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Biocompatibility of poly(lactic acid) with incorporated graphene-based materials

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Resumo:The incorporation of graphene-based materials has been shown to improve mechanical properties of poly(lactic acid) (PLA). In this work, PLA films and composite PLA films incorporating two graphene-based materials – graphene oxide (GO) and graphene nanoplatelets (GNP) – were prepared and characterized regarding not only biocompatibility, but also surface topography, chemistry and wettability. The presence of both fillers changed the films surface topography, increasing the roughness, and modified the wettability – the polar component of surface free energy increased 59% with GO and decreased 56% with GNP. Mouse embryo fibroblasts incubated with both fillers exceeded the IC50 in both cases with a concentration of 10 μg mL−1. No variations in cell proliferation at the surface of the composite films were observed, except for those containing GO after 24 h incubation, which presented higher cell proliferation than pristine PLA films. Platelet adhesion to PLA and PLA/GNP films was lower in the presence of plasma proteins than when no proteins were present. Furthermore, incorporation of GNP into PLA reduced platelet activation in the presence of plasma proteins. The results indicated that low concentrations of GO and GNP may be incorporated safely in PLA to improve aspects relevant for biomedical applications, such as mechanical properties.
Autores principais:Pinto, Artur Moreira
Outros Autores:Moreira, Susana Margarida Gomes; Gonçalves, Inês; Gama, F. M.; Mendes, Adélio; Magalhães, Fernão D.
Assunto:Topography Wettability Cytotoxicity Platelets Hemocompatibility
Ano:2013
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Pinto, Artur Moreira
author2 Moreira, Susana Margarida Gomes
Gonçalves, Inês
Gama, F. M.
Mendes, Adélio
Magalhães, Fernão D.
author2_role author
author
author
author
author
author_facet Pinto, Artur Moreira
Moreira, Susana Margarida Gomes
Gonçalves, Inês
Gama, F. M.
Mendes, Adélio
Magalhães, Fernão D.
author_role author
contributor_name_str_mv RepositóriUM - Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Pinto, Artur Moreira\"},{\"Person.name\":\"Moreira, Susana Margarida Gomes\"},{\"Person.name\":\"Gonçalves, Inês\"},{\"Person.name\":\"Gama, F. M.\"},{\"Person.name\":\"Mendes, Adélio\"},{\"Person.name\":\"Magalhães, Fernão D.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv RepositóriUM - Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Pinto, Artur Moreira
Moreira, Susana Margarida Gomes
Gonçalves, Inês
Gama, F. M.
Mendes, Adélio
Magalhães, Fernão D.
datacite.date.Accepted.fl_str_mv 2013-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2013-06-05T14:13:32Z
datacite.date.embargoed.fl_str_mv 2013-06-05T14:13:32Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Topography
Wettability
Cytotoxicity
Platelets
Hemocompatibility
datacite.titles.title.fl_str_mv Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
dc.contributor.none.fl_str_mv RepositóriUM - Universidade do Minho
dc.creator.none.fl_str_mv Pinto, Artur Moreira
Moreira, Susana Margarida Gomes
Gonçalves, Inês
Gama, F. M.
Mendes, Adélio
Magalhães, Fernão D.
dc.date.Accepted.fl_str_mv 2013-01-01T00:00:00Z
dc.date.available.fl_str_mv 2013-06-05T14:13:32Z
dc.date.embargoed.fl_str_mv 2013-06-05T14:13:32Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/24335
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Elsevier
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Topography
Wettability
Cytotoxicity
Platelets
Hemocompatibility
dc.title.fl_str_mv Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description The incorporation of graphene-based materials has been shown to improve mechanical properties of poly(lactic acid) (PLA). In this work, PLA films and composite PLA films incorporating two graphene-based materials – graphene oxide (GO) and graphene nanoplatelets (GNP) – were prepared and characterized regarding not only biocompatibility, but also surface topography, chemistry and wettability. The presence of both fillers changed the films surface topography, increasing the roughness, and modified the wettability – the polar component of surface free energy increased 59% with GO and decreased 56% with GNP. Mouse embryo fibroblasts incubated with both fillers exceeded the IC50 in both cases with a concentration of 10 μg mL−1. No variations in cell proliferation at the surface of the composite films were observed, except for those containing GO after 24 h incubation, which presented higher cell proliferation than pristine PLA films. Platelet adhesion to PLA and PLA/GNP films was lower in the presence of plasma proteins than when no proteins were present. Furthermore, incorporation of GNP into PLA reduced platelet activation in the presence of plasma proteins. The results indicated that low concentrations of GO and GNP may be incorporated safely in PLA to improve aspects relevant for biomedical applications, such as mechanical properties.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://repositorium.uminho.pt/bitstreams/f2ab7d94-e072-4455-976c-ca739e077e3b/download
id rum_bd1c8e2d2cc7abb151bc279c68c5fdb2
identifier.url.fl_str_mv https://hdl.handle.net/1822/24335
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/24335
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Pinto, Artur Moreira
Moreira, Susana Margarida Gomes
Gonçalves, Inês
Gama, F. M.
Mendes, Adélio
Magalhães, Fernão D.
publishDate 2013
publisher.none.fl_str_mv Elsevier
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engElsevierporThe incorporation of graphene-based materials has been shown to improve mechanical properties of poly(lactic acid) (PLA). In this work, PLA films and composite PLA films incorporating two graphene-based materials – graphene oxide (GO) and graphene nanoplatelets (GNP) – were prepared and characterized regarding not only biocompatibility, but also surface topography, chemistry and wettability. The presence of both fillers changed the films surface topography, increasing the roughness, and modified the wettability – the polar component of surface free energy increased 59% with GO and decreased 56% with GNP. Mouse embryo fibroblasts incubated with both fillers exceeded the IC50 in both cases with a concentration of 10 μg mL−1. No variations in cell proliferation at the surface of the composite films were observed, except for those containing GO after 24 h incubation, which presented higher cell proliferation than pristine PLA films. Platelet adhesion to PLA and PLA/GNP films was lower in the presence of plasma proteins than when no proteins were present. Furthermore, incorporation of GNP into PLA reduced platelet activation in the presence of plasma proteins. The results indicated that low concentrations of GO and GNP may be incorporated safely in PLA to improve aspects relevant for biomedical applications, such as mechanical properties.application/pdfporBiocompatibility of poly(lactic acid) with incorporated graphene-based materialsPinto, Artur MoreiraMoreira, Susana Margarida GomesGonçalves, InêsGama, F. M.Mendes, AdélioMagalhães, Fernão D.HostingInstitutionOrganizationalRepositóriUM - Universidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptPMID23333912ISSNIsPartOf0927-7765DOIIsPartOf10.1016/j.colsurfb.2012.12.0062013-06-05T14:13:32Z20132013-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/24335http://purl.org/coar/access_right/c_abf2open accessTopographyWettabilityCytotoxicityPlateletsHemocompatibility1853463 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://repositorium.uminho.pt/bitstreams/f2ab7d94-e072-4455-976c-ca739e077e3b/download
spellingShingle Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
Pinto, Artur Moreira
Topography
Wettability
Cytotoxicity
Platelets
Hemocompatibility
status SINGLETON
subject.fl_str_mv Topography
Wettability
Cytotoxicity
Platelets
Hemocompatibility
title Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
title_full Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
title_fullStr Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
title_full_unstemmed Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
title_short Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
title_sort Biocompatibility of poly(lactic acid) with incorporated graphene-based materials
topic Topography
Wettability
Cytotoxicity
Platelets
Hemocompatibility
topic_facet Topography
Wettability
Cytotoxicity
Platelets
Hemocompatibility
url https://hdl.handle.net/1822/24335
visible 1