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Cellulose nanowhisker obtained from cotton rejected by textile industry

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Resumo:This study aimed to characterize cellulose nanowhiskers (NWs) extracted from discarded cotton fibers. The nanocellulose was characterized by dynamic light scattering, zeta potential, Scanning Transmission Electron Microscopy (STEM), Atomic force microscopy (AFM) and X-ray powder diffraction (XRD). The nanocrystals are characterized by a rod-like morphology with sizes between 100 nm and 300 nm. The acidic hydrolyses applied to the extract nanocrystals increased the crystallinity index from 72 to 86%. The average length and diameter obtained were 98.1±4.7 and 8.0±3.4 nm, respectively. The aspect ratio of the fibers, around 12.3, was lower than the values usually reported in the literature. The dynamic light scattering results were in accordance with the nano crystal dimensions showing an average size of 235 nm. Cellulose NWs obtained from cotton rejected by textile industry due to their abundance, low cost, high crystallinity, strength, low weight and biodegradability, are the ideal candidates for the processing of polymer nanocomposites.
Autores principais:Nascimento, José Heriberto Oliveira do
Outros Autores:Luz, Rodrigo F.; Galvão, Felipe M. F.; Melo, José Daniel D.; Oliveira, Fernando R.; Ladchumananandasivam, Rasiah; Zille, Andrea
Assunto:Cellulose nanowhisker cotton textile Hydrolisys Engenharia e Tecnologia::Engenharia dos Materiais
Ano:2015
País:Portugal
Tipo de documento:outro
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Nascimento, José Heriberto Oliveira do
author2 Luz, Rodrigo F.
Galvão, Felipe M. F.
Melo, José Daniel D.
Oliveira, Fernando R.
Ladchumananandasivam, Rasiah
Zille, Andrea
author2_role author
author
author
author
author
author
author_facet Nascimento, José Heriberto Oliveira do
Luz, Rodrigo F.
Galvão, Felipe M. F.
Melo, José Daniel D.
Oliveira, Fernando R.
Ladchumananandasivam, Rasiah
Zille, Andrea
author_role author
contributor_name_str_mv RepositóriUM - Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Nascimento, José Heriberto Oliveira do\"},{\"Person.name\":\"Luz, Rodrigo F.\"},{\"Person.name\":\"Galvão, Felipe M. F.\"},{\"Person.name\":\"Melo, José Daniel D.\"},{\"Person.name\":\"Oliveira, Fernando R.\"},{\"Person.name\":\"Ladchumananandasivam, Rasiah\"},{\"Person.name\":\"Zille, Andrea\"}]
datacite.contributors.contributor.contributorName.fl_str_mv RepositóriUM - Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Nascimento, José Heriberto Oliveira do
Luz, Rodrigo F.
Galvão, Felipe M. F.
Melo, José Daniel D.
Oliveira, Fernando R.
Ladchumananandasivam, Rasiah
Zille, Andrea
datacite.date.Accepted.fl_str_mv 2015-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2015-05-26T15:03:16Z
datacite.date.embargoed.fl_str_mv 2015-05-26T15:03:16Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Cellulose nanowhisker
cotton
textile
Hydrolisys
Engenharia e Tecnologia::Engenharia dos Materiais
datacite.titles.title.fl_str_mv Cellulose nanowhisker obtained from cotton rejected by textile industry
dc.contributor.none.fl_str_mv RepositóriUM - Universidade do Minho
dc.creator.none.fl_str_mv Nascimento, José Heriberto Oliveira do
Luz, Rodrigo F.
Galvão, Felipe M. F.
Melo, José Daniel D.
Oliveira, Fernando R.
Ladchumananandasivam, Rasiah
Zille, Andrea
dc.date.Accepted.fl_str_mv 2015-01-01T00:00:00Z
dc.date.available.fl_str_mv 2015-05-26T15:03:16Z
dc.date.embargoed.fl_str_mv 2015-05-26T15:03:16Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/35285
dc.language.none.fl_str_mv eng
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Cellulose nanowhisker
cotton
textile
Hydrolisys
Engenharia e Tecnologia::Engenharia dos Materiais
dc.title.fl_str_mv Cellulose nanowhisker obtained from cotton rejected by textile industry
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_1843
description This study aimed to characterize cellulose nanowhiskers (NWs) extracted from discarded cotton fibers. The nanocellulose was characterized by dynamic light scattering, zeta potential, Scanning Transmission Electron Microscopy (STEM), Atomic force microscopy (AFM) and X-ray powder diffraction (XRD). The nanocrystals are characterized by a rod-like morphology with sizes between 100 nm and 300 nm. The acidic hydrolyses applied to the extract nanocrystals increased the crystallinity index from 72 to 86%. The average length and diameter obtained were 98.1±4.7 and 8.0±3.4 nm, respectively. The aspect ratio of the fibers, around 12.3, was lower than the values usually reported in the literature. The dynamic light scattering results were in accordance with the nano crystal dimensions showing an average size of 235 nm. Cellulose NWs obtained from cotton rejected by textile industry due to their abundance, low cost, high crystallinity, strength, low weight and biodegradability, are the ideal candidates for the processing of polymer nanocomposites.
dirty 0
eu_rights_str_mv openAccess
format other
fulltext.url.fl_str_mv https://repositorium.uminho.pt/bitstreams/3793e41b-1370-4ee7-baf6-abd8305316b6/download
id rum_bbeebf2a565cd7a67c875319f602a9b3
identifier.url.fl_str_mv https://hdl.handle.net/1822/35285
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/35285
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Nascimento, José Heriberto Oliveira do
Luz, Rodrigo F.
Galvão, Felipe M. F.
Melo, José Daniel D.
Oliveira, Fernando R.
Ladchumananandasivam, Rasiah
Zille, Andrea
publishDate 2015
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engporThis study aimed to characterize cellulose nanowhiskers (NWs) extracted from discarded cotton fibers. The nanocellulose was characterized by dynamic light scattering, zeta potential, Scanning Transmission Electron Microscopy (STEM), Atomic force microscopy (AFM) and X-ray powder diffraction (XRD). The nanocrystals are characterized by a rod-like morphology with sizes between 100 nm and 300 nm. The acidic hydrolyses applied to the extract nanocrystals increased the crystallinity index from 72 to 86%. The average length and diameter obtained were 98.1±4.7 and 8.0±3.4 nm, respectively. The aspect ratio of the fibers, around 12.3, was lower than the values usually reported in the literature. The dynamic light scattering results were in accordance with the nano crystal dimensions showing an average size of 235 nm. Cellulose NWs obtained from cotton rejected by textile industry due to their abundance, low cost, high crystallinity, strength, low weight and biodegradability, are the ideal candidates for the processing of polymer nanocomposites.application/pdfporCellulose nanowhisker obtained from cotton rejected by textile industryNascimento, José Heriberto Oliveira doLuz, Rodrigo F.Galvão, Felipe M. F.Melo, José Daniel D.Oliveira, Fernando R.Ladchumananandasivam, RasiahZille, AndreaHostingInstitutionOrganizationalRepositóriUM - Universidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptDOIIsPartOf10.13140/RG.2.1.1609.87242015-05-26T15:03:16Z20152015-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/35285http://purl.org/coar/access_right/c_abf2open accessCellulose nanowhiskercottontextileHydrolisyshttp://www.oecd.org/science/inno/38235147.pdfFields of Science and Technology (FOS)Engenharia e Tecnologia::Engenharia dos Materiais1764072 bytesother research producthttp://purl.org/coar/resource_type/c_1843otherhttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://repositorium.uminho.pt/bitstreams/3793e41b-1370-4ee7-baf6-abd8305316b6/download
spellingShingle Cellulose nanowhisker obtained from cotton rejected by textile industry
Nascimento, José Heriberto Oliveira do
Cellulose nanowhisker
cotton
textile
Hydrolisys
Engenharia e Tecnologia::Engenharia dos Materiais
status SINGLETON
subject.fl_str_mv Cellulose nanowhisker
cotton
textile
Hydrolisys
subject.other.fl_str_mv Engenharia e Tecnologia::Engenharia dos Materiais
title Cellulose nanowhisker obtained from cotton rejected by textile industry
title_full Cellulose nanowhisker obtained from cotton rejected by textile industry
title_fullStr Cellulose nanowhisker obtained from cotton rejected by textile industry
title_full_unstemmed Cellulose nanowhisker obtained from cotton rejected by textile industry
title_short Cellulose nanowhisker obtained from cotton rejected by textile industry
title_sort Cellulose nanowhisker obtained from cotton rejected by textile industry
topic Cellulose nanowhisker
cotton
textile
Hydrolisys
Engenharia e Tecnologia::Engenharia dos Materiais
topic_facet Cellulose nanowhisker
cotton
textile
Hydrolisys
Engenharia e Tecnologia::Engenharia dos Materiais
url https://hdl.handle.net/1822/35285
visible 1