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Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response

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Resumo:Besnoitia besnoiti is an apicomplexan parasite responsible for bovine besnoitiosis, a disease with a high prevalence in tropical and subtropical regions and re-emerging in Europe. Despite the great economical losses associated with besnoitiosis, this disease has been underestimated and poorly studied, and neither an effective therapy nor a vaccine to be used in Europe is available. Protein disulfide isomerase (PDI) is an essential enzyme for the acquisition of the correct three-dimensional structure of proteins. Current evidence suggests that in Neospora caninum and Toxoplasma gondii, which are closely related to B. besnoiti, PDI plays an important role in host cell invasion, is a relevant target for the host immune response, and represents a promising drug target and/or vaccine candidate. In this work, we presented the nucleotide sequence of the B. besnoiti PDI gene and a 3D theoretical model was built by comparative homology using Swiss-Model server. B. besnoiti expresses a PDI with 471 amino acids, structurally similar to human and yeast PDIs, with four thioredoxin-like domains a, b, b’, a’ and a C-terminal extension c. The a and a’ domains present the characteristic active site pattern CxxC, in this case CGHC and CGYC, respectively. Analysis of the phylogenetic tree for PDI within the phylum Apicomplexa reinforced the close relationship among B. besnoiti, N. caninum and T. gondii. Recombinant B. besnoiti PDI (recBbPDI) and truncated versions corresponding to domains a, b, b’ and a’c were expressed in a heterologous system. Mice were immunized with recBbPDI for the production of monoclonal antibodies (mAbs) by hybridoma technology and four mAbs were produced and characterized. RecBbPDI and domain a’c (recBb-a’c) were functionally active and exhibited a dose dependent cross-linking activity of insulin. In the presence of bacitracin, tocinoic acid, 5,5′-dithiobis(2-nitrobenzoic acid) (DTNB) and 4-chloromercuribenzoic acid (pCMBA) activity of both enzymes was inhibited, in a dose dependent manner. The same happened with recBbPDI in the presence of mAbs (with the exception of T8a), but not with recBb-a’c, whose activity was not sensitive to the presence of mAbs. In vitro proliferation of B. besnoiti tachyzoites was diminished in the presence of PDI inhibitors and anti-PDI mAbs, indicating that this enzyme seems to intervene in the process of host cell adhesion/invasion. In this way, considering the inhibitions obtained, both in the host cell invasion ability and in the enzyme catalytic activity, PDI can represent a potential target for addressing the treatment and/or prevention of besnoitiosis. The panel of monoclonal antibodies here developed represents an important tool for future studies.
Autores principais:Marcelino, Eduardo Miguel Baptista Ferreira
Assunto:Besnoitia besnoiti protein disulfide isomerase PDI monoclonal antibody host cell invasion enzima isomerase de dissulfureto anticorpos monoclonais invasão célula hospedeira
Ano:2016
País:Portugal
Tipo de documento:tese de doutoramento
Tipo de acesso:acesso aberto
Instituição associada:Universidade de Lisboa
Idioma:inglês
Origem:Repositório da Universidade de Lisboa
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author Marcelino, Eduardo Miguel Baptista Ferreira
author_facet Marcelino, Eduardo Miguel Baptista Ferreira
Marcelino, Eduardo Miguel Baptista Ferreira
author_role author
contributor_name_str_mv Leitão, José Alexandre da Costa Perdigão e Cameira
Novo, Carlos Manuel Mendes
Repositório Científico de Acesso Aberto da ULisboa
country_str PT
creators_json_str [{\"Person.name\":\"Marcelino, Eduardo Miguel Baptista Ferreira\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Leitão, José Alexandre da Costa Perdigão e Cameira
Novo, Carlos Manuel Mendes
Repositório Científico de Acesso Aberto da ULisboa
datacite.creators.creator.creatorName.fl_str_mv Marcelino, Eduardo Miguel Baptista Ferreira
datacite.date.Accepted.fl_str_mv 2016-06-07T00:00:00Z
datacite.date.available.fl_str_mv 2017-06-30T00:30:11Z
datacite.date.embargoed.fl_str_mv 2017-06-30T00:30:11Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Besnoitia besnoiti
protein disulfide isomerase
PDI
monoclonal antibody
host cell invasion
enzima isomerase de dissulfureto
anticorpos monoclonais
invasão célula hospedeira
datacite.titles.title.fl_str_mv Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
dc.contributor.none.fl_str_mv Leitão, José Alexandre da Costa Perdigão e Cameira
Novo, Carlos Manuel Mendes
Repositório Científico de Acesso Aberto da ULisboa
dc.creator.none.fl_str_mv Marcelino, Eduardo Miguel Baptista Ferreira
dc.date.Accepted.fl_str_mv 2016-06-07T00:00:00Z
dc.date.available.fl_str_mv 2017-06-30T00:30:11Z
dc.date.embargoed.fl_str_mv 2017-06-30T00:30:11Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv http://hdl.handle.net/10400.5/11693
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv Universidade de Lisboa. Faculdade de Medicina Veterinária
dc.rights.cclincense.fl_str_mv http://creativecommons.org/licenses/by/4.0/
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Besnoitia besnoiti
protein disulfide isomerase
PDI
monoclonal antibody
host cell invasion
enzima isomerase de dissulfureto
anticorpos monoclonais
invasão célula hospedeira
dc.title.fl_str_mv Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_db06
description Besnoitia besnoiti is an apicomplexan parasite responsible for bovine besnoitiosis, a disease with a high prevalence in tropical and subtropical regions and re-emerging in Europe. Despite the great economical losses associated with besnoitiosis, this disease has been underestimated and poorly studied, and neither an effective therapy nor a vaccine to be used in Europe is available. Protein disulfide isomerase (PDI) is an essential enzyme for the acquisition of the correct three-dimensional structure of proteins. Current evidence suggests that in Neospora caninum and Toxoplasma gondii, which are closely related to B. besnoiti, PDI plays an important role in host cell invasion, is a relevant target for the host immune response, and represents a promising drug target and/or vaccine candidate. In this work, we presented the nucleotide sequence of the B. besnoiti PDI gene and a 3D theoretical model was built by comparative homology using Swiss-Model server. B. besnoiti expresses a PDI with 471 amino acids, structurally similar to human and yeast PDIs, with four thioredoxin-like domains a, b, b’, a’ and a C-terminal extension c. The a and a’ domains present the characteristic active site pattern CxxC, in this case CGHC and CGYC, respectively. Analysis of the phylogenetic tree for PDI within the phylum Apicomplexa reinforced the close relationship among B. besnoiti, N. caninum and T. gondii. Recombinant B. besnoiti PDI (recBbPDI) and truncated versions corresponding to domains a, b, b’ and a’c were expressed in a heterologous system. Mice were immunized with recBbPDI for the production of monoclonal antibodies (mAbs) by hybridoma technology and four mAbs were produced and characterized. RecBbPDI and domain a’c (recBb-a’c) were functionally active and exhibited a dose dependent cross-linking activity of insulin. In the presence of bacitracin, tocinoic acid, 5,5′-dithiobis(2-nitrobenzoic acid) (DTNB) and 4-chloromercuribenzoic acid (pCMBA) activity of both enzymes was inhibited, in a dose dependent manner. The same happened with recBbPDI in the presence of mAbs (with the exception of T8a), but not with recBb-a’c, whose activity was not sensitive to the presence of mAbs. In vitro proliferation of B. besnoiti tachyzoites was diminished in the presence of PDI inhibitors and anti-PDI mAbs, indicating that this enzyme seems to intervene in the process of host cell adhesion/invasion. In this way, considering the inhibitions obtained, both in the host cell invasion ability and in the enzyme catalytic activity, PDI can represent a potential target for addressing the treatment and/or prevention of besnoitiosis. The panel of monoclonal antibodies here developed represents an important tool for future studies.
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format doctoralThesis
fulltext.url.fl_str_mv https://repositorio.ulisboa.pt/bitstreams/a8aff77d-fb06-4a8b-b12a-bdef2f658400/download
id ul_ea2c2cc06f483e9793984eda7bda2f45
identifier.url.fl_str_mv http://hdl.handle.net/10400.5/11693
instacron_str ul
institution Universidade de Lisboa
instname_str Universidade de Lisboa
language eng
network_acronym_str ul
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oai_identifier_str oai:repositorio.ulisboa.pt:10400.5/11693
organization_str_mv urn:organizationAcronym:ul
person_str_mv Marcelino, Eduardo Miguel Baptista Ferreira
publishDate 2016
publisher.none.fl_str_mv Universidade de Lisboa. Faculdade de Medicina Veterinária
reponame_str Repositório da Universidade de Lisboa
repository_id_str urn:repositoryAcronym:ul
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spelling engUniversidade de Lisboa. Faculdade de Medicina Veterináriapt_PTBesnoitia besnoiti is an apicomplexan parasite responsible for bovine besnoitiosis, a disease with a high prevalence in tropical and subtropical regions and re-emerging in Europe. Despite the great economical losses associated with besnoitiosis, this disease has been underestimated and poorly studied, and neither an effective therapy nor a vaccine to be used in Europe is available. Protein disulfide isomerase (PDI) is an essential enzyme for the acquisition of the correct three-dimensional structure of proteins. Current evidence suggests that in Neospora caninum and Toxoplasma gondii, which are closely related to B. besnoiti, PDI plays an important role in host cell invasion, is a relevant target for the host immune response, and represents a promising drug target and/or vaccine candidate. In this work, we presented the nucleotide sequence of the B. besnoiti PDI gene and a 3D theoretical model was built by comparative homology using Swiss-Model server. B. besnoiti expresses a PDI with 471 amino acids, structurally similar to human and yeast PDIs, with four thioredoxin-like domains a, b, b’, a’ and a C-terminal extension c. The a and a’ domains present the characteristic active site pattern CxxC, in this case CGHC and CGYC, respectively. Analysis of the phylogenetic tree for PDI within the phylum Apicomplexa reinforced the close relationship among B. besnoiti, N. caninum and T. gondii. Recombinant B. besnoiti PDI (recBbPDI) and truncated versions corresponding to domains a, b, b’ and a’c were expressed in a heterologous system. Mice were immunized with recBbPDI for the production of monoclonal antibodies (mAbs) by hybridoma technology and four mAbs were produced and characterized. RecBbPDI and domain a’c (recBb-a’c) were functionally active and exhibited a dose dependent cross-linking activity of insulin. In the presence of bacitracin, tocinoic acid, 5,5′-dithiobis(2-nitrobenzoic acid) (DTNB) and 4-chloromercuribenzoic acid (pCMBA) activity of both enzymes was inhibited, in a dose dependent manner. The same happened with recBbPDI in the presence of mAbs (with the exception of T8a), but not with recBb-a’c, whose activity was not sensitive to the presence of mAbs. In vitro proliferation of B. besnoiti tachyzoites was diminished in the presence of PDI inhibitors and anti-PDI mAbs, indicating that this enzyme seems to intervene in the process of host cell adhesion/invasion. In this way, considering the inhibitions obtained, both in the host cell invasion ability and in the enzyme catalytic activity, PDI can represent a potential target for addressing the treatment and/or prevention of besnoitiosis. The panel of monoclonal antibodies here developed represents an important tool for future studies.application/pdfpt_PTProtein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune responseMarcelino, Eduardo Miguel Baptista FerreiraLeitão, José Alexandre da Costa Perdigão e CameiraNovo, Carlos Manuel MendesHostingInstitutionOrganizationalRepositório Científico de Acesso Aberto da ULisboae-mailmailto:repositorio@reitoria.ulisboa.ptrepositorio@reitoria.ulisboa.ptURNurn:tid:1012629732017-06-30T00:30:11Z2016-06-072016-06-07T00:00:00ZHandlehttp://hdl.handle.net/10400.5/11693http://purl.org/coar/access_right/c_abf2open accessBesnoitia besnoitiprotein disulfide isomerasePDImonoclonal antibodyhost cell invasionenzima isomerase de dissulfuretoanticorpos monoclonaisinvasão célula hospedeira4980136 bytesliteraturehttp://purl.org/coar/resource_type/c_db06doctoral thesis2016-06-07http://creativecommons.org/licenses/by/4.0/http://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://repositorio.ulisboa.pt/bitstreams/a8aff77d-fb06-4a8b-b12a-bdef2f658400/download
spellingShingle Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
Marcelino, Eduardo Miguel Baptista Ferreira
Besnoitia besnoiti
protein disulfide isomerase
PDI
monoclonal antibody
host cell invasion
enzima isomerase de dissulfureto
anticorpos monoclonais
invasão célula hospedeira
Marcelino, Eduardo Miguel Baptista Ferreira
Besnoitia besnoiti
protein disulfide isomerase
PDI
monoclonal antibody
host cell invasion
enzima isomerase de dissulfureto
anticorpos monoclonais
invasão célula hospedeira
status SINGLETON
subject.fl_str_mv Besnoitia besnoiti
protein disulfide isomerase
PDI
monoclonal antibody
host cell invasion
enzima isomerase de dissulfureto
anticorpos monoclonais
invasão célula hospedeira
title Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
title_full Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
title_fullStr Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
title_full_unstemmed Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
title_short Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
title_sort Protein disulfide isomerase as a target for besnoitiosis therapy : molecular characterization and studies of its role in infection and host immune response
topic Besnoitia besnoiti
protein disulfide isomerase
PDI
monoclonal antibody
host cell invasion
enzima isomerase de dissulfureto
anticorpos monoclonais
invasão célula hospedeira
topic_facet Besnoitia besnoiti
protein disulfide isomerase
PDI
monoclonal antibody
host cell invasion
enzima isomerase de dissulfureto
anticorpos monoclonais
invasão célula hospedeira
url http://hdl.handle.net/10400.5/11693
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