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Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme

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Resumo:The integration of enzymes with semiconductor light absorbers in semiartificial photosynthetic assemblies offers an emerging strategy for solar fuel production. However, such colloidal biohybrid systems rely currently on sacrificial reagents, and semiconductor-enzyme powder systems that couple fuel production to water oxidation are therefore needed to mimic an overall photosynthetic reaction. Here, we present a Z-scheme colloidal enzyme system that produces fuel with electrons sourced from water. This “closed-cycle” semiartificial approach utilizes particulate SrTiO3:La,Rh and BiVO4:Mo (light absorbers), hydrogenase or formate dehydrogenase (cocatalyst), and a molecular cobalt complex (a redox mediator). Under simulated solar irradiation, this system continuously generates molecular hydrogen or formate, while co-producing molecular oxygen for 10 h using only sunlight, water, and carbon dioxide as inputs. In-depth analysis using quartz crystal microbalance, photoelectrochemical impedance spectroscopy, transient photocurrent spectroscopy, and intensity-modulated photovoltage spectroscopy provides mechanistic understanding and characterization of the semiconductor-enzyme hybrid interface. This study provides a rational platform to assemble functional semiartificial colloidal Z-scheme systems for solar fuel synthesis.
Autores principais:Liu, Yongpeng
Outros Autores:Bin Mohamad Annuar, Ariffin; Rodríguez-Jiménez, Santiago; Yeung, Celine Wing See; Wang, Qian; Coito, Ana M.; Manuel, Rita R.; Pereira, Inês A.C.; Reisner, Erwin
Assunto:Catalysis General Chemistry Biochemistry Colloid and Surface Chemistry
Ano:2024
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade Nova de Lisboa
Idioma:inglês
Origem:Repositório Institucional da UNL
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author Liu, Yongpeng
author2 Bin Mohamad Annuar, Ariffin
Rodríguez-Jiménez, Santiago
Yeung, Celine Wing See
Wang, Qian
Coito, Ana M.
Manuel, Rita R.
Pereira, Inês A.C.
Reisner, Erwin
author2_role author
author
author
author
author
author
author
author
author_facet Liu, Yongpeng
Bin Mohamad Annuar, Ariffin
Rodríguez-Jiménez, Santiago
Yeung, Celine Wing See
Wang, Qian
Coito, Ana M.
Manuel, Rita R.
Pereira, Inês A.C.
Reisner, Erwin
author_role author
contributor_name_str_mv Instituto de Tecnologia Química e Biológica António Xavier (ITQB)
ACS - American Chemical Society
RUN
country_str PT
creators_json_txt [{\"Person.name\":\"Liu, Yongpeng\"},{\"Person.name\":\"Bin Mohamad Annuar, Ariffin\"},{\"Person.name\":\"Rodríguez-Jiménez, Santiago\"},{\"Person.name\":\"Yeung, Celine Wing See\"},{\"Person.name\":\"Wang, Qian\"},{\"Person.name\":\"Coito, Ana M.\"},{\"Person.name\":\"Manuel, Rita R.\"},{\"Person.name\":\"Pereira, Inês A.C.\"},{\"Person.name\":\"Reisner, Erwin\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Instituto de Tecnologia Química e Biológica António Xavier (ITQB)
ACS - American Chemical Society
RUN
datacite.creators.creator.creatorName.fl_str_mv Liu, Yongpeng
Bin Mohamad Annuar, Ariffin
Rodríguez-Jiménez, Santiago
Yeung, Celine Wing See
Wang, Qian
Coito, Ana M.
Manuel, Rita R.
Pereira, Inês A.C.
Reisner, Erwin
datacite.date.Accepted.fl_str_mv 2024-10-16T00:00:00Z
datacite.date.available.fl_str_mv 2025-05-07T21:24:18Z
datacite.date.embargoed.fl_str_mv 2025-05-07T21:24:18Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Catalysis
General Chemistry
Biochemistry
Colloid and Surface Chemistry
datacite.titles.title.fl_str_mv Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
dc.contributor.none.fl_str_mv Instituto de Tecnologia Química e Biológica António Xavier (ITQB)
ACS - American Chemical Society
RUN
dc.creator.none.fl_str_mv Liu, Yongpeng
Bin Mohamad Annuar, Ariffin
Rodríguez-Jiménez, Santiago
Yeung, Celine Wing See
Wang, Qian
Coito, Ana M.
Manuel, Rita R.
Pereira, Inês A.C.
Reisner, Erwin
dc.date.Accepted.fl_str_mv 2024-10-16T00:00:00Z
dc.date.available.fl_str_mv 2025-05-07T21:24:18Z
dc.date.embargoed.fl_str_mv 2025-05-07T21:24:18Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10362/182778
dc.language.none.fl_str_mv eng
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Catalysis
General Chemistry
Biochemistry
Colloid and Surface Chemistry
dc.title.fl_str_mv Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description The integration of enzymes with semiconductor light absorbers in semiartificial photosynthetic assemblies offers an emerging strategy for solar fuel production. However, such colloidal biohybrid systems rely currently on sacrificial reagents, and semiconductor-enzyme powder systems that couple fuel production to water oxidation are therefore needed to mimic an overall photosynthetic reaction. Here, we present a Z-scheme colloidal enzyme system that produces fuel with electrons sourced from water. This “closed-cycle” semiartificial approach utilizes particulate SrTiO3:La,Rh and BiVO4:Mo (light absorbers), hydrogenase or formate dehydrogenase (cocatalyst), and a molecular cobalt complex (a redox mediator). Under simulated solar irradiation, this system continuously generates molecular hydrogen or formate, while co-producing molecular oxygen for 10 h using only sunlight, water, and carbon dioxide as inputs. In-depth analysis using quartz crystal microbalance, photoelectrochemical impedance spectroscopy, transient photocurrent spectroscopy, and intensity-modulated photovoltage spectroscopy provides mechanistic understanding and characterization of the semiconductor-enzyme hybrid interface. This study provides a rational platform to assemble functional semiartificial colloidal Z-scheme systems for solar fuel synthesis.
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eu_rights_str_mv openAccess
format article
fulltext.url.fl_str_mv https://run.unl.pt/bitstreams/09e85dfa-bf89-45bf-855e-fb23ec20d130/download
id run_ded1942e4504e4c7bc531f9ca1144cdf
identifier.url.fl_str_mv http://hdl.handle.net/10362/182778
inst_facet_str urn:organizationAcronym:unl{{{_:::_}}}Universidade Nova de Lisboa
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institution Universidade Nova de Lisboa
instname_str Universidade Nova de Lisboa
language eng
network_acronym_str run
network_name_str Repositório Institucional da UNL
oai_identifier_str oai:run.unl.pt:10362/182778
organization_str_mv urn:organizationAcronym:unl
person_str_mv Liu, Yongpeng
Bin Mohamad Annuar, Ariffin
Rodríguez-Jiménez, Santiago
Yeung, Celine Wing See
Wang, Qian
Coito, Ana M.
Manuel, Rita R.
Pereira, Inês A.C.
Reisner, Erwin
publishDate 2024
repo_facet_str urn:repositoryAcronym:run{{{_:::_}}}Repositório Institucional da UNL
reponame_str Repositório Institucional da UNL
repository_id_str urn:repositoryAcronym:run
service_str_mv urn:repositoryAcronym:run
spelling engenThe integration of enzymes with semiconductor light absorbers in semiartificial photosynthetic assemblies offers an emerging strategy for solar fuel production. However, such colloidal biohybrid systems rely currently on sacrificial reagents, and semiconductor-enzyme powder systems that couple fuel production to water oxidation are therefore needed to mimic an overall photosynthetic reaction. Here, we present a Z-scheme colloidal enzyme system that produces fuel with electrons sourced from water. This “closed-cycle” semiartificial approach utilizes particulate SrTiO3:La,Rh and BiVO4:Mo (light absorbers), hydrogenase or formate dehydrogenase (cocatalyst), and a molecular cobalt complex (a redox mediator). Under simulated solar irradiation, this system continuously generates molecular hydrogen or formate, while co-producing molecular oxygen for 10 h using only sunlight, water, and carbon dioxide as inputs. In-depth analysis using quartz crystal microbalance, photoelectrochemical impedance spectroscopy, transient photocurrent spectroscopy, and intensity-modulated photovoltage spectroscopy provides mechanistic understanding and characterization of the semiconductor-enzyme hybrid interface. This study provides a rational platform to assemble functional semiartificial colloidal Z-scheme systems for solar fuel synthesis.application/pdfenSolar Fuel Synthesis Using a Semiartificial Colloidal Z-SchemeLiu, YongpengBin Mohamad Annuar, AriffinRodríguez-Jiménez, SantiagoYeung, Celine Wing SeeWang, QianCoito, Ana M.Manuel, Rita R.Pereira, Inês A.C.Reisner, ErwinInstituto de Tecnologia Química e Biológica António Xavier (ITQB)ACS - American Chemical SocietyHostingInstitutionOrganizationalRUNe-mailmailto:run@unl.ptrun@unl.ptISSNIsPartOf0002-7863URNIsPartOfPURE: 111148056URNIsPartOfPURE UUID: feada21d-8402-4f62-9dd1-e5710ec614a0URNIsPartOfScopus: 85207154942URNIsPartOfPubMed: 39413284DOIIsPartOf10.1021/jacs.4c118272025-05-07T21:24:18Z2024-10-162024-10-16T00:00:00ZHandlehttp://hdl.handle.net/10362/182778http://purl.org/coar/access_right/c_abf2open accessCatalysisGeneral ChemistryBiochemistryColloid and Surface Chemistry4402879 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://run.unl.pt/bitstreams/09e85dfa-bf89-45bf-855e-fb23ec20d130/download
spellingShingle Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
Liu, Yongpeng
Catalysis
General Chemistry
Biochemistry
Colloid and Surface Chemistry
status SINGLETON
subject.fl_str_mv Catalysis
General Chemistry
Biochemistry
Colloid and Surface Chemistry
title Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
title_full Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
title_fullStr Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
title_full_unstemmed Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
title_short Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
title_sort Solar Fuel Synthesis Using a Semiartificial Colloidal Z-Scheme
topic Catalysis
General Chemistry
Biochemistry
Colloid and Surface Chemistry
topic_facet Catalysis
General Chemistry
Biochemistry
Colloid and Surface Chemistry
url http://hdl.handle.net/10362/182778
visible 1