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Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds

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Resumo:Ceratonia siliqua L., commonly known as the carob tree is native to the Mediterranean countries and is widely known and consumed. Due to its chemical constituents, flavoring properties, and nutritional benefits, it has the potential to be of significant importance to the food industry1. The carob bean is made up of 90% pulp and 10% seeds. Those seeds are widely used in the food industry as a thickening agent (E-410). However, knowledge about phenolic composition and its relation to biological properties is scarce. This study used seeds of thirteen carob varieties harvested in Algarve, Portugal. The phenolic composition of the hydroethanolic extracts was analyzed by HPLC-DAD-ESI/MS. The antioxidant, anti-inflammatory, cytotoxic and antibacterial properties of the extracts were also analysed. The phenolic composition was analyzed by HPLC-DAD-ESI/MS. Cytotoxic activity was evaluated by the colourimetric method of sulforhodamine B. Anti-inflammatory activity was determined by inhibition of NO production in murine macrophages. The antibacterial activity was evaluated through the method of successive microdilutions and the antioxidant activity through the TBARS and CAA assays. Seventeen phenolics compounds were tentatively identified, being (Epi)catechin dimer type  dimer and apigenin-O-hexosyl-pentoside the most abundant ones (3.08 – 11.67 mg/mL). All the varieties studied exhibited the capacity to inhibit TBARS formation. The extract obtained from the Gasparinha variety was the only one that inhibited the reactive oxygen species formation in the CAA assay. For the cytotoxic activity only Cavi, Cardeira and Pé Comprido varieties demonstrated the ability to inhibit the proliferation of the tumor cell lines tested, without showing a hepatotoxic effect. All extracts presented a broad-spectrum microbial growth inhibition without an efficient bactericidal power. These findings highlight Carob seed as a rich source of structurally diverse biomolecules with potential application as additives in food formulation development. However, further studies are needed to understand the correlation between phenolic compounds and the bioactive properties associated with carob seed tissues.
Autores principais:Marcelino, Sandra Andreia
Outros Autores:Mandim, Filipa; Oludemi, Taofiq; Dias, Maria Inês; Barracosa, Paulo; Prieto Lage, Miguel A.; Barros, Lillian
Assunto:Ceratonia siliqua L. seeds Research Subject Categories::TECHNOLOGY::Chemical engineering::Food technology
Ano:2022
País:Portugal
Tipo de documento:documento de conferência
Tipo de acesso:acesso aberto
Instituição associada:Instituto Politécnico de Bragança
Idioma:inglês
Origem:Biblioteca Digital do IPB
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author Marcelino, Sandra Andreia
author2 Mandim, Filipa
Oludemi, Taofiq
Dias, Maria Inês
Barracosa, Paulo
Prieto Lage, Miguel A.
Barros, Lillian
author2_role author
author
author
author
author
author
author_facet Marcelino, Sandra Andreia
Mandim, Filipa
Oludemi, Taofiq
Dias, Maria Inês
Barracosa, Paulo
Prieto Lage, Miguel A.
Barros, Lillian
author_role author
contributor_name_str_mv Biblioteca Digital do IPB
country_str PT
creators_json_txt [{\"Person.name\":\"Marcelino, Sandra Andreia\",\"Person.identifier.orcid\":\"0000-0003-1490-9445\"},{\"Person.name\":\"Mandim, Filipa\",\"Person.identifier.orcid\":\"0000-0002-6494-2326\"},{\"Person.name\":\"Oludemi, Taofiq\",\"Person.identifier.orcid\":\"0000-0003-2822-3532\"},{\"Person.name\":\"Dias, Maria Inês\",\"Person.identifier.orcid\":\"0000-0001-8744-7814\"},{\"Person.name\":\"Barracosa, Paulo\"},{\"Person.name\":\"Prieto Lage, Miguel A.\",\"Person.identifier.orcid\":\"0000-0002-3513-0054\"},{\"Person.name\":\"Barros, Lillian\",\"Person.identifier.orcid\":\"0000-0002-9050-5189\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Biblioteca Digital do IPB
datacite.creators.creator.creatorName.fl_str_mv Marcelino, Sandra Andreia
Mandim, Filipa
Oludemi, Taofiq
Dias, Maria Inês
Barracosa, Paulo
Prieto Lage, Miguel A.
Barros, Lillian
datacite.date.Accepted.fl_str_mv 2022-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2023-03-21T15:07:29Z
datacite.date.embargoed.fl_str_mv 2023-03-21T15:07:29Z
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datacite.subjects.subject.fl_str_mv Ceratonia siliqua L. seeds
Research Subject Categories::TECHNOLOGY::Chemical engineering::Food technology
datacite.titles.title.fl_str_mv Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
dc.contributor.none.fl_str_mv Biblioteca Digital do IPB
dc.creator.none.fl_str_mv Marcelino, Sandra Andreia
Mandim, Filipa
Oludemi, Taofiq
Dias, Maria Inês
Barracosa, Paulo
Prieto Lage, Miguel A.
Barros, Lillian
dc.date.Accepted.fl_str_mv 2022-01-01T00:00:00Z
dc.date.available.fl_str_mv 2023-03-21T15:07:29Z
dc.date.embargoed.fl_str_mv 2023-03-21T15:07:29Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10198/27909
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Sociedade Portuguesa de Química
dc.rights.cclincense.fl_str_mv http://creativecommons.org/licenses/by/4.0/
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Ceratonia siliqua L. seeds
Research Subject Categories::TECHNOLOGY::Chemical engineering::Food technology
dc.title.fl_str_mv Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_c94f
description Ceratonia siliqua L., commonly known as the carob tree is native to the Mediterranean countries and is widely known and consumed. Due to its chemical constituents, flavoring properties, and nutritional benefits, it has the potential to be of significant importance to the food industry1. The carob bean is made up of 90% pulp and 10% seeds. Those seeds are widely used in the food industry as a thickening agent (E-410). However, knowledge about phenolic composition and its relation to biological properties is scarce. This study used seeds of thirteen carob varieties harvested in Algarve, Portugal. The phenolic composition of the hydroethanolic extracts was analyzed by HPLC-DAD-ESI/MS. The antioxidant, anti-inflammatory, cytotoxic and antibacterial properties of the extracts were also analysed. The phenolic composition was analyzed by HPLC-DAD-ESI/MS. Cytotoxic activity was evaluated by the colourimetric method of sulforhodamine B. Anti-inflammatory activity was determined by inhibition of NO production in murine macrophages. The antibacterial activity was evaluated through the method of successive microdilutions and the antioxidant activity through the TBARS and CAA assays. Seventeen phenolics compounds were tentatively identified, being (Epi)catechin dimer type  dimer and apigenin-O-hexosyl-pentoside the most abundant ones (3.08 – 11.67 mg/mL). All the varieties studied exhibited the capacity to inhibit TBARS formation. The extract obtained from the Gasparinha variety was the only one that inhibited the reactive oxygen species formation in the CAA assay. For the cytotoxic activity only Cavi, Cardeira and Pé Comprido varieties demonstrated the ability to inhibit the proliferation of the tumor cell lines tested, without showing a hepatotoxic effect. All extracts presented a broad-spectrum microbial growth inhibition without an efficient bactericidal power. These findings highlight Carob seed as a rich source of structurally diverse biomolecules with potential application as additives in food formulation development. However, further studies are needed to understand the correlation between phenolic compounds and the bioactive properties associated with carob seed tissues.
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person_str_mv Marcelino, Sandra Andreia
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Mandim, Filipa
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Oludemi, Taofiq
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Dias, Maria Inês
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Barracosa, Paulo
Prieto Lage, Miguel A.
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Barros, Lillian
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spelling engSociedade Portuguesa de Químicapt_PTCeratonia siliqua L., commonly known as the carob tree is native to the Mediterranean countries and is widely known and consumed. Due to its chemical constituents, flavoring properties, and nutritional benefits, it has the potential to be of significant importance to the food industry1. The carob bean is made up of 90% pulp and 10% seeds. Those seeds are widely used in the food industry as a thickening agent (E-410). However, knowledge about phenolic composition and its relation to biological properties is scarce. This study used seeds of thirteen carob varieties harvested in Algarve, Portugal. The phenolic composition of the hydroethanolic extracts was analyzed by HPLC-DAD-ESI/MS. The antioxidant, anti-inflammatory, cytotoxic and antibacterial properties of the extracts were also analysed. The phenolic composition was analyzed by HPLC-DAD-ESI/MS. Cytotoxic activity was evaluated by the colourimetric method of sulforhodamine B. Anti-inflammatory activity was determined by inhibition of NO production in murine macrophages. The antibacterial activity was evaluated through the method of successive microdilutions and the antioxidant activity through the TBARS and CAA assays. Seventeen phenolics compounds were tentatively identified, being (Epi)catechin dimer type  dimer and apigenin-O-hexosyl-pentoside the most abundant ones (3.08 – 11.67 mg/mL). All the varieties studied exhibited the capacity to inhibit TBARS formation. The extract obtained from the Gasparinha variety was the only one that inhibited the reactive oxygen species formation in the CAA assay. For the cytotoxic activity only Cavi, Cardeira and Pé Comprido varieties demonstrated the ability to inhibit the proliferation of the tumor cell lines tested, without showing a hepatotoxic effect. All extracts presented a broad-spectrum microbial growth inhibition without an efficient bactericidal power. These findings highlight Carob seed as a rich source of structurally diverse biomolecules with potential application as additives in food formulation development. However, further studies are needed to understand the correlation between phenolic compounds and the bioactive properties associated with carob seed tissues.application/pdfpt_PTGenetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seedsPersonalMarcelino, Sandra AndreiaDSpacehttp://dspace.org/items/d116a005-efaf-410f-8dae-8ded6c79b9d9DSpacehttp://dspace.org/items/d116a005-efaf-410f-8dae-8ded6c79b9d9MarcelinoSandra AndreiaORCIDhttp://orcid.org0000-0003-1490-9445PersonalMandim, FilipaDSpacehttp://dspace.org/items/bcc274d4-7e6c-46a8-8e49-2752f9dbfbcdDSpacehttp://dspace.org/items/bcc274d4-7e6c-46a8-8e49-2752f9dbfbcdMandimFilipaCiência IDhttps://www.ciencia-id.ptF318-9049-EB99ORCIDhttp://orcid.org0000-0002-6494-2326PersonalOludemi, TaofiqDSpacehttp://dspace.org/items/74ac0f55-9896-40ec-8444-523044e80c4aDSpacehttp://dspace.org/items/74ac0f55-9896-40ec-8444-523044e80c4aOludemiTaofiqCiência IDhttps://www.ciencia-id.ptE318-A5CD-6626ORCIDhttp://orcid.org0000-0003-2822-3532PersonalDias, Maria InêsDSpacehttp://dspace.org/items/7ca8432b-e7f4-4116-a56e-9eba0d4403bdDSpacehttp://dspace.org/items/7ca8432b-e7f4-4116-a56e-9eba0d4403bdDiasMaria InêsCiência IDhttps://www.ciencia-id.pt2A13-4BE6-C7CFORCIDhttp://orcid.org0000-0001-8744-7814Researcher IDhttps://www.researcherid.comM-8242-2013Scopus Author IDhttps://www.scopus.com54388787000Barracosa, PauloPersonalPrieto Lage, Miguel A.DSpacehttp://dspace.org/items/13260615-fd28-4b8b-9dd4-8a8466007579DSpacehttp://dspace.org/items/13260615-fd28-4b8b-9dd4-8a8466007579PrietoMiguel A.Ciência IDhttps://www.ciencia-id.pt221E-1E00-AB74ORCIDhttp://orcid.org0000-0002-3513-0054Researcher IDhttps://www.researcherid.comG-4516-2011Scopus Author IDhttps://www.scopus.com35937495700Scopus Author IDhttps://www.scopus.com57207755963PersonalBarros, LillianDSpacehttp://dspace.org/items/3af07ffe-f914-48ba-a5d5-efcf70fdce01DSpacehttp://dspace.org/items/3af07ffe-f914-48ba-a5d5-efcf70fdce01BarrosLillianCiência IDhttps://www.ciencia-id.pt9616-35CB-D001ORCIDhttp://orcid.org0000-0002-9050-5189Researcher IDhttps://www.researcherid.comJ-3600-2013Researcher IDhttps://www.researcherid.comJ-3600-2013Scopus Author IDhttps://www.scopus.com35236343600Scopus Author IDhttps://www.scopus.com57194900801HostingInstitutionOrganizationalBiblioteca Digital do IPBe-mailmailto:dspace@ipb.ptdspace@ipb.pt2023-03-21T15:07:29Z20222022-01-01T00:00:00ZHandlehttp://hdl.handle.net/10198/27909http://purl.org/coar/access_right/c_abf2open accessCeratonia siliqua L. seedsResearch Subject Categories::TECHNOLOGY::Chemical engineering::Food technology686117 bytesFundação para a Ciência e a TecnologiaMountain Research Center6817 - DCRRNI IDCrossref Funder IDhttp://doi.org/10.13039/501100001871Fundação para a Ciência e a TecnologiaMountain Research Center6817 - DCRRNI IDCrossref Funder IDhttp://doi.org/10.13039/501100001871Fundação para a Ciência e a TecnologiaIntegrated strategies for the development of a novel functional beverage with sustainable production systemsCrossref Funder IDhttp://doi.org/10.13039/501100001871other research producthttp://purl.org/coar/resource_type/c_c94fconference object2022http://creativecommons.org/licenses/by/4.0/http://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://bibliotecadigital.ipb.pt/bitstreams/80ee2351-8fe1-4143-82b3-5f59d0a12f45/downloadLivro de Resumos do 12º Encontro Nacional de Cromatografia & XIV WARPA176176Aveiro
spellingShingle Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
Marcelino, Sandra Andreia
Ceratonia siliqua L. seeds
Research Subject Categories::TECHNOLOGY::Chemical engineering::Food technology
status SINGLETON
subject.fl_str_mv Ceratonia siliqua L. seeds
Research Subject Categories::TECHNOLOGY::Chemical engineering::Food technology
title Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
title_full Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
title_fullStr Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
title_full_unstemmed Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
title_short Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
title_sort Genetic information influence on phenolic composition and bioactivities of Ceratonia siliqua L. seeds
topic Ceratonia siliqua L. seeds
Research Subject Categories::TECHNOLOGY::Chemical engineering::Food technology
topic_facet Ceratonia siliqua L. seeds
Research Subject Categories::TECHNOLOGY::Chemical engineering::Food technology
url http://hdl.handle.net/10198/27909
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