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Short-chain di-ureasil ormolytes doped with potassium triflate: Phase diagram and conductivity behavior

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Detalhes bibliográficos
Resumo:Di-urea cross-linked poly(oxyethylene)/siloxane hybrids, synthesized by the sol-gel process and containing a wide concentration range of potassium triflate, KCF3SO3, have been analyzed by x-ray diffraction and differential scanning calorimetry. The pseudo-phase diagram proposed has been taken into account in the interpretation of the complex impedance measurements. The xerogels prepared are obtained as transparent, thin monoliths . At room temperature the highest conductivity found was 2 x 10-6Scm-1.
Autores principais:Zea Bermudez, V. de
Outros Autores:Correia, M. Gomes; Silva, Maria Manuela; Barros, Sandra Cerqueira; Smith, Michael John; Ferreira, R. A. Sá; Carlos, L. D.; Molina, C.; Ribeiro, A. J. L.
Assunto:Di-ureasils Phase diagram Ionic conductivity Thermal analysis potassium triflate
Ano:2003
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
Descrição
Resumo:Di-urea cross-linked poly(oxyethylene)/siloxane hybrids, synthesized by the sol-gel process and containing a wide concentration range of potassium triflate, KCF3SO3, have been analyzed by x-ray diffraction and differential scanning calorimetry. The pseudo-phase diagram proposed has been taken into account in the interpretation of the complex impedance measurements. The xerogels prepared are obtained as transparent, thin monoliths . At room temperature the highest conductivity found was 2 x 10-6Scm-1.