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Cross-linked alginate-gelatine beads

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Resumo:This work is focused on the development of a new particulate drug delivery system using a sodium alginate matrix containing pindolol as a model drug molecule for intestinal drug prolonged release. Calcium alginate beads are known to be unable to control the release of most insoluble drugs. Pindolol-loaded alginate-gelatine beads have been developed using a solvent-free technique that involves a cross-linking reaction. Modifications in matrix structure and physicochemical behaviour caused by the cross-linking reaction were assessed during particle formation and drug release. Several parameters, such as matrix gelling rate, encapsulation efficiency, drug release profile and matrix erosion rate, were investigated. Physicochemical characterisation indicates the formation of a new alginate-gelatine matrix and shows that pindolol does not interfere with the matrix formation process. Matrix swelling of calcium alginate beads induced by phosphate buffer ends up in erosion and destruction. However, for cross-linked beads swelling does not lead to complete erosion, which may be the main cause of pindolol retention within the matrix. The modifications introduced in the initial calcium alginate formulation by means of an appropriate method such as the use of a cross-linking agent successfully changed the matrix performance, allowing the controlled release of pindolol. (C) 2004 Elsevier B.V. All rights reserved.
Autores principais:Almeida, PF
Outros Autores:Almeida, AJ
Assunto:Chemistry, Multidisciplinary Pharmacology & Pharmacy
Ano:2004
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso a metadados
Instituição associada:Universidade de Lisboa
Idioma:inglês
Origem:Repositório da Universidade de Lisboa
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author Almeida, PF
author2 Almeida, AJ
author2_role author
author_facet Almeida, PF
Almeida, AJ
author_role author
contributor_name_str_mv Repositório Científico de Acesso Aberto da ULisboa
country_str PT
creators_json_txt [{\"Person.name\":\"Almeida, PF\"},{\"Person.name\":\"Almeida, AJ\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Repositório Científico de Acesso Aberto da ULisboa
datacite.creators.creator.creatorName.fl_str_mv Almeida, PF
Almeida, AJ
datacite.date.Accepted.fl_str_mv 2004-01-01T00:00:00Z
datacite.date.available.fl_str_mv 2015-12-30T10:17:16Z
datacite.date.embargoed.fl_str_mv 2015-12-30T10:17:16Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_14cb
datacite.subjects.subject.fl_str_mv Chemistry, Multidisciplinary
Pharmacology & Pharmacy
datacite.titles.title.fl_str_mv Cross-linked alginate-gelatine beads
a new matrix for controlled release of pindolol
dc.contributor.none.fl_str_mv Repositório Científico de Acesso Aberto da ULisboa
dc.creator.none.fl_str_mv Almeida, PF
Almeida, AJ
dc.date.Accepted.fl_str_mv 2004-01-01T00:00:00Z
dc.date.available.fl_str_mv 2015-12-30T10:17:16Z
dc.date.embargoed.fl_str_mv 2015-12-30T10:17:16Z
dc.identifier.none.fl_str_mv http://hdl.handle.net/10451/20984
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv ELSEVIER SCIENCE BV
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_14cb
dc.subject.none.fl_str_mv Chemistry, Multidisciplinary
Pharmacology & Pharmacy
dc.title.fl_str_mv Cross-linked alginate-gelatine beads
a new matrix for controlled release of pindolol
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description This work is focused on the development of a new particulate drug delivery system using a sodium alginate matrix containing pindolol as a model drug molecule for intestinal drug prolonged release. Calcium alginate beads are known to be unable to control the release of most insoluble drugs. Pindolol-loaded alginate-gelatine beads have been developed using a solvent-free technique that involves a cross-linking reaction. Modifications in matrix structure and physicochemical behaviour caused by the cross-linking reaction were assessed during particle formation and drug release. Several parameters, such as matrix gelling rate, encapsulation efficiency, drug release profile and matrix erosion rate, were investigated. Physicochemical characterisation indicates the formation of a new alginate-gelatine matrix and shows that pindolol does not interfere with the matrix formation process. Matrix swelling of calcium alginate beads induced by phosphate buffer ends up in erosion and destruction. However, for cross-linked beads swelling does not lead to complete erosion, which may be the main cause of pindolol retention within the matrix. The modifications introduced in the initial calcium alginate formulation by means of an appropriate method such as the use of a cross-linking agent successfully changed the matrix performance, allowing the controlled release of pindolol. (C) 2004 Elsevier B.V. All rights reserved.
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id ul_0f64db57dec62b4d192a9d4e2e4525dc
identifier.url.fl_str_mv http://hdl.handle.net/10451/20984
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institution Universidade de Lisboa
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language eng
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oai_identifier_str oai:repositorio.ulisboa.pt:10451/20984
organization_str_mv urn:organizationAcronym:ul
person_str_mv Almeida, PF
Almeida, AJ
publishDate 2004
publisher.none.fl_str_mv ELSEVIER SCIENCE BV
reponame_str Repositório da Universidade de Lisboa
repository_id_str urn:repositoryAcronym:ul
service_str_mv urn:repositoryAcronym:ul
spelling engELSEVIER SCIENCE BVThis work is focused on the development of a new particulate drug delivery system using a sodium alginate matrix containing pindolol as a model drug molecule for intestinal drug prolonged release. Calcium alginate beads are known to be unable to control the release of most insoluble drugs. Pindolol-loaded alginate-gelatine beads have been developed using a solvent-free technique that involves a cross-linking reaction. Modifications in matrix structure and physicochemical behaviour caused by the cross-linking reaction were assessed during particle formation and drug release. Several parameters, such as matrix gelling rate, encapsulation efficiency, drug release profile and matrix erosion rate, were investigated. Physicochemical characterisation indicates the formation of a new alginate-gelatine matrix and shows that pindolol does not interfere with the matrix formation process. Matrix swelling of calcium alginate beads induced by phosphate buffer ends up in erosion and destruction. However, for cross-linked beads swelling does not lead to complete erosion, which may be the main cause of pindolol retention within the matrix. The modifications introduced in the initial calcium alginate formulation by means of an appropriate method such as the use of a cross-linking agent successfully changed the matrix performance, allowing the controlled release of pindolol. (C) 2004 Elsevier B.V. All rights reserved.Cross-linked alginate-gelatine beadsa new matrix for controlled release of pindololAlmeida, PFAlmeida, AJHostingInstitutionOrganizationalRepositório Científico de Acesso Aberto da ULisboae-mailmailto:repositorio@reitoria.ulisboa.ptrepositorio@reitoria.ulisboa.ptISSNIsPartOf0168-3659DOIIsPartOfhttp://dx.doi.org/10.1016/j.conrel.2004.03.0152015-12-30T10:17:16Z20042004-01-01T00:00:00ZHandlehttp://hdl.handle.net/10451/20984http://purl.org/coar/access_right/c_14cbmetadata only accessChemistry, MultidisciplinaryPharmacology & Pharmacyliteraturehttp://purl.org/coar/resource_type/c_6501journal articleJOURNAL OF CONTROLLED RELEASEVol. 97431439
spellingShingle Cross-linked alginate-gelatine beads
Almeida, PF
Chemistry, Multidisciplinary
Pharmacology & Pharmacy
status SINGLETON
subject.fl_str_mv Chemistry, Multidisciplinary
Pharmacology & Pharmacy
title Cross-linked alginate-gelatine beads
title_full Cross-linked alginate-gelatine beads
title_fullStr Cross-linked alginate-gelatine beads
title_full_unstemmed Cross-linked alginate-gelatine beads
title_short Cross-linked alginate-gelatine beads
title_sort Cross-linked alginate-gelatine beads
topic Chemistry, Multidisciplinary
Pharmacology & Pharmacy
topic_facet Chemistry, Multidisciplinary
Pharmacology & Pharmacy
url http://hdl.handle.net/10451/20984
visible 1