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Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum

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Resumo:We present insights into the mechanism of action of marinoquinolines (MQ), a novel class of lead candidates. Using a divergent synthetic approach, we developed a series of 20 new analogues with fluorescence properties. Structure–activity relationships analysis identified 19 as an attractive compound showing a combination of favorable in vitro (IC503D7= 0.28 μM; CC50HepG2= 53 μM), ex vivo (EC50Pf= 1.2 μM; EC50Pv= 0.53 μM), in vivo (3 × 50 mg/kg oral dose resulted in a 96% reduction in parasitemia in Plasmodium berghei-infected mice), physicochemical (Sol7.4= 171 μM; LogD7.4= 3.9), and pharmacokinetic (P_app = 9.4 × 10–6cm/s, human Clinthep,mic= 0.61–0.68 μL min–1mg–1) properties. Compound 19 selectively accumulates in infected erythrocytes, enters the digest vacuole and inhibits Plasmodium falciparum proteolytic activity, suggesting that MQs act as protease inhibitors. These findings strengthen the evidence that MQs are promising lead candidates for antimalarial drug discovery.
Autores principais:Santos Barbosa, Patricia
Outros Autores:Souza, Guilherme Eduardo; Maluf, Sarah El Chamy; Bonatto, Vinícius; Moura, Caio Silva; Mendes, Giovana Rossi; Valdes, Talita Alvarenga; Annunciato, Yasmin; Rossetto, Barbara dos Santos; Ventura, Priscilla Dantas de Souza; Ortin, Gilberto Gaspar Duarte; da Silva, Wellington; Icimoto, Marcelo Yudi; Ferreira, Amália dos Santos; Cruz, Fabio C.; Teles, Carolina B. G.; Pereira, Dhelio B.; Cassiano, Gustavo Capatti; Santana, Sofia; Prudêncio, Miguel; Barbosa, Camila S.; Moura, Igor M. R.; Giampauli, Renan Marcel; De Sousa, Irene Layane; Rocco, Silvana Aparecida; Gazarini, Marcos L.; Correia, Carlos Roque Duarte; Aguiar, Anna Caroline Campos; Guido, Rafael Victorio Carvalho
Assunto:Molecular Medicine Drug Discovery
Ano:2025
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade Nova de Lisboa
Idioma:inglês
Origem:Repositório Institucional da UNL
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author Santos Barbosa, Patricia
author2 Souza, Guilherme Eduardo
Maluf, Sarah El Chamy
Bonatto, Vinícius
Moura, Caio Silva
Mendes, Giovana Rossi
Valdes, Talita Alvarenga
Annunciato, Yasmin
Rossetto, Barbara dos Santos
Ventura, Priscilla Dantas de Souza
Ortin, Gilberto Gaspar Duarte
da Silva, Wellington
Icimoto, Marcelo Yudi
Ferreira, Amália dos Santos
Cruz, Fabio C.
Teles, Carolina B. G.
Pereira, Dhelio B.
Cassiano, Gustavo Capatti
Santana, Sofia
Prudêncio, Miguel
Barbosa, Camila S.
Moura, Igor M. R.
Giampauli, Renan Marcel
De Sousa, Irene Layane
Rocco, Silvana Aparecida
Gazarini, Marcos L.
Correia, Carlos Roque Duarte
Aguiar, Anna Caroline Campos
Guido, Rafael Victorio Carvalho
author2_role author
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author
author
author
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author
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author
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author
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author
author_facet Santos Barbosa, Patricia
Souza, Guilherme Eduardo
Maluf, Sarah El Chamy
Bonatto, Vinícius
Moura, Caio Silva
Mendes, Giovana Rossi
Valdes, Talita Alvarenga
Annunciato, Yasmin
Rossetto, Barbara dos Santos
Ventura, Priscilla Dantas de Souza
Ortin, Gilberto Gaspar Duarte
da Silva, Wellington
Icimoto, Marcelo Yudi
Ferreira, Amália dos Santos
Cruz, Fabio C.
Teles, Carolina B. G.
Pereira, Dhelio B.
Cassiano, Gustavo Capatti
Santana, Sofia
Prudêncio, Miguel
Barbosa, Camila S.
Moura, Igor M. R.
Giampauli, Renan Marcel
De Sousa, Irene Layane
Rocco, Silvana Aparecida
Gazarini, Marcos L.
Correia, Carlos Roque Duarte
Aguiar, Anna Caroline Campos
Guido, Rafael Victorio Carvalho
author_role author
contributor_name_str_mv Laboratório Associado de Translacção e Inovação para a Saúde Global - LA Real (Pólo IHMT)
Vector borne diseases and pathogens (VBD)
Global Health and Tropical Medicine (GHTM)
Instituto de Higiene e Medicina Tropical (IHMT)
ACS - American Chemical Society
RUN
country_str PT
creators_json_txt [{\"Person.name\":\"Santos Barbosa, Patricia\"},{\"Person.name\":\"Souza, Guilherme Eduardo\"},{\"Person.name\":\"Maluf, Sarah El Chamy\"},{\"Person.name\":\"Bonatto, Vinícius\"},{\"Person.name\":\"Moura, Caio Silva\"},{\"Person.name\":\"Mendes, Giovana Rossi\"},{\"Person.name\":\"Valdes, Talita Alvarenga\"},{\"Person.name\":\"Annunciato, Yasmin\"},{\"Person.name\":\"Rossetto, Barbara dos Santos\"},{\"Person.name\":\"Ventura, Priscilla Dantas de Souza\"},{\"Person.name\":\"Ortin, Gilberto Gaspar Duarte\"},{\"Person.name\":\"da Silva, Wellington\"},{\"Person.name\":\"Icimoto, Marcelo Yudi\"},{\"Person.name\":\"Ferreira, Amália dos Santos\"},{\"Person.name\":\"Cruz, Fabio C.\"},{\"Person.name\":\"Teles, Carolina B. G.\"},{\"Person.name\":\"Pereira, Dhelio B.\"},{\"Person.name\":\"Cassiano, Gustavo Capatti\"},{\"Person.name\":\"Santana, Sofia\"},{\"Person.name\":\"Prudêncio, Miguel\"},{\"Person.name\":\"Barbosa, Camila S.\"},{\"Person.name\":\"Moura, Igor M. R.\"},{\"Person.name\":\"Giampauli, Renan Marcel\"},{\"Person.name\":\"De Sousa, Irene Layane\"},{\"Person.name\":\"Rocco, Silvana Aparecida\"},{\"Person.name\":\"Gazarini, Marcos L.\"},{\"Person.name\":\"Correia, Carlos Roque Duarte\"},{\"Person.name\":\"Aguiar, Anna Caroline Campos\"},{\"Person.name\":\"Guido, Rafael Victorio Carvalho\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Laboratório Associado de Translacção e Inovação para a Saúde Global - LA Real (Pólo IHMT)
Vector borne diseases and pathogens (VBD)
Global Health and Tropical Medicine (GHTM)
Instituto de Higiene e Medicina Tropical (IHMT)
ACS - American Chemical Society
RUN
datacite.creators.creator.creatorName.fl_str_mv Santos Barbosa, Patricia
Souza, Guilherme Eduardo
Maluf, Sarah El Chamy
Bonatto, Vinícius
Moura, Caio Silva
Mendes, Giovana Rossi
Valdes, Talita Alvarenga
Annunciato, Yasmin
Rossetto, Barbara dos Santos
Ventura, Priscilla Dantas de Souza
Ortin, Gilberto Gaspar Duarte
da Silva, Wellington
Icimoto, Marcelo Yudi
Ferreira, Amália dos Santos
Cruz, Fabio C.
Teles, Carolina B. G.
Pereira, Dhelio B.
Cassiano, Gustavo Capatti
Santana, Sofia
Prudêncio, Miguel
Barbosa, Camila S.
Moura, Igor M. R.
Giampauli, Renan Marcel
De Sousa, Irene Layane
Rocco, Silvana Aparecida
Gazarini, Marcos L.
Correia, Carlos Roque Duarte
Aguiar, Anna Caroline Campos
Guido, Rafael Victorio Carvalho
datacite.date.Accepted.fl_str_mv 2025-10-23T00:00:00Z
datacite.date.available.fl_str_mv 2026-03-11T15:29:02Z
datacite.date.embargoed.fl_str_mv 2026-03-11T15:29:02Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Molecular Medicine
Drug Discovery
datacite.titles.title.fl_str_mv Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
SAR Analysis, Mode of Action and In Vivo Studies
dc.contributor.none.fl_str_mv Laboratório Associado de Translacção e Inovação para a Saúde Global - LA Real (Pólo IHMT)
Vector borne diseases and pathogens (VBD)
Global Health and Tropical Medicine (GHTM)
Instituto de Higiene e Medicina Tropical (IHMT)
ACS - American Chemical Society
RUN
dc.creator.none.fl_str_mv Santos Barbosa, Patricia
Souza, Guilherme Eduardo
Maluf, Sarah El Chamy
Bonatto, Vinícius
Moura, Caio Silva
Mendes, Giovana Rossi
Valdes, Talita Alvarenga
Annunciato, Yasmin
Rossetto, Barbara dos Santos
Ventura, Priscilla Dantas de Souza
Ortin, Gilberto Gaspar Duarte
da Silva, Wellington
Icimoto, Marcelo Yudi
Ferreira, Amália dos Santos
Cruz, Fabio C.
Teles, Carolina B. G.
Pereira, Dhelio B.
Cassiano, Gustavo Capatti
Santana, Sofia
Prudêncio, Miguel
Barbosa, Camila S.
Moura, Igor M. R.
Giampauli, Renan Marcel
De Sousa, Irene Layane
Rocco, Silvana Aparecida
Gazarini, Marcos L.
Correia, Carlos Roque Duarte
Aguiar, Anna Caroline Campos
Guido, Rafael Victorio Carvalho
dc.date.Accepted.fl_str_mv 2025-10-23T00:00:00Z
dc.date.available.fl_str_mv 2026-03-11T15:29:02Z
dc.date.embargoed.fl_str_mv 2026-03-11T15:29:02Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10362/201282
dc.language.none.fl_str_mv eng
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Molecular Medicine
Drug Discovery
dc.title.fl_str_mv Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
SAR Analysis, Mode of Action and In Vivo Studies
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description We present insights into the mechanism of action of marinoquinolines (MQ), a novel class of lead candidates. Using a divergent synthetic approach, we developed a series of 20 new analogues with fluorescence properties. Structure–activity relationships analysis identified 19 as an attractive compound showing a combination of favorable in vitro (IC503D7= 0.28 μM; CC50HepG2= 53 μM), ex vivo (EC50Pf= 1.2 μM; EC50Pv= 0.53 μM), in vivo (3 × 50 mg/kg oral dose resulted in a 96% reduction in parasitemia in Plasmodium berghei-infected mice), physicochemical (Sol7.4= 171 μM; LogD7.4= 3.9), and pharmacokinetic (P_app = 9.4 × 10–6cm/s, human Clinthep,mic= 0.61–0.68 μL min–1mg–1) properties. Compound 19 selectively accumulates in infected erythrocytes, enters the digest vacuole and inhibits Plasmodium falciparum proteolytic activity, suggesting that MQs act as protease inhibitors. These findings strengthen the evidence that MQs are promising lead candidates for antimalarial drug discovery.
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eu_rights_str_mv openAccess
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fulltext.url.fl_str_mv https://run.unl.pt/bitstreams/5c2c73b3-23df-4bdf-9aad-93188073e1df/download
id run_615d4cbff84e6f8407dc7ff3f2d8afaf
identifier.url.fl_str_mv http://hdl.handle.net/10362/201282
inst_facet_str urn:organizationAcronym:unl{{{_:::_}}}Universidade Nova de Lisboa
instacron_str unl
institution Universidade Nova de Lisboa
instname_str Universidade Nova de Lisboa
language eng
network_acronym_str run
network_name_str Repositório Institucional da UNL
oai_identifier_str oai:run.unl.pt:10362/201282
organization_str_mv urn:organizationAcronym:unl
person_str_mv Santos Barbosa, Patricia
Souza, Guilherme Eduardo
Maluf, Sarah El Chamy
Bonatto, Vinícius
Moura, Caio Silva
Mendes, Giovana Rossi
Valdes, Talita Alvarenga
Annunciato, Yasmin
Rossetto, Barbara dos Santos
Ventura, Priscilla Dantas de Souza
Ortin, Gilberto Gaspar Duarte
da Silva, Wellington
Icimoto, Marcelo Yudi
Ferreira, Amália dos Santos
Cruz, Fabio C.
Teles, Carolina B. G.
Pereira, Dhelio B.
Cassiano, Gustavo Capatti
Santana, Sofia
Prudêncio, Miguel
Barbosa, Camila S.
Moura, Igor M. R.
Giampauli, Renan Marcel
De Sousa, Irene Layane
Rocco, Silvana Aparecida
Gazarini, Marcos L.
Correia, Carlos Roque Duarte
Aguiar, Anna Caroline Campos
Guido, Rafael Victorio Carvalho
publishDate 2025
repo_facet_str urn:repositoryAcronym:run{{{_:::_}}}Repositório Institucional da UNL
reponame_str Repositório Institucional da UNL
repository_id_str urn:repositoryAcronym:run
service_str_mv urn:repositoryAcronym:run
spelling engenWe present insights into the mechanism of action of marinoquinolines (MQ), a novel class of lead candidates. Using a divergent synthetic approach, we developed a series of 20 new analogues with fluorescence properties. Structure–activity relationships analysis identified 19 as an attractive compound showing a combination of favorable in vitro (IC503D7= 0.28 μM; CC50HepG2= 53 μM), ex vivo (EC50Pf= 1.2 μM; EC50Pv= 0.53 μM), in vivo (3 × 50 mg/kg oral dose resulted in a 96% reduction in parasitemia in Plasmodium berghei-infected mice), physicochemical (Sol7.4= 171 μM; LogD7.4= 3.9), and pharmacokinetic (P_app = 9.4 × 10–6cm/s, human Clinthep,mic= 0.61–0.68 μL min–1mg–1) properties. Compound 19 selectively accumulates in infected erythrocytes, enters the digest vacuole and inhibits Plasmodium falciparum proteolytic activity, suggesting that MQs act as protease inhibitors. These findings strengthen the evidence that MQs are promising lead candidates for antimalarial drug discovery.application/pdfenFluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparumSubtitleenSAR Analysis, Mode of Action and In Vivo StudiesSantos Barbosa, PatriciaSouza, Guilherme EduardoMaluf, Sarah El ChamyBonatto, ViníciusMoura, Caio SilvaMendes, Giovana RossiValdes, Talita AlvarengaAnnunciato, YasminRossetto, Barbara dos SantosVentura, Priscilla Dantas de SouzaOrtin, Gilberto Gaspar Duarteda Silva, WellingtonIcimoto, Marcelo YudiFerreira, Amália dos SantosCruz, Fabio C.Teles, Carolina B. G.Pereira, Dhelio B.Cassiano, Gustavo CapattiSantana, SofiaPrudêncio, MiguelBarbosa, Camila S.Moura, Igor M. R.Giampauli, Renan MarcelDe Sousa, Irene LayaneRocco, Silvana AparecidaGazarini, Marcos L.Correia, Carlos Roque DuarteAguiar, Anna Caroline CamposGuido, Rafael Victorio CarvalhoLaboratório Associado de Translacção e Inovação para a Saúde Global - LA Real (Pólo IHMT)Vector borne diseases and pathogens (VBD)Global Health and Tropical Medicine (GHTM)Instituto de Higiene e Medicina Tropical (IHMT)ACS - American Chemical SocietyHostingInstitutionOrganizationalRUNe-mailmailto:run@unl.ptrun@unl.ptISSNIsPartOf0022-2623URNIsPartOfPURE: 152514430URNIsPartOfPURE UUID: d4cb10d7-e7ab-4737-a188-8183ea22561cURNIsPartOfScopus: 105019589475URNIsPartOfWOS: 001584713400001URNIsPartOfPubMed: 41026123URNIsPartOfPubMedCentral: PMC12557366DOIIsPartOf10.1021/acs.jmedchem.5c001382026-03-11T15:29:02Z2025-10-232025-10-23T00:00:00ZHandlehttp://hdl.handle.net/10362/201282http://purl.org/coar/access_right/c_abf2open accessMolecular MedicineDrug Discovery12828731 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://run.unl.pt/bitstreams/5c2c73b3-23df-4bdf-9aad-93188073e1df/download
spellingShingle Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
Santos Barbosa, Patricia
Molecular Medicine
Drug Discovery
status SINGLETON
subject.fl_str_mv Molecular Medicine
Drug Discovery
title Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
title_full Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
title_fullStr Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
title_full_unstemmed Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
title_short Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
title_sort Fluorescent Marinoquinoline Derivative as Inhibitors of Plasmodium falciparum
topic Molecular Medicine
Drug Discovery
topic_facet Molecular Medicine
Drug Discovery
url http://hdl.handle.net/10362/201282
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