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Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones

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Resumo:In order to evaluate the application of quinolone as a new photocleavable protecting group, in comparison with coumarin, a series of model phenylalanine conjugates were prepared by reaction with chloromethylated O and N heterocycles. The photophysical properties of the resulting ester conjugates were evaluated as well as the photosensitivity under irradiation at 250, 300, 350, and 419 nm. The results obtained showed that the quinolone conjugates were readily photolysed, with complete release of the amino acid in short irradiation times and could be considered a new addition to the family of photocleavable protecting groups for the carboxylic acid function of amino acids.
Autores principais:Fonseca, Andrea S. C.
Outros Autores:Gonçalves, M. Sameiro T.; Costa, Susana P. G.
Assunto:Coumarin Quinolone Bioconjugates Amino acids Photocleavable protecting groups
Ano:2010
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Fonseca, Andrea S. C.
author2 Gonçalves, M. Sameiro T.
Costa, Susana P. G.
author2_role author
author
author_facet Fonseca, Andrea S. C.
Gonçalves, M. Sameiro T.
Costa, Susana P. G.
author_role author
contributor_name_str_mv Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Fonseca, Andrea S. C.\"},{\"Person.name\":\"Gonçalves, M. Sameiro T.\"},{\"Person.name\":\"Costa, Susana P. G.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Fonseca, Andrea S. C.
Gonçalves, M. Sameiro T.
Costa, Susana P. G.
datacite.date.Accepted.fl_str_mv 2010-08-01T00:00:00Z
datacite.date.embargoed.fl_str_mv 10000-01-01T00:00:00Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Coumarin
Quinolone
Bioconjugates
Amino acids
Photocleavable protecting groups
datacite.titles.title.fl_str_mv Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
dc.contributor.none.fl_str_mv Universidade do Minho
dc.creator.none.fl_str_mv Fonseca, Andrea S. C.
Gonçalves, M. Sameiro T.
Costa, Susana P. G.
dc.date.Accepted.fl_str_mv 2010-08-01T00:00:00Z
dc.date.embargoed.fl_str_mv 10000-01-01T00:00:00Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/86437
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Springer
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Coumarin
Quinolone
Bioconjugates
Amino acids
Photocleavable protecting groups
dc.title.fl_str_mv Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description In order to evaluate the application of quinolone as a new photocleavable protecting group, in comparison with coumarin, a series of model phenylalanine conjugates were prepared by reaction with chloromethylated O and N heterocycles. The photophysical properties of the resulting ester conjugates were evaluated as well as the photosensitivity under irradiation at 250, 300, 350, and 419 nm. The results obtained showed that the quinolone conjugates were readily photolysed, with complete release of the amino acid in short irradiation times and could be considered a new addition to the family of photocleavable protecting groups for the carboxylic acid function of amino acids.
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eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://prod-dspace.uminho.pt/bitstreams/588f89a8-9830-4e26-ab04-9ba52c564de3/download
id rum_c746ef3f2ea4bcdbeac387b2e56ced9a
identifier.url.fl_str_mv https://hdl.handle.net/1822/86437
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/86437
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Fonseca, Andrea S. C.
Gonçalves, M. Sameiro T.
Costa, Susana P. G.
publishDate 2010
publisher.none.fl_str_mv Springer
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engSpringerporIn order to evaluate the application of quinolone as a new photocleavable protecting group, in comparison with coumarin, a series of model phenylalanine conjugates were prepared by reaction with chloromethylated O and N heterocycles. The photophysical properties of the resulting ester conjugates were evaluated as well as the photosensitivity under irradiation at 250, 300, 350, and 419 nm. The results obtained showed that the quinolone conjugates were readily photolysed, with complete release of the amino acid in short irradiation times and could be considered a new addition to the family of photocleavable protecting groups for the carboxylic acid function of amino acids.application/pdfengLight-induced cleavage of model phenylalanine conjugates based on coumarins and quinolonesFonseca, Andrea S. C.Gonçalves, M. Sameiro T.Costa, Susana P. G.HostingInstitutionOrganizationalUniversidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptISSNIsPartOf0939-4451DOIIsPartOf10.1007/s00726-010-0492-82010-082023-09-03T09:08:40Z2010-08-01T00:00:00Z10000-01-01T00:00:00ZHandlehttps://hdl.handle.net/1822/86437http://purl.org/coar/access_right/c_abf2open accessCoumarinQuinoloneBioconjugatesAmino acidsPhotocleavable protecting groups553386 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://prod-dspace.uminho.pt/bitstreams/588f89a8-9830-4e26-ab04-9ba52c564de3/download
spellingShingle Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
Fonseca, Andrea S. C.
Coumarin
Quinolone
Bioconjugates
Amino acids
Photocleavable protecting groups
status SINGLETON
subject.fl_str_mv Coumarin
Quinolone
Bioconjugates
Amino acids
Photocleavable protecting groups
title Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
title_full Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
title_fullStr Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
title_full_unstemmed Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
title_short Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
title_sort Light-induced cleavage of model phenylalanine conjugates based on coumarins and quinolones
topic Coumarin
Quinolone
Bioconjugates
Amino acids
Photocleavable protecting groups
topic_facet Coumarin
Quinolone
Bioconjugates
Amino acids
Photocleavable protecting groups
url https://hdl.handle.net/1822/86437
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