemical Reaction Engineering (ISCRE)Maastricht, The Netherlands |
| spellingShingle | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor Graça, Nuno S. Multifunctional reactors Simulated moving bed Acetals Amberlyst 15 |
| status | SINGLETON |
| subject.fl_str_mv | Multifunctional reactors Simulated moving bed Acetals Amberlyst 15 |
| title | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| title_full | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| title_fullStr | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| title_full_unstemmed | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| title_short | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| title_sort | Synthesis of 1,1-dibutoxyethane in a simulated moving bed adsorptive reactor |
| topic | Multifunctional reactors Simulated moving bed Acetals Amberlyst 15 |
| topic_facet | Multifunctional reactors Simulated moving bed Acetals Amberlyst 15 |
| url | http://hdl.handle.net/10198/9146 |
| visible | 1 |