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Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry

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Resumo:In recent years, significant attention has been given to “green” product innovation and related manufacturing processes. This work reports the preparation of few-layer graphene (FLG) and respective PLA-based composites by an ecofriendly, efficient, and cost-effective approach. FLG was produced in a scaledup process, based on the noncovalent functionalization of a micronized graphite with a pyrene derivate (PY), in aqueous solution. The exfoliation degree, morphology, and thermal stability of the exfoliated material were evaluated. Then, the influence of the pristine graphite and FLG on the morphology, crystallinity, thermal and mechanical properties of PLA composites produced by melt mixing is reported for the first time. The composites prepared with the lowest loading of 0.05 wt% demonstrated suitability for further processing for potential applications where product safety is crucial, such as in biomedicine.
Autores principais:Peixoto, Tânia
Outros Autores:Nunes, Joana; Lopes, Maria A.; Marinho, Elina Margarida Ribeiro; Proença, M. Fernanda R. P.; Lopes, Paulo Estevão Caldeira; Paiva, Maria C.
Assunto:Composites Eco-friendly Few-layer graphene Graphite Melt mixing PLA
Ano:2022
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Peixoto, Tânia
author2 Nunes, Joana
Lopes, Maria A.
Marinho, Elina Margarida Ribeiro
Proença, M. Fernanda R. P.
Lopes, Paulo Estevão Caldeira
Paiva, Maria C.
author2_role author
author
author
author
author
author
author_facet Peixoto, Tânia
Nunes, Joana
Lopes, Maria A.
Marinho, Elina Margarida Ribeiro
Proença, M. Fernanda R. P.
Lopes, Paulo Estevão Caldeira
Paiva, Maria C.
author_role author
contributor_name_str_mv Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Peixoto, Tânia\"},{\"Person.name\":\"Nunes, Joana\"},{\"Person.name\":\"Lopes, Maria A.\"},{\"Person.name\":\"Marinho, Elina Margarida Ribeiro\"},{\"Person.name\":\"Proença, M. Fernanda R. P.\"},{\"Person.name\":\"Lopes, Paulo Estevão Caldeira\"},{\"Person.name\":\"Paiva, Maria C.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Peixoto, Tânia
Nunes, Joana
Lopes, Maria A.
Marinho, Elina Margarida Ribeiro
Proença, M. Fernanda R. P.
Lopes, Paulo Estevão Caldeira
Paiva, Maria C.
datacite.date.Accepted.fl_str_mv 2022-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2024-01-04T11:30:10Z
datacite.date.embargoed.fl_str_mv 2024-01-04T11:30:10Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Composites
Eco-friendly
Few-layer graphene
Graphite
Melt mixing
PLA
datacite.titles.title.fl_str_mv Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
dc.contributor.none.fl_str_mv Universidade do Minho
dc.creator.none.fl_str_mv Peixoto, Tânia
Nunes, Joana
Lopes, Maria A.
Marinho, Elina Margarida Ribeiro
Proença, M. Fernanda R. P.
Lopes, Paulo Estevão Caldeira
Paiva, Maria C.
dc.date.Accepted.fl_str_mv 2022-01-01T00:00:00Z
dc.date.available.fl_str_mv 2024-01-04T11:30:10Z
dc.date.embargoed.fl_str_mv 2024-01-04T11:30:10Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/87915
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Wiley
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Composites
Eco-friendly
Few-layer graphene
Graphite
Melt mixing
PLA
dc.title.fl_str_mv Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description In recent years, significant attention has been given to “green” product innovation and related manufacturing processes. This work reports the preparation of few-layer graphene (FLG) and respective PLA-based composites by an ecofriendly, efficient, and cost-effective approach. FLG was produced in a scaledup process, based on the noncovalent functionalization of a micronized graphite with a pyrene derivate (PY), in aqueous solution. The exfoliation degree, morphology, and thermal stability of the exfoliated material were evaluated. Then, the influence of the pristine graphite and FLG on the morphology, crystallinity, thermal and mechanical properties of PLA composites produced by melt mixing is reported for the first time. The composites prepared with the lowest loading of 0.05 wt% demonstrated suitability for further processing for potential applications where product safety is crucial, such as in biomedicine.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://prod-dspace.uminho.pt/bitstreams/0b006466-c4ed-43e0-bb02-3b88f442005f/download
id rum_b2dd75f8564cd0d84205e3251ab494d6
identifier.url.fl_str_mv https://hdl.handle.net/1822/87915
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/87915
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Peixoto, Tânia
Nunes, Joana
Lopes, Maria A.
Marinho, Elina Margarida Ribeiro
Proença, M. Fernanda R. P.
Lopes, Paulo Estevão Caldeira
Paiva, Maria C.
publishDate 2022
publisher.none.fl_str_mv Wiley
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engWileyporIn recent years, significant attention has been given to “green” product innovation and related manufacturing processes. This work reports the preparation of few-layer graphene (FLG) and respective PLA-based composites by an ecofriendly, efficient, and cost-effective approach. FLG was produced in a scaledup process, based on the noncovalent functionalization of a micronized graphite with a pyrene derivate (PY), in aqueous solution. The exfoliation degree, morphology, and thermal stability of the exfoliated material were evaluated. Then, the influence of the pristine graphite and FLG on the morphology, crystallinity, thermal and mechanical properties of PLA composites produced by melt mixing is reported for the first time. The composites prepared with the lowest loading of 0.05 wt% demonstrated suitability for further processing for potential applications where product safety is crucial, such as in biomedicine.application/pdfporPoly(lactic acid) composites with few layer graphene produced by noncovalent chemistryPeixoto, TâniaNunes, JoanaLopes, Maria A.Marinho, Elina Margarida RibeiroProença, M. Fernanda R. P.Lopes, Paulo Estevão CaldeiraPaiva, Maria C.HostingInstitutionOrganizationalUniversidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptISSNIsPartOf0272-8397DOIIsPartOf10.1002/pc.270122024-01-04T11:30:10Z20222022-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/87915http://purl.org/coar/access_right/c_abf2open accessCompositesEco-friendlyFew-layer grapheneGraphiteMelt mixingPLA7199223 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://prod-dspace.uminho.pt/bitstreams/0b006466-c4ed-43e0-bb02-3b88f442005f/download
spellingShingle Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
Peixoto, Tânia
Composites
Eco-friendly
Few-layer graphene
Graphite
Melt mixing
PLA
status SINGLETON
subject.fl_str_mv Composites
Eco-friendly
Few-layer graphene
Graphite
Melt mixing
PLA
title Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
title_full Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
title_fullStr Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
title_full_unstemmed Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
title_short Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
title_sort Poly(lactic acid) composites with few layer graphene produced by noncovalent chemistry
topic Composites
Eco-friendly
Few-layer graphene
Graphite
Melt mixing
PLA
topic_facet Composites
Eco-friendly
Few-layer graphene
Graphite
Melt mixing
PLA
url https://hdl.handle.net/1822/87915
visible 1