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Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus

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Resumo:Identifying bioactive molecules from marine organisms is still vastly understudied. Fish remain an untapped source of bioactive molecules, even when considering species whose toxicity to other fish species has been noticed before. We assessed potential applications of crude body mucus of the Lusitanian toadfish (Halobratachus didactylus) and characterized its peptide fraction composition. Mucus samples from three individuals (two wild and one captive) revealed potential antioxidant, antihypertensive, and antimicrobial activities. For antioxidant activity, the best results of 2371 ± 97 µmol Trolox Equivalent/g protein for ORAC and 154 ± 6 µmol Trolox Equivalent/g protein for ABTS were obtained. For antihypertensive activity, the relevant inhibitory activity of ACE resulted in IC50 of 60 ± 7 µg protein/mL. Antimicrobial activity was also identified against the pathogenic bacteria Escherichia coli and Listeria monocytogenes. The peptide profile of the crude body mucus was obtained through size exclusion chromatography, with a conspicuous peak at ca. 800 Da. LC-MS/MS allowed the detection of the most probable peptide sequences of this dominant peptide. This is the first study where the bioactive potential of mucus from the Lusitanian toadfish is demonstrated. Peptides with such properties can be applied in the food and pharmaceutical industries.
Autores principais:Cunha, Marta Fernandez
Outros Autores:Coscueta, Ezequiel; Emilia Brassesco, M.; Marques, Rita; Neto, José; Almada, Frederico José Oliveira de; Goncalves, David; Pintado, Maria Manuela
Assunto:Ichthyocrinotoxins Antimicrobial Antioxidant Antihypertensive Peptides
Ano:2023
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Ispa-Instituto Universitário
Idioma:inglês
Origem:Repositório do Ispa - Instituto Universitário
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author Cunha, Marta Fernandez
author2 Coscueta, Ezequiel
Emilia Brassesco, M.
Marques, Rita
Neto, José
Almada, Frederico José Oliveira de
Goncalves, David
Pintado, Maria Manuela
author2_role author
author
author
author
author
author
author
author_facet Cunha, Marta Fernandez
Coscueta, Ezequiel
Emilia Brassesco, M.
Marques, Rita
Neto, José
Almada, Frederico José Oliveira de
Goncalves, David
Pintado, Maria Manuela
author_role author
contributor_name_str_mv Repositório do ISPA
country_str PT
creators_json_str [{\"Person.name\":\"Cunha, Marta Fernandez\",\"Person.identifier.orcid\":\"0000-0001-5935-8670\"},{\"Person.name\":\"Coscueta, Ezequiel\",\"Person.identifier.orcid\":\"0000-0003-4496-2001\"},{\"Person.name\":\"Emilia Brassesco, M.\",\"Person.identifier.orcid\":\"0000-0001-9027-4643\"},{\"Person.name\":\"Marques, Rita\"},{\"Person.name\":\"Neto, José\"},{\"Person.name\":\"Almada, Frederico José Oliveira de\",\"Person.identifier.orcid\":\"0000-0002-1389-8951\"},{\"Person.name\":\"Goncalves, David\",\"Person.identifier.orcid\":\"0000-0001-6851-7215\"},{\"Person.name\":\"Pintado, Maria Manuela\",\"Person.identifier.orcid\":\"0000-0002-0760-3184\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Repositório do ISPA
datacite.creators.creator.creatorName.fl_str_mv Cunha, Marta Fernandez
Coscueta, Ezequiel
Emilia Brassesco, M.
Marques, Rita
Neto, José
Almada, Frederico José Oliveira de
Goncalves, David
Pintado, Maria Manuela
datacite.date.Accepted.fl_str_mv 2023-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2024-02-27T19:18:43Z
datacite.date.embargoed.fl_str_mv 2024-02-27T19:18:43Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Ichthyocrinotoxins
Antimicrobial
Antioxidant
Antihypertensive
Peptides
datacite.titles.title.fl_str_mv Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
dc.contributor.none.fl_str_mv Repositório do ISPA
dc.creator.none.fl_str_mv Cunha, Marta Fernandez
Coscueta, Ezequiel
Emilia Brassesco, M.
Marques, Rita
Neto, José
Almada, Frederico José Oliveira de
Goncalves, David
Pintado, Maria Manuela
dc.date.Accepted.fl_str_mv 2023-01-01T00:00:00Z
dc.date.available.fl_str_mv 2024-02-27T19:18:43Z
dc.date.embargoed.fl_str_mv 2024-02-27T19:18:43Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10400.12/9620
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv MDPI
dc.rights.cclincense.fl_str_mv http://creativecommons.org/licenses/by-nc/4.0/
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Ichthyocrinotoxins
Antimicrobial
Antioxidant
Antihypertensive
Peptides
dc.title.fl_str_mv Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description Identifying bioactive molecules from marine organisms is still vastly understudied. Fish remain an untapped source of bioactive molecules, even when considering species whose toxicity to other fish species has been noticed before. We assessed potential applications of crude body mucus of the Lusitanian toadfish (Halobratachus didactylus) and characterized its peptide fraction composition. Mucus samples from three individuals (two wild and one captive) revealed potential antioxidant, antihypertensive, and antimicrobial activities. For antioxidant activity, the best results of 2371 ± 97 µmol Trolox Equivalent/g protein for ORAC and 154 ± 6 µmol Trolox Equivalent/g protein for ABTS were obtained. For antihypertensive activity, the relevant inhibitory activity of ACE resulted in IC50 of 60 ± 7 µg protein/mL. Antimicrobial activity was also identified against the pathogenic bacteria Escherichia coli and Listeria monocytogenes. The peptide profile of the crude body mucus was obtained through size exclusion chromatography, with a conspicuous peak at ca. 800 Da. LC-MS/MS allowed the detection of the most probable peptide sequences of this dominant peptide. This is the first study where the bioactive potential of mucus from the Lusitanian toadfish is demonstrated. Peptides with such properties can be applied in the food and pharmaceutical industries.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://repositorio.ispa.pt/bitstreams/7a11bc53-530b-48a3-93d3-472431fed30e/download
funding.funder.alternateName_str_mv FCT
funding.funder.identifier_str_mv http://doi.org/10.13039/501100001871
funding.funder.name_str_mv Fundação para a Ciência e a Tecnologia
funding.identifier_str_mv UI/BD/150955/2021
funding.name_str_mv POR_CENTRO
funding_str_mv UI/BD/150955/2021
info:eu-repo/grantAgreement/FCT/POR_CENTRO/UI%2FBD%2F150955%2F2021/PT
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identifier.url.fl_str_mv http://hdl.handle.net/10400.12/9620
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instname_str Ispa-Instituto Universitário
language eng
network_acronym_str ispa
network_name_str Repositório do Ispa - Instituto Universitário
oai_identifier_str oai:repositorio.ispa.pt:10400.12/9620
organization_str_mv urn:organizationAcronym:ispa
person_str_mv Cunha, Marta Fernandez
Cunha, Marta Fernandez
http://orcid.org/0000-0001-5935-8670
0000-0001-5935-8670
Coscueta, Ezequiel
Coscueta, Ezequiel
https://www.ciencia-id.pt/6614-705D-EBA7
6614-705D-EBA7
http://orcid.org/0000-0003-4496-2001
0000-0003-4496-2001
Emilia Brassesco, M.
Emilia Brassesco, M.
https://www.ciencia-id.pt/4819-BAD3-AF07
4819-BAD3-AF07
http://orcid.org/0000-0001-9027-4643
0000-0001-9027-4643
Marques, Rita
Neto, José
Almada, Frederico José Oliveira de
Almada, Frederico José Oliveira de
https://www.ciencia-id.pt/0215-02F9-6D3E
0215-02F9-6D3E
http://orcid.org/0000-0002-1389-8951
0000-0002-1389-8951
Goncalves, David
Goncalves, David
https://www.ciencia-id.pt/331D-3437-C4CD
331D-3437-C4CD
http://orcid.org/0000-0001-6851-7215
0000-0001-6851-7215
Pintado, Maria Manuela
Pintado, Maria Manuela
https://www.ciencia-id.pt/2F13-AAE0-3405
2F13-AAE0-3405
http://orcid.org/0000-0002-0760-3184
0000-0002-0760-3184
publishDate 2023
publisher.none.fl_str_mv MDPI
reponame_str Repositório do Ispa - Instituto Universitário
repository_id_str urn:repositoryAcronym:ispa
service_str_mv urn:repositoryAcronym:ispa
spelling engMDPIpt_PTIdentifying bioactive molecules from marine organisms is still vastly understudied. Fish remain an untapped source of bioactive molecules, even when considering species whose toxicity to other fish species has been noticed before. We assessed potential applications of crude body mucus of the Lusitanian toadfish (Halobratachus didactylus) and characterized its peptide fraction composition. Mucus samples from three individuals (two wild and one captive) revealed potential antioxidant, antihypertensive, and antimicrobial activities. For antioxidant activity, the best results of 2371 ± 97 µmol Trolox Equivalent/g protein for ORAC and 154 ± 6 µmol Trolox Equivalent/g protein for ABTS were obtained. For antihypertensive activity, the relevant inhibitory activity of ACE resulted in IC50 of 60 ± 7 µg protein/mL. Antimicrobial activity was also identified against the pathogenic bacteria Escherichia coli and Listeria monocytogenes. The peptide profile of the crude body mucus was obtained through size exclusion chromatography, with a conspicuous peak at ca. 800 Da. LC-MS/MS allowed the detection of the most probable peptide sequences of this dominant peptide. This is the first study where the bioactive potential of mucus from the Lusitanian toadfish is demonstrated. Peptides with such properties can be applied in the food and pharmaceutical industries.application/pdfpt_PTExploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylusPersonalCunha, Marta FernandezDSpacehttp://dspace.org/items/801d530c-c6f6-4df1-924f-bce736f967fdDSpacehttp://dspace.org/items/801d530c-c6f6-4df1-924f-bce736f967fdFernandez CunhaMartaORCIDhttp://orcid.org0000-0001-5935-8670PersonalCoscueta, EzequielDSpacehttp://dspace.org/items/34b50ef9-7150-4c49-b926-ebf7de3ce090DSpacehttp://dspace.org/items/34b50ef9-7150-4c49-b926-ebf7de3ce090CoscuetaEzequielCiência IDhttps://www.ciencia-id.pt6614-705D-EBA7ORCIDhttp://orcid.org0000-0003-4496-2001Researcher IDhttps://www.researcherid.comJ-7033-2016Scopus Author IDhttps://www.scopus.com56986455000Scopus Author IDhttps://www.scopus.com56986455000PersonalEmilia Brassesco, M.DSpacehttp://dspace.org/items/6134b4a6-5042-47d1-a045-e9378385b801DSpacehttp://dspace.org/items/6134b4a6-5042-47d1-a045-e9378385b801BrassescoMaria EmiliaCiência IDhttps://www.ciencia-id.pt4819-BAD3-AF07ORCIDhttp://orcid.org0000-0001-9027-4643Scopus Author IDhttps://www.scopus.com57190497489Marques, RitaNeto, JoséPersonalAlmada, Frederico José Oliveira deDSpacehttp://dspace.org/items/a19a10df-787c-46d8-8609-e6d2bed22ea3DSpacehttp://dspace.org/items/a19a10df-787c-46d8-8609-e6d2bed22ea3AlmadaFredericoCiência IDhttps://www.ciencia-id.pt0215-02F9-6D3EORCIDhttp://orcid.org0000-0002-1389-8951PersonalGoncalves, DavidDSpacehttp://dspace.org/items/27b0d293-10b6-4dbb-8036-398892702e14DSpacehttp://dspace.org/items/27b0d293-10b6-4dbb-8036-398892702e14GoncalvesDavidCiência IDhttps://www.ciencia-id.pt331D-3437-C4CDORCIDhttp://orcid.org0000-0001-6851-7215Researcher IDhttps://www.researcherid.comL-3514-2016Scopus Author IDhttps://www.scopus.com7005392651PersonalPintado, Maria ManuelaDSpacehttp://dspace.org/items/282afe88-aa53-4748-ac0f-2ad99cbf9604DSpacehttp://dspace.org/items/282afe88-aa53-4748-ac0f-2ad99cbf9604PintadoMaria ManuelaCiência IDhttps://www.ciencia-id.pt2F13-AAE0-3405ORCIDhttp://orcid.org0000-0002-0760-3184Scopus Author IDhttps://www.scopus.com7004483898HostingInstitutionOrganizationalRepositório do ISPAe-mailmailto:repositorio@ispa.ptrepositorio@ispa.ptISSNIsPartOf14203049DOIIsPartOf10.3390/molecules281864582024-02-27T19:18:43Z20232023-01-01T00:00:00ZHandlehttp://hdl.handle.net/10400.12/9620http://purl.org/coar/access_right/c_abf2open accessIchthyocrinotoxinsAntimicrobialAntioxidantAntihypertensivePeptides2495604 bytesFundação para a Ciência e a TecnologiaFishVen - Fish venom diversity in Atlanto-Mediterranean scorpionfish Scorpaena. Venomics, evolution and impact on fisheries.info:eu-repo/grantAgreement/FCT/POR_CENTRO/UI%2FBD%2F150955%2F2021/PTUI/BD/150955/2021POR_CENTROCrossref Funder IDhttp://doi.org/10.13039/501100001871literaturehttp://purl.org/coar/resource_type/c_6501journal article2023http://creativecommons.org/licenses/by-nc/4.0/http://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://repositorio.ispa.pt/bitstreams/7a11bc53-530b-48a3-93d3-472431fed30e/downloadMolecules28186458Switzerland
spellingShingle Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
Cunha, Marta Fernandez
Ichthyocrinotoxins
Antimicrobial
Antioxidant
Antihypertensive
Peptides
subject.fl_str_mv Ichthyocrinotoxins
Antimicrobial
Antioxidant
Antihypertensive
Peptides
title Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
title_full Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
title_fullStr Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
title_full_unstemmed Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
title_short Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
title_sort Exploring bioactivities and peptide content of body mucus from the lusitanian toadfish Halobatrachus didactylus
topic Ichthyocrinotoxins
Antimicrobial
Antioxidant
Antihypertensive
Peptides
topic_facet Ichthyocrinotoxins
Antimicrobial
Antioxidant
Antihypertensive
Peptides
url http://hdl.handle.net/10400.12/9620
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