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Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair

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Resumo:The aim of this study was to develop and characterize a double layer biomembrane for dual drug delivery to be used for the treatment of wounds. The membrane was composed of chitosan, hydroxypropyl methylcellulose and lidocaine chloride (anesthetic drug) in the first layer, and of sodium alginate-polymyxin B sulphate (antibiotic) nanoparticles as the second layer. A product with excellent thickness (0.01-0.02 mm), adequate mechanical properties with respect to elasticity, stiffness, tension, and compatible pH for lesion application has been successfully obtained. The incorporation of the drugs was confirmed analysing the membrane cross-sections by scanning electron microscopy. A strong interaction between the drugs and the functional groups of respective polymers was confirmed by Fourier-Transform Infrared Spectroscopy, thermal analysis and X-ray diffraction. Microbiological assays showed a high antimicrobial activity when polymyxin B was present to act against the Staphylococcus aureus and Pseudomonas aeruginosa strains. Low cytotoxicity observed in a cell viability colorimetric assay and SEM analysis suggest biocompatibility between the developed biomembrane and the cell culture. The in vivo assay allowed visualizing the healing potential by calculating the wound retraction index and by histological analysis. Our results confirm the effectiveness of the developed innovative biomaterial for tissue repair and regeneration in an animal model.
Autores principais:Oliveira, D. M. L.
Outros Autores:Rezende, P. S.; Barbosa, T. C.; Nalone, L. A.; Bani, C.; Tavares, D. S.; Silva, C. F. da; Chaud, M. V.; Padilha, F.; Cano, A.; Albuquerque Júnior, R. L. C. de; Souto, Eliana B.; Severino, P.
Assunto:double membrane polymyxin B sulphate lidocaine hydrochloride solid lipid nanoparticles burst release controlled release
Ano:2020
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Oliveira, D. M. L.
author2 Rezende, P. S.
Barbosa, T. C.
Nalone, L. A.
Bani, C.
Tavares, D. S.
Silva, C. F. da
Chaud, M. V.
Padilha, F.
Cano, A.
Albuquerque Júnior, R. L. C. de
Souto, Eliana B.
Severino, P.
author2_role author
author
author
author
author
author
author
author
author
author
author
author
author_facet Oliveira, D. M. L.
Rezende, P. S.
Barbosa, T. C.
Nalone, L. A.
Bani, C.
Tavares, D. S.
Silva, C. F. da
Chaud, M. V.
Padilha, F.
Cano, A.
Albuquerque Júnior, R. L. C. de
Souto, Eliana B.
Severino, P.
author_role author
contributor_name_str_mv RepositóriUM - Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Oliveira, D. M. L.\"},{\"Person.name\":\"Rezende, P. S.\"},{\"Person.name\":\"Barbosa, T. C.\"},{\"Person.name\":\"Nalone, L. A.\"},{\"Person.name\":\"Bani, C.\"},{\"Person.name\":\"Tavares, D. S.\"},{\"Person.name\":\"Silva, C. F. da\"},{\"Person.name\":\"Chaud, M. V.\"},{\"Person.name\":\"Padilha, F.\"},{\"Person.name\":\"Cano, A.\"},{\"Person.name\":\"Albuquerque Júnior, R. L. C. de\"},{\"Person.name\":\"Souto, Eliana B.\"},{\"Person.name\":\"Severino, P.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv RepositóriUM - Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Oliveira, D. M. L.
Rezende, P. S.
Barbosa, T. C.
Nalone, L. A.
Bani, C.
Tavares, D. S.
Silva, C. F. da
Chaud, M. V.
Padilha, F.
Cano, A.
Albuquerque Júnior, R. L. C. de
Souto, Eliana B.
Severino, P.
datacite.date.Accepted.fl_str_mv 2020-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2020-11-02T17:37:10Z
datacite.date.embargoed.fl_str_mv 2020-11-02T17:37:10Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv double membrane
polymyxin B sulphate
lidocaine hydrochloride
solid lipid nanoparticles
burst release
controlled release
datacite.titles.title.fl_str_mv Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
dc.contributor.none.fl_str_mv RepositóriUM - Universidade do Minho
dc.creator.none.fl_str_mv Oliveira, D. M. L.
Rezende, P. S.
Barbosa, T. C.
Nalone, L. A.
Bani, C.
Tavares, D. S.
Silva, C. F. da
Chaud, M. V.
Padilha, F.
Cano, A.
Albuquerque Júnior, R. L. C. de
Souto, Eliana B.
Severino, P.
dc.date.Accepted.fl_str_mv 2020-01-01T00:00:00Z
dc.date.available.fl_str_mv 2020-11-02T17:37:10Z
dc.date.embargoed.fl_str_mv 2020-11-02T17:37:10Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/67979
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Elsevier
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv double membrane
polymyxin B sulphate
lidocaine hydrochloride
solid lipid nanoparticles
burst release
controlled release
dc.title.fl_str_mv Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description The aim of this study was to develop and characterize a double layer biomembrane for dual drug delivery to be used for the treatment of wounds. The membrane was composed of chitosan, hydroxypropyl methylcellulose and lidocaine chloride (anesthetic drug) in the first layer, and of sodium alginate-polymyxin B sulphate (antibiotic) nanoparticles as the second layer. A product with excellent thickness (0.01-0.02 mm), adequate mechanical properties with respect to elasticity, stiffness, tension, and compatible pH for lesion application has been successfully obtained. The incorporation of the drugs was confirmed analysing the membrane cross-sections by scanning electron microscopy. A strong interaction between the drugs and the functional groups of respective polymers was confirmed by Fourier-Transform Infrared Spectroscopy, thermal analysis and X-ray diffraction. Microbiological assays showed a high antimicrobial activity when polymyxin B was present to act against the Staphylococcus aureus and Pseudomonas aeruginosa strains. Low cytotoxicity observed in a cell viability colorimetric assay and SEM analysis suggest biocompatibility between the developed biomembrane and the cell culture. The in vivo assay allowed visualizing the healing potential by calculating the wound retraction index and by histological analysis. Our results confirm the effectiveness of the developed innovative biomaterial for tissue repair and regeneration in an animal model.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://repositorium.uminho.pt/bitstreams/b9a94d1d-566c-4e19-9d29-794059c01810/download
id rum_711fcb4a3189cd493003fee320e7461c
identifier.url.fl_str_mv https://hdl.handle.net/1822/67979
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/67979
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Oliveira, D. M. L.
Rezende, P. S.
Barbosa, T. C.
Nalone, L. A.
Bani, C.
Tavares, D. S.
Silva, C. F. da
Chaud, M. V.
Padilha, F.
Cano, A.
Albuquerque Júnior, R. L. C. de
Souto, Eliana B.
Severino, P.
publishDate 2020
publisher.none.fl_str_mv Elsevier
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engElsevierporThe aim of this study was to develop and characterize a double layer biomembrane for dual drug delivery to be used for the treatment of wounds. The membrane was composed of chitosan, hydroxypropyl methylcellulose and lidocaine chloride (anesthetic drug) in the first layer, and of sodium alginate-polymyxin B sulphate (antibiotic) nanoparticles as the second layer. A product with excellent thickness (0.01-0.02 mm), adequate mechanical properties with respect to elasticity, stiffness, tension, and compatible pH for lesion application has been successfully obtained. The incorporation of the drugs was confirmed analysing the membrane cross-sections by scanning electron microscopy. A strong interaction between the drugs and the functional groups of respective polymers was confirmed by Fourier-Transform Infrared Spectroscopy, thermal analysis and X-ray diffraction. Microbiological assays showed a high antimicrobial activity when polymyxin B was present to act against the Staphylococcus aureus and Pseudomonas aeruginosa strains. Low cytotoxicity observed in a cell viability colorimetric assay and SEM analysis suggest biocompatibility between the developed biomembrane and the cell culture. The in vivo assay allowed visualizing the healing potential by calculating the wound retraction index and by histological analysis. Our results confirm the effectiveness of the developed innovative biomaterial for tissue repair and regeneration in an animal model.application/pdfporDouble membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repairOliveira, D. M. L.Rezende, P. S.Barbosa, T. C.Nalone, L. A.Bani, C.Tavares, D. S.Silva, C. F. daChaud, M. V.Padilha, F.Cano, A.Albuquerque Júnior, R. L. C. deSouto, Eliana B.Severino, P.HostingInstitutionOrganizationalRepositóriUM - Universidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptCITATIONOliveira, D. M. L.; Rezende, P. S.; Barbosa, T. C.; Nalone, L. A.; Bani, C.; Tavares, D. S.; Silva, C. F. da; Chaud, M. V.; Padilha, F.; Cano, A.; Albuquerque Júnior, R. L. C. de; Souto, Eliana; Severino, P., Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair. International Journal of Pharmaceutics, 591(120001), 2020PMID33141086ISSNIsPartOf0378-5173DOIIsPartOf10.1016/j.ijpharm.2020.1200012020-11-02T17:37:10Z20202020-10-31T11:45:15Z2020-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/67979http://purl.org/coar/access_right/c_abf2open accessdouble membranepolymyxin B sulphatelidocaine hydrochloridesolid lipid nanoparticlesburst releasecontrolled release15587734 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://repositorium.uminho.pt/bitstreams/b9a94d1d-566c-4e19-9d29-794059c01810/download
spellingShingle Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
Oliveira, D. M. L.
double membrane
polymyxin B sulphate
lidocaine hydrochloride
solid lipid nanoparticles
burst release
controlled release
status SINGLETON
subject.fl_str_mv double membrane
polymyxin B sulphate
lidocaine hydrochloride
solid lipid nanoparticles
burst release
controlled release
title Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
title_full Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
title_fullStr Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
title_full_unstemmed Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
title_short Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
title_sort Double membrane based on lidocaine-coated polymyxin-alginate nanoparticles for wound healing: in vitro characterization and in vivo tissue repair
topic double membrane
polymyxin B sulphate
lidocaine hydrochloride
solid lipid nanoparticles
burst release
controlled release
topic_facet double membrane
polymyxin B sulphate
lidocaine hydrochloride
solid lipid nanoparticles
burst release
controlled release
url https://hdl.handle.net/1822/67979
visible 1