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Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor

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Resumo:One of the major challenges in biofuels production from lignocellulosic biomass is the generation of high glucose titers from cellulose in the enzymatic hydrolysis stage of pretreated biomass to guarantee a cost-effective process. Therefore, the enzymatic saccharification on cellulose at high solid loading is an alternative. In this work, the agave bagasse was hydrothermally pretreated and optimized at 194°C/30min, obtaining a pretreated solid rich in cellulose content (>46.46%), and subjected to enzymatic hydrolysis at high solid levels. A horizontal bioreactor was designed for enzyme saccharification at high solid loadings [25% (w/v)]. The bioreactor improved mixing efficiency, with cellulose conversions up to 98% (195.6g/L at 72h). Moreover, mathematical modeling of cellulase deactivation demonstrated that cellulases lose most of their initial activity in the first hours of the reaction. Also, cellulose was characterized by X-ray diffraction, and the pretreated solids were visualized using scanning electron microscopy.
Autores principais:Pino, Marcela Sofía
Outros Autores:Rodríguez-Jasso, Rosa M.; Michelin, Michele; Ruiz, Héctor A.
Assunto:Glucan Glucose Biofuels Autohydrolysis Severity Factor Biorefinery
Ano:2019
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Pino, Marcela Sofía
author2 Rodríguez-Jasso, Rosa M.
Michelin, Michele
Ruiz, Héctor A.
author2_role author
author
author
author_facet Pino, Marcela Sofía
Rodríguez-Jasso, Rosa M.
Michelin, Michele
Ruiz, Héctor A.
author_role author
contributor_name_str_mv RepositóriUM - Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Pino, Marcela Sofía\"},{\"Person.name\":\"Rodríguez-Jasso, Rosa M.\"},{\"Person.name\":\"Michelin, Michele\"},{\"Person.name\":\"Ruiz, Héctor A.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv RepositóriUM - Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Pino, Marcela Sofía
Rodríguez-Jasso, Rosa M.
Michelin, Michele
Ruiz, Héctor A.
datacite.date.Accepted.fl_str_mv 2019-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2019-02-18T11:04:03Z
datacite.date.embargoed.fl_str_mv 2019-02-18T11:04:03Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Glucan
Glucose
Biofuels
Autohydrolysis
Severity Factor
Biorefinery
datacite.titles.title.fl_str_mv Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
dc.contributor.none.fl_str_mv RepositóriUM - Universidade do Minho
dc.creator.none.fl_str_mv Pino, Marcela Sofía
Rodríguez-Jasso, Rosa M.
Michelin, Michele
Ruiz, Héctor A.
dc.date.Accepted.fl_str_mv 2019-01-01T00:00:00Z
dc.date.available.fl_str_mv 2019-02-18T11:04:03Z
dc.date.embargoed.fl_str_mv 2019-02-18T11:04:03Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/59092
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Elsevier
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Glucan
Glucose
Biofuels
Autohydrolysis
Severity Factor
Biorefinery
dc.title.fl_str_mv Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description One of the major challenges in biofuels production from lignocellulosic biomass is the generation of high glucose titers from cellulose in the enzymatic hydrolysis stage of pretreated biomass to guarantee a cost-effective process. Therefore, the enzymatic saccharification on cellulose at high solid loading is an alternative. In this work, the agave bagasse was hydrothermally pretreated and optimized at 194°C/30min, obtaining a pretreated solid rich in cellulose content (>46.46%), and subjected to enzymatic hydrolysis at high solid levels. A horizontal bioreactor was designed for enzyme saccharification at high solid loadings [25% (w/v)]. The bioreactor improved mixing efficiency, with cellulose conversions up to 98% (195.6g/L at 72h). Moreover, mathematical modeling of cellulase deactivation demonstrated that cellulases lose most of their initial activity in the first hours of the reaction. Also, cellulose was characterized by X-ray diffraction, and the pretreated solids were visualized using scanning electron microscopy.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://repositorium.uminho.pt/bitstreams/44fa4e0d-d9e4-4cdd-b598-0843916a1ba8/download
id rum_9bfe02ca9362c1cd9dca97b54a5e33e5
identifier.url.fl_str_mv https://hdl.handle.net/1822/59092
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/59092
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Pino, Marcela Sofía
Rodríguez-Jasso, Rosa M.
Michelin, Michele
Ruiz, Héctor A.
publishDate 2019
publisher.none.fl_str_mv Elsevier
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engElsevierporOne of the major challenges in biofuels production from lignocellulosic biomass is the generation of high glucose titers from cellulose in the enzymatic hydrolysis stage of pretreated biomass to guarantee a cost-effective process. Therefore, the enzymatic saccharification on cellulose at high solid loading is an alternative. In this work, the agave bagasse was hydrothermally pretreated and optimized at 194°C/30min, obtaining a pretreated solid rich in cellulose content (>46.46%), and subjected to enzymatic hydrolysis at high solid levels. A horizontal bioreactor was designed for enzyme saccharification at high solid loadings [25% (w/v)]. The bioreactor improved mixing efficiency, with cellulose conversions up to 98% (195.6g/L at 72h). Moreover, mathematical modeling of cellulase deactivation demonstrated that cellulases lose most of their initial activity in the first hours of the reaction. Also, cellulose was characterized by X-ray diffraction, and the pretreated solids were visualized using scanning electron microscopy.application/pdfporEnhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactorPino, Marcela SofíaRodríguez-Jasso, Rosa M.Michelin, MicheleRuiz, Héctor A.HostingInstitutionOrganizationalRepositóriUM - Universidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptCITATIONPino, Marcela; Rodríguez-Jasso, Rosa M.; Michelin, Michele; Ruiz, Héctor A., Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor. Carbohydrate Polymers, 211, 349-359, 2019PMID30824099ISSNIsPartOf0144-8617EISSNIsPartOf0144-8617DOIIsPartOf10.1016/j.carbpol.2019.01.1112019-02-18T11:04:03Z20192019-02-17T12:48:39Z2019-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/59092http://purl.org/coar/access_right/c_abf2open accessGlucanGlucoseBiofuelsAutohydrolysisSeverity FactorBiorefinery3618564 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://repositorium.uminho.pt/bitstreams/44fa4e0d-d9e4-4cdd-b598-0843916a1ba8/download
spellingShingle Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
Pino, Marcela Sofía
Glucan
Glucose
Biofuels
Autohydrolysis
Severity Factor
Biorefinery
status SINGLETON
subject.fl_str_mv Glucan
Glucose
Biofuels
Autohydrolysis
Severity Factor
Biorefinery
title Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
title_full Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
title_fullStr Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
title_full_unstemmed Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
title_short Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
title_sort Enhancement and modeling of enzymatic hydrolysis on cellulose from Agave bagasse hydrothermally pretreated in a horizontal bioreactor
topic Glucan
Glucose
Biofuels
Autohydrolysis
Severity Factor
Biorefinery
topic_facet Glucan
Glucose
Biofuels
Autohydrolysis
Severity Factor
Biorefinery
url https://hdl.handle.net/1822/59092
visible 1