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Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications

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Summary:Different rare-earth elements (Dy, Gd, Tb and Yb) doped LiMn 2 O 4 spinel active material were prepared by sol-gel method. The rare earth doping elements decrease particle size but do not affect the formation of cubic spinel structure. Further, these dopants have strong influence in the overall electrical properties of the cathodes prepared from them. In the cyclic voltammetry measurements, two pairs of separated redox peaks are observed, independently to dopants. LiMn 2 O 4 doped gadolinium (Gd) and dysprosium (Dy) exhibit a comparable room temperature rate capability to pristine LiMn 2 O 4 with discharge capacity of 94.5 mAh g -1 and 82.3 mAh g -1 , respectively, versus 73.4 mAh g -1 for pristine LiMn 2 O 4 at a rate of C5. Terbium (Tb) and ytterbium (Yb) doping show, on the other hand, lower performance. After 50 cycles at C2, the capacity fade is 7% for LiMn 1.95 Dy 0.05 O 4 and 14% for LiMn 1.95 Gd 0.05 O 4 , whereas for LiMn 2 O 4 it is 32%. The improved cycling performance of LiMn 2 O 4 doped with Gd and Dy is attributed to the powder size and atomic radius of the elements. Differences of the capacity retention on cycling are attributed to superior structural stability due to rare earth doping. These results indicate that improved cathode materials doped with rare earth element are suitable for lithium-ion battery applications
Main Authors:Ram, Pura
Other Authors:Gören, Attila; Ferdov, S.; Silva, Maria Manuela; Singhal, Rahul; Costa, C. M.; Sharma, Rakesh K.; Lanceros-Méndez, S.
Subject:Ciências Naturais::Ciências Físicas
Year:2016
Country:Portugal
Document type:article
Access type:restricted access
Associated institution:Universidade do Minho
Language:English
Origin:RepositóriUM - Universidade do Minho
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author Ram, Pura
author2 Gören, Attila
Ferdov, S.
Silva, Maria Manuela
Singhal, Rahul
Costa, C. M.
Sharma, Rakesh K.
Lanceros-Méndez, S.
author2_role author
author
author
author
author
author
author
author_facet Ram, Pura
Gören, Attila
Ferdov, S.
Silva, Maria Manuela
Singhal, Rahul
Costa, C. M.
Sharma, Rakesh K.
Lanceros-Méndez, S.
author_role author
contributor_name_str_mv RepositóriUM - Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Ram, Pura\"},{\"Person.name\":\"Gören, Attila\"},{\"Person.name\":\"Ferdov, S.\"},{\"Person.name\":\"Silva, Maria Manuela\"},{\"Person.name\":\"Singhal, Rahul\"},{\"Person.name\":\"Costa, C. M.\"},{\"Person.name\":\"Sharma, Rakesh K.\"},{\"Person.name\":\"Lanceros-Méndez, S.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv RepositóriUM - Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Ram, Pura
Gören, Attila
Ferdov, S.
Silva, Maria Manuela
Singhal, Rahul
Costa, C. M.
Sharma, Rakesh K.
Lanceros-Méndez, S.
datacite.date.Accepted.fl_str_mv 2016-01-01T00:00:00Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_16ec
datacite.subjects.subject.fl_str_mv Ciências Naturais::Ciências Físicas
datacite.titles.title.fl_str_mv Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
dc.contributor.none.fl_str_mv RepositóriUM - Universidade do Minho
dc.creator.none.fl_str_mv Ram, Pura
Gören, Attila
Ferdov, S.
Silva, Maria Manuela
Singhal, Rahul
Costa, C. M.
Sharma, Rakesh K.
Lanceros-Méndez, S.
dc.date.Accepted.fl_str_mv 2016-01-01T00:00:00Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/43522
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Royal Society of Chemistry
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_16ec
dc.subject.none.fl_str_mv Ciências Naturais::Ciências Físicas
dc.title.fl_str_mv Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description Different rare-earth elements (Dy, Gd, Tb and Yb) doped LiMn 2 O 4 spinel active material were prepared by sol-gel method. The rare earth doping elements decrease particle size but do not affect the formation of cubic spinel structure. Further, these dopants have strong influence in the overall electrical properties of the cathodes prepared from them. In the cyclic voltammetry measurements, two pairs of separated redox peaks are observed, independently to dopants. LiMn 2 O 4 doped gadolinium (Gd) and dysprosium (Dy) exhibit a comparable room temperature rate capability to pristine LiMn 2 O 4 with discharge capacity of 94.5 mAh g -1 and 82.3 mAh g -1 , respectively, versus 73.4 mAh g -1 for pristine LiMn 2 O 4 at a rate of C5. Terbium (Tb) and ytterbium (Yb) doping show, on the other hand, lower performance. After 50 cycles at C2, the capacity fade is 7% for LiMn 1.95 Dy 0.05 O 4 and 14% for LiMn 1.95 Gd 0.05 O 4 , whereas for LiMn 2 O 4 it is 32%. The improved cycling performance of LiMn 2 O 4 doped with Gd and Dy is attributed to the powder size and atomic radius of the elements. Differences of the capacity retention on cycling are attributed to superior structural stability due to rare earth doping. These results indicate that improved cathode materials doped with rare earth element are suitable for lithium-ion battery applications
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id rum_baae2c80d293d4e7dbb4ff17eb95fd01
identifier.url.fl_str_mv https://hdl.handle.net/1822/43522
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/43522
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Ram, Pura
Gören, Attila
Ferdov, S.
Silva, Maria Manuela
Singhal, Rahul
Costa, C. M.
Sharma, Rakesh K.
Lanceros-Méndez, S.
publishDate 2016
publisher.none.fl_str_mv Royal Society of Chemistry
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engRoyal Society of ChemistryporDifferent rare-earth elements (Dy, Gd, Tb and Yb) doped LiMn 2 O 4 spinel active material were prepared by sol-gel method. The rare earth doping elements decrease particle size but do not affect the formation of cubic spinel structure. Further, these dopants have strong influence in the overall electrical properties of the cathodes prepared from them. In the cyclic voltammetry measurements, two pairs of separated redox peaks are observed, independently to dopants. LiMn 2 O 4 doped gadolinium (Gd) and dysprosium (Dy) exhibit a comparable room temperature rate capability to pristine LiMn 2 O 4 with discharge capacity of 94.5 mAh g -1 and 82.3 mAh g -1 , respectively, versus 73.4 mAh g -1 for pristine LiMn 2 O 4 at a rate of C5. Terbium (Tb) and ytterbium (Yb) doping show, on the other hand, lower performance. After 50 cycles at C2, the capacity fade is 7% for LiMn 1.95 Dy 0.05 O 4 and 14% for LiMn 1.95 Gd 0.05 O 4 , whereas for LiMn 2 O 4 it is 32%. The improved cycling performance of LiMn 2 O 4 doped with Gd and Dy is attributed to the powder size and atomic radius of the elements. Differences of the capacity retention on cycling are attributed to superior structural stability due to rare earth doping. These results indicate that improved cathode materials doped with rare earth element are suitable for lithium-ion battery applicationsapplication/pdfporImproved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applicationsRam, PuraGören, AttilaFerdov, S.Silva, Maria ManuelaSinghal, RahulCosta, C. M.Sharma, Rakesh K.Lanceros-Méndez, S.HostingInstitutionOrganizationalRepositóriUM - Universidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptCITATIONRam, P., Goren, A., Ferdov, S., Silva, M. M., Singhal, R., Costa, C. M., . . . Lanceros-Mendez, S. (2016). Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications. New Journal of Chemistry, 40(7), 6244-6252. doi: 10.1039/c6nj00198jISSNIsPartOf1144-0546DOIIsPartOf10.1039/c6nj00198j20162016-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/43522http://purl.org/coar/access_right/c_16ecrestricted accesshttp://www.oecd.org/science/inno/38235147.pdfFields of Science and Technology (FOS)Ciências Naturais::Ciências Físicas1107809 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_16ecapplication/pdffulltexthttps://repositorium.uminho.pt/bitstreams/d48cc830-a2f6-44d3-8b44-bff78bc87bb6/download
spellingShingle Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
Ram, Pura
Ciências Naturais::Ciências Físicas
status SINGLETON
subject.other.fl_str_mv Ciências Naturais::Ciências Físicas
title Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
title_full Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
title_fullStr Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
title_full_unstemmed Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
title_short Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
title_sort Improved performance of rare earth doped LiMn2O4 cathodes for lithium-ion battery applications
topic Ciências Naturais::Ciências Físicas
topic_facet Ciências Naturais::Ciências Físicas
url https://hdl.handle.net/1822/43522
visible 1