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Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps

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Resumo:The relationships between clay minerals and associated iron and arsenic-rich phases are a main scientific issue in reactive mine waste-dumps. Therefore, this paper documents the composition and morphology of the fine fraction (<2 μm), including the nano-sized Fe and As precipitates, associated with clay minerals in three distinctive sulfide-rich waste-dumps: Cerdeirinha, Lapa Grande, and Penedono (Northern Portugal). The obtained results indicated that the study sites have similar relative proportions of the detrital materials. However, major differences were observed in the remainder phases, which is in accordance with the mineralogy that was inherited from the respective ore deposits. In general, the clay mineral assemblage is dominated by the presence of illite, halloysite(7 Å), and beidellite. There are also associated minerals, such as jarosite and goethite, as well as amorphous As-rich nanoprecipitates with specific morphologies. Moreover, the results suggested that AMD conditions control the physical–chemical transformations, namely constraining the stability of the secondary phases formed by weathering in the waste dumps. Acidity is responsible for the degradation of the clay minerals, which is reflected in their crystalochemistry, structural order–disorder, and morphology. On the contrary, jarosite is more stable, being a dominant mineral in such environmental conditions. The stability of amorphous ferric arsenates or its evolution to a more crystalline phase is dependent on the Fe:As ratio, which is lower in Penedono. The study of the secondary products, especially the nanoparticles, puts in evidence their ability to control the mobility of trace elements, suggesting potential applications in environmental technology, including remediation of reactive mine waste-dumps.
Autores principais:Valente, Teresa Maria Fernandes
Outros Autores:Gomes, Patrícia; Braga, Maria Amália Castro Sequeira; Dionísio, Amélia; Pamplona, J.; Grande, J. A.
Assunto:Halloysite(7 Å) Beidellite Jarosite Goethite As-Fe-rich nanoparticles Mine waste -dumps Halloysite(7 angstrom)
Ano:2015
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso restrito
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Valente, Teresa Maria Fernandes
author2 Gomes, Patrícia
Braga, Maria Amália Castro Sequeira
Dionísio, Amélia
Pamplona, J.
Grande, J. A.
author2_role author
author
author
author
author
author_facet Valente, Teresa Maria Fernandes
Gomes, Patrícia
Braga, Maria Amália Castro Sequeira
Dionísio, Amélia
Pamplona, J.
Grande, J. A.
author_role author
contributor_name_str_mv Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Valente, Teresa Maria Fernandes\"},{\"Person.name\":\"Gomes, Patrícia\"},{\"Person.name\":\"Braga, Maria Amália Castro Sequeira\"},{\"Person.name\":\"Dionísio, Amélia\"},{\"Person.name\":\"Pamplona, J.\"},{\"Person.name\":\"Grande, J. A.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Valente, Teresa Maria Fernandes
Gomes, Patrícia
Braga, Maria Amália Castro Sequeira
Dionísio, Amélia
Pamplona, J.
Grande, J. A.
datacite.date.Accepted.fl_str_mv 2015-03-25T00:00:00Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_16ec
datacite.subjects.subject.fl_str_mv Halloysite(7 Å)
Beidellite
Jarosite
Goethite
As-Fe-rich nanoparticles
Mine waste -dumps
Halloysite(7 angstrom)
datacite.titles.title.fl_str_mv Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
dc.contributor.none.fl_str_mv Universidade do Minho
dc.creator.none.fl_str_mv Valente, Teresa Maria Fernandes
Gomes, Patrícia
Braga, Maria Amália Castro Sequeira
Dionísio, Amélia
Pamplona, J.
Grande, J. A.
dc.date.Accepted.fl_str_mv 2015-03-25T00:00:00Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/45608
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Elsevier
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_16ec
dc.subject.none.fl_str_mv Halloysite(7 Å)
Beidellite
Jarosite
Goethite
As-Fe-rich nanoparticles
Mine waste -dumps
Halloysite(7 angstrom)
dc.title.fl_str_mv Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description The relationships between clay minerals and associated iron and arsenic-rich phases are a main scientific issue in reactive mine waste-dumps. Therefore, this paper documents the composition and morphology of the fine fraction (<2 μm), including the nano-sized Fe and As precipitates, associated with clay minerals in three distinctive sulfide-rich waste-dumps: Cerdeirinha, Lapa Grande, and Penedono (Northern Portugal). The obtained results indicated that the study sites have similar relative proportions of the detrital materials. However, major differences were observed in the remainder phases, which is in accordance with the mineralogy that was inherited from the respective ore deposits. In general, the clay mineral assemblage is dominated by the presence of illite, halloysite(7 Å), and beidellite. There are also associated minerals, such as jarosite and goethite, as well as amorphous As-rich nanoprecipitates with specific morphologies. Moreover, the results suggested that AMD conditions control the physical–chemical transformations, namely constraining the stability of the secondary phases formed by weathering in the waste dumps. Acidity is responsible for the degradation of the clay minerals, which is reflected in their crystalochemistry, structural order–disorder, and morphology. On the contrary, jarosite is more stable, being a dominant mineral in such environmental conditions. The stability of amorphous ferric arsenates or its evolution to a more crystalline phase is dependent on the Fe:As ratio, which is lower in Penedono. The study of the secondary products, especially the nanoparticles, puts in evidence their ability to control the mobility of trace elements, suggesting potential applications in environmental technology, including remediation of reactive mine waste-dumps.
dirty 0
eu_rights_str_mv restrictedAccess
format article
fulltext.url.fl_str_mv https://prod-dspace.uminho.pt/bitstreams/0996d16b-de46-4d36-a18e-51bc1a684dab/download
id rum_3d0a4a4ac970024c7cf3e7acfba74c19
identifier.url.fl_str_mv https://hdl.handle.net/1822/45608
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/45608
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Valente, Teresa Maria Fernandes
Gomes, Patrícia
Braga, Maria Amália Castro Sequeira
Dionísio, Amélia
Pamplona, J.
Grande, J. A.
publishDate 2015
publisher.none.fl_str_mv Elsevier
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engElsevierporThe relationships between clay minerals and associated iron and arsenic-rich phases are a main scientific issue in reactive mine waste-dumps. Therefore, this paper documents the composition and morphology of the fine fraction (<2 μm), including the nano-sized Fe and As precipitates, associated with clay minerals in three distinctive sulfide-rich waste-dumps: Cerdeirinha, Lapa Grande, and Penedono (Northern Portugal). The obtained results indicated that the study sites have similar relative proportions of the detrital materials. However, major differences were observed in the remainder phases, which is in accordance with the mineralogy that was inherited from the respective ore deposits. In general, the clay mineral assemblage is dominated by the presence of illite, halloysite(7 Å), and beidellite. There are also associated minerals, such as jarosite and goethite, as well as amorphous As-rich nanoprecipitates with specific morphologies. Moreover, the results suggested that AMD conditions control the physical–chemical transformations, namely constraining the stability of the secondary phases formed by weathering in the waste dumps. Acidity is responsible for the degradation of the clay minerals, which is reflected in their crystalochemistry, structural order–disorder, and morphology. On the contrary, jarosite is more stable, being a dominant mineral in such environmental conditions. The stability of amorphous ferric arsenates or its evolution to a more crystalline phase is dependent on the Fe:As ratio, which is lower in Penedono. The study of the secondary products, especially the nanoparticles, puts in evidence their ability to control the mobility of trace elements, suggesting potential applications in environmental technology, including remediation of reactive mine waste-dumps.application/pdfporIron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumpsValente, Teresa Maria FernandesGomes, PatríciaBraga, Maria Amália Castro SequeiraDionísio, AméliaPamplona, J.Grande, J. A.HostingInstitutionOrganizationalUniversidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptISSNIsPartOf0341-8162DOIIsPartOf10.1016/j.catena.2015.03.0092015-03-252014-102015-03-25T00:00:00ZHandlehttps://hdl.handle.net/1822/45608http://purl.org/coar/access_right/c_16ecrestricted accessHalloysite(7 Å)BeidelliteJarositeGoethiteAs-Fe-rich nanoparticlesMine waste -dumpsHalloysite(7 angstrom)2026951 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_16ecapplication/pdffulltexthttps://prod-dspace.uminho.pt/bitstreams/0996d16b-de46-4d36-a18e-51bc1a684dab/download
spellingShingle Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
Valente, Teresa Maria Fernandes
Halloysite(7 Å)
Beidellite
Jarosite
Goethite
As-Fe-rich nanoparticles
Mine waste -dumps
Halloysite(7 angstrom)
status SINGLETON
subject.fl_str_mv Halloysite(7 Å)
Beidellite
Jarosite
Goethite
As-Fe-rich nanoparticles
Mine waste -dumps
Halloysite(7 angstrom)
title Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
title_full Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
title_fullStr Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
title_full_unstemmed Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
title_short Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
title_sort Iron and arsenic-rich nanoprecipitates associated with clay minerals in sulfide-rich waste dumps
topic Halloysite(7 Å)
Beidellite
Jarosite
Goethite
As-Fe-rich nanoparticles
Mine waste -dumps
Halloysite(7 angstrom)
topic_facet Halloysite(7 Å)
Beidellite
Jarosite
Goethite
As-Fe-rich nanoparticles
Mine waste -dumps
Halloysite(7 angstrom)
url https://hdl.handle.net/1822/45608
visible 1