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Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications

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Resumo:In this work, the authors propose a new quick sol–gel procedure for bioglass nanoparticles production containing 10% mol of silver (AgBGs). These new AgBGs are characterized by Zeta potential analysis, scanning electron microscopy with X-ray microanalysis (SEM/EDS), X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and microbiological tests to confirm their bioactive and antibacterial properties. SEM shows that the average particle size is less than 200 nm and EDS confirms the successful incorporation of Ag2O in the bioglass matrix. XRD confirms the amorphous nature of the AgBGs and, after SBF immersion, reveals their bioactive behavior with the presence of crystalline phase of calcium silicate and phosphorus oxide, which are also detected by FTIR analysis. FTIR also confirms the formation of typical siloxane bonds resulting from the condensation of silicate glass. Lastly, it is found that the developed AgBGs has an antibacterial effect against two different types of bacteria, thus demonstrating their ability to reduce the bacterial infection within 16 h.
Autores principais:Vale, Ana Catarina
Outros Autores:Carvalho, Ana Luísa; Barbosa, Ana Margarida Martins; Torrado, Egídio; Mano, J. F.; Alves, N. M.
Assunto:Antibacterial properties Biomineralization Silicate glass Silver doped nanoparticles
Ano:2018
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Vale, Ana Catarina
author2 Carvalho, Ana Luísa
Barbosa, Ana Margarida Martins
Torrado, Egídio
Mano, J. F.
Alves, N. M.
author2_role author
author
author
author
author
author_facet Vale, Ana Catarina
Carvalho, Ana Luísa
Barbosa, Ana Margarida Martins
Torrado, Egídio
Mano, J. F.
Alves, N. M.
author_role author
contributor_name_str_mv Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Vale, Ana Catarina\"},{\"Person.name\":\"Carvalho, Ana Luísa\"},{\"Person.name\":\"Barbosa, Ana Margarida Martins\"},{\"Person.name\":\"Torrado, Egídio\"},{\"Person.name\":\"Mano, J. F.\"},{\"Person.name\":\"Alves, N. M.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Vale, Ana Catarina
Carvalho, Ana Luísa
Barbosa, Ana Margarida Martins
Torrado, Egídio
Mano, J. F.
Alves, N. M.
datacite.date.Accepted.fl_str_mv 2018-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2018-02-22T10:08:56Z
datacite.date.embargoed.fl_str_mv 2018-02-22T10:08:56Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Antibacterial properties
Biomineralization
Silicate glass
Silver doped nanoparticles
datacite.titles.title.fl_str_mv Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
dc.contributor.none.fl_str_mv Universidade do Minho
dc.creator.none.fl_str_mv Vale, Ana Catarina
Carvalho, Ana Luísa
Barbosa, Ana Margarida Martins
Torrado, Egídio
Mano, J. F.
Alves, N. M.
dc.date.Accepted.fl_str_mv 2018-01-01T00:00:00Z
dc.date.available.fl_str_mv 2018-02-22T10:08:56Z
dc.date.embargoed.fl_str_mv 2018-02-22T10:08:56Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/50827
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Wiley
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Antibacterial properties
Biomineralization
Silicate glass
Silver doped nanoparticles
dc.title.fl_str_mv Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description In this work, the authors propose a new quick sol–gel procedure for bioglass nanoparticles production containing 10% mol of silver (AgBGs). These new AgBGs are characterized by Zeta potential analysis, scanning electron microscopy with X-ray microanalysis (SEM/EDS), X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and microbiological tests to confirm their bioactive and antibacterial properties. SEM shows that the average particle size is less than 200 nm and EDS confirms the successful incorporation of Ag2O in the bioglass matrix. XRD confirms the amorphous nature of the AgBGs and, after SBF immersion, reveals their bioactive behavior with the presence of crystalline phase of calcium silicate and phosphorus oxide, which are also detected by FTIR analysis. FTIR also confirms the formation of typical siloxane bonds resulting from the condensation of silicate glass. Lastly, it is found that the developed AgBGs has an antibacterial effect against two different types of bacteria, thus demonstrating their ability to reduce the bacterial infection within 16 h.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://prod-dspace.uminho.pt/bitstreams/ae03447c-9b27-4e49-88d2-c6bb1e0c676c/download
id rum_aeafb22b6bca29dfbebfdbea2484ca6e
identifier.url.fl_str_mv https://hdl.handle.net/1822/50827
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/50827
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Vale, Ana Catarina
Carvalho, Ana Luísa
Barbosa, Ana Margarida Martins
Torrado, Egídio
Mano, J. F.
Alves, N. M.
publishDate 2018
publisher.none.fl_str_mv Wiley
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engWileyporIn this work, the authors propose a new quick sol–gel procedure for bioglass nanoparticles production containing 10% mol of silver (AgBGs). These new AgBGs are characterized by Zeta potential analysis, scanning electron microscopy with X-ray microanalysis (SEM/EDS), X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and microbiological tests to confirm their bioactive and antibacterial properties. SEM shows that the average particle size is less than 200 nm and EDS confirms the successful incorporation of Ag2O in the bioglass matrix. XRD confirms the amorphous nature of the AgBGs and, after SBF immersion, reveals their bioactive behavior with the presence of crystalline phase of calcium silicate and phosphorus oxide, which are also detected by FTIR analysis. FTIR also confirms the formation of typical siloxane bonds resulting from the condensation of silicate glass. Lastly, it is found that the developed AgBGs has an antibacterial effect against two different types of bacteria, thus demonstrating their ability to reduce the bacterial infection within 16 h.application/pdfporNovel antibacterial and bioactive silicate glass nanoparticles for biomedical applicationsVale, Ana CatarinaCarvalho, Ana LuísaBarbosa, Ana Margarida MartinsTorrado, EgídioMano, J. F.Alves, N. M.HostingInstitutionOrganizationalUniversidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptISSNIsPartOf1438-1656DOIIsPartOf10.1002/adem.2017008552018-02-22T10:08:56Z20182018-01-25T10:23:41Z2018-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/50827http://purl.org/coar/access_right/c_abf2open accessAntibacterial propertiesBiomineralizationSilicate glassSilver doped nanoparticles628660 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://prod-dspace.uminho.pt/bitstreams/ae03447c-9b27-4e49-88d2-c6bb1e0c676c/download
spellingShingle Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
Vale, Ana Catarina
Antibacterial properties
Biomineralization
Silicate glass
Silver doped nanoparticles
status SINGLETON
subject.fl_str_mv Antibacterial properties
Biomineralization
Silicate glass
Silver doped nanoparticles
title Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
title_full Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
title_fullStr Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
title_full_unstemmed Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
title_short Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
title_sort Novel antibacterial and bioactive silicate glass nanoparticles for biomedical applications
topic Antibacterial properties
Biomineralization
Silicate glass
Silver doped nanoparticles
topic_facet Antibacterial properties
Biomineralization
Silicate glass
Silver doped nanoparticles
url https://hdl.handle.net/1822/50827
visible 1