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Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1

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Resumo:The contribution of Fe(II)-oxidizing bacteria to iron cycling in freshwater, groundwater, and marine environments has been widely recognized in recent years. These organisms perform extracellular electron transfer (EET), which constitutes the foundations of bioelectrochemical systems for the production of biofuels and bioenergy. It was proposed that the Gram-negative bacterium Sideroxydans lithotrophicus ES-1 oxidizes soluble ferrous Fe(II) at the surface of the cell and performs EET through the Mto redox pathway. This pathway is composed by the periplasmic monoheme cytochrome MtoD that is proposed to bridge electron transfer between the cell exterior and the cytoplasm. This makes its functional and structural characterization, as well as evaluating the interaction process with its physiological partners, essential for understanding the mechanisms underlying EET. Here, we report the complete assignment of the heme proton and carbon signals together with a near-complete assignment of 1H, 13C and 15N backbone and side chain resonances for the reduced, diamagnetic form of the protein. These data pave the way to identify and structurally map the molecular interaction regions between the cytochrome MtoD and its physiological redox partners, to explore the EET processes of S. lithotrophicus ES-1.
Autores principais:Coelho, Anaísa
Outros Autores:Silva, José M.; Cantini, Francesca; Piccioli, Mario; Louro, Ricardo O.; Paquete, Catarina M.
Assunto:Cytochromes Extracellular electron transfer MtoD NMR resonance assignment Ring current shifts Structural Biology Biochemistry SDG 6 - Clean Water and Sanitation SDG 14 - Life Below Water
Ano:2024
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade Nova de Lisboa
Idioma:inglês
Origem:Repositório Institucional da UNL
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author Coelho, Anaísa
author2 Silva, José M.
Cantini, Francesca
Piccioli, Mario
Louro, Ricardo O.
Paquete, Catarina M.
author2_role author
author
author
author
author
author_facet Coelho, Anaísa
Silva, José M.
Cantini, Francesca
Piccioli, Mario
Louro, Ricardo O.
Paquete, Catarina M.
author_role author
contributor_name_str_mv Instituto de Tecnologia Química e Biológica António Xavier (ITQB)
Springer
RUN
country_str PT
creators_json_txt [{\"Person.name\":\"Coelho, Anaísa\"},{\"Person.name\":\"Silva, José M.\"},{\"Person.name\":\"Cantini, Francesca\"},{\"Person.name\":\"Piccioli, Mario\"},{\"Person.name\":\"Louro, Ricardo O.\"},{\"Person.name\":\"Paquete, Catarina M.\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Instituto de Tecnologia Química e Biológica António Xavier (ITQB)
Springer
RUN
datacite.creators.creator.creatorName.fl_str_mv Coelho, Anaísa
Silva, José M.
Cantini, Francesca
Piccioli, Mario
Louro, Ricardo O.
Paquete, Catarina M.
datacite.date.Accepted.fl_str_mv 2024-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2025-05-07T21:19:24Z
datacite.date.embargoed.fl_str_mv 2025-05-07T21:19:24Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Cytochromes
Extracellular electron transfer
MtoD
NMR resonance assignment
Ring current shifts
Structural Biology
Biochemistry
SDG 6 - Clean Water and Sanitation
SDG 14 - Life Below Water
datacite.titles.title.fl_str_mv Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
dc.contributor.none.fl_str_mv Instituto de Tecnologia Química e Biológica António Xavier (ITQB)
Springer
RUN
dc.creator.none.fl_str_mv Coelho, Anaísa
Silva, José M.
Cantini, Francesca
Piccioli, Mario
Louro, Ricardo O.
Paquete, Catarina M.
dc.date.Accepted.fl_str_mv 2024-01-01T00:00:00Z
dc.date.available.fl_str_mv 2025-05-07T21:19:24Z
dc.date.embargoed.fl_str_mv 2025-05-07T21:19:24Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10362/182746
dc.language.none.fl_str_mv eng
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Cytochromes
Extracellular electron transfer
MtoD
NMR resonance assignment
Ring current shifts
Structural Biology
Biochemistry
SDG 6 - Clean Water and Sanitation
SDG 14 - Life Below Water
dc.title.fl_str_mv Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description The contribution of Fe(II)-oxidizing bacteria to iron cycling in freshwater, groundwater, and marine environments has been widely recognized in recent years. These organisms perform extracellular electron transfer (EET), which constitutes the foundations of bioelectrochemical systems for the production of biofuels and bioenergy. It was proposed that the Gram-negative bacterium Sideroxydans lithotrophicus ES-1 oxidizes soluble ferrous Fe(II) at the surface of the cell and performs EET through the Mto redox pathway. This pathway is composed by the periplasmic monoheme cytochrome MtoD that is proposed to bridge electron transfer between the cell exterior and the cytoplasm. This makes its functional and structural characterization, as well as evaluating the interaction process with its physiological partners, essential for understanding the mechanisms underlying EET. Here, we report the complete assignment of the heme proton and carbon signals together with a near-complete assignment of 1H, 13C and 15N backbone and side chain resonances for the reduced, diamagnetic form of the protein. These data pave the way to identify and structurally map the molecular interaction regions between the cytochrome MtoD and its physiological redox partners, to explore the EET processes of S. lithotrophicus ES-1.
dirty 0
eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://run.unl.pt/bitstreams/417594bd-0ed6-4db2-88e4-75aa75605780/download
id run_c1bf455ea3279ced0232dd4e3d064eb9
identifier.url.fl_str_mv http://hdl.handle.net/10362/182746
inst_facet_str urn:organizationAcronym:unl{{{_:::_}}}Universidade Nova de Lisboa
instacron_str unl
institution Universidade Nova de Lisboa
instname_str Universidade Nova de Lisboa
language eng
network_acronym_str run
network_name_str Repositório Institucional da UNL
oai_identifier_str oai:run.unl.pt:10362/182746
organization_str_mv urn:organizationAcronym:unl
person_str_mv Coelho, Anaísa
Silva, José M.
Cantini, Francesca
Piccioli, Mario
Louro, Ricardo O.
Paquete, Catarina M.
publishDate 2024
repo_facet_str urn:repositoryAcronym:run{{{_:::_}}}Repositório Institucional da UNL
reponame_str Repositório Institucional da UNL
repository_id_str urn:repositoryAcronym:run
service_str_mv urn:repositoryAcronym:run
spelling engenThe contribution of Fe(II)-oxidizing bacteria to iron cycling in freshwater, groundwater, and marine environments has been widely recognized in recent years. These organisms perform extracellular electron transfer (EET), which constitutes the foundations of bioelectrochemical systems for the production of biofuels and bioenergy. It was proposed that the Gram-negative bacterium Sideroxydans lithotrophicus ES-1 oxidizes soluble ferrous Fe(II) at the surface of the cell and performs EET through the Mto redox pathway. This pathway is composed by the periplasmic monoheme cytochrome MtoD that is proposed to bridge electron transfer between the cell exterior and the cytoplasm. This makes its functional and structural characterization, as well as evaluating the interaction process with its physiological partners, essential for understanding the mechanisms underlying EET. Here, we report the complete assignment of the heme proton and carbon signals together with a near-complete assignment of 1H, 13C and 15N backbone and side chain resonances for the reduced, diamagnetic form of the protein. These data pave the way to identify and structurally map the molecular interaction regions between the cytochrome MtoD and its physiological redox partners, to explore the EET processes of S. lithotrophicus ES-1.application/pdfenResonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1Coelho, AnaísaSilva, José M.Cantini, FrancescaPiccioli, MarioLouro, Ricardo O.Paquete, Catarina M.Instituto de Tecnologia Química e Biológica António Xavier (ITQB)SpringerHostingInstitutionOrganizationalRUNe-mailmailto:run@unl.ptrun@unl.ptISSNIsPartOf1874-2718URNIsPartOfPURE: 99908831URNIsPartOfPURE UUID: 3908f254-7bb1-4e4a-963a-edd52c59a601URNIsPartOfScopus: 85195255574DOIIsPartOf10.1007/s12104-024-10180-82025-05-07T21:19:24Z20242024-01-01T00:00:00ZHandlehttp://hdl.handle.net/10362/182746http://purl.org/coar/access_right/c_abf2open accessCytochromesExtracellular electron transferMtoDNMR resonance assignmentRing current shiftsStructural BiologyBiochemistrySDG 6 - Clean Water and SanitationSDG 14 - Life Below Water1468792 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://run.unl.pt/bitstreams/417594bd-0ed6-4db2-88e4-75aa75605780/download
spellingShingle Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
Coelho, Anaísa
Cytochromes
Extracellular electron transfer
MtoD
NMR resonance assignment
Ring current shifts
Structural Biology
Biochemistry
SDG 6 - Clean Water and Sanitation
SDG 14 - Life Below Water
status SINGLETON
subject.fl_str_mv Cytochromes
Extracellular electron transfer
MtoD
NMR resonance assignment
Ring current shifts
Structural Biology
Biochemistry
SDG 6 - Clean Water and Sanitation
SDG 14 - Life Below Water
title Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
title_full Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
title_fullStr Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
title_full_unstemmed Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
title_short Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
title_sort Resonance assignments of cytochrome MtoD from the extracellular electron uptake pathway of sideroxydans lithotrophicus ES-1
topic Cytochromes
Extracellular electron transfer
MtoD
NMR resonance assignment
Ring current shifts
Structural Biology
Biochemistry
SDG 6 - Clean Water and Sanitation
SDG 14 - Life Below Water
topic_facet Cytochromes
Extracellular electron transfer
MtoD
NMR resonance assignment
Ring current shifts
Structural Biology
Biochemistry
SDG 6 - Clean Water and Sanitation
SDG 14 - Life Below Water
url http://hdl.handle.net/10362/182746
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