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Headspace solid-phase microextraction and gas chromatography/ion trap-mass spectrometry applied to a living system: Pieris brassicae fed with kale

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Resumo:The influence of Pieris brassicae feeding on kale was monitored, by evaluating its effect on the volatiles released by the plant through time. This is the first study applying headspace solid-phase microextraction (HS-SPME) and gas chromatography/ion trap-mass spectrometry to an isolated insect, as most studies analyse the insect–plant system as a whole, being unable to evaluate the contribution of the insect itself. Substantial differences were noticed between the volatiles composition of kale before and after the insect’s attack. More than 60 compounds were found, including terpenes, lipoxygenase pathway by-products, ketones, norisoprenoids, etc. After insect attack, l-camphor, sabinene and a-thujene were found and limonene and eucalyptol suffered a noticeable increase. A considerable rise in (Z)-3-hexenyl acetate was also observed. In vivo accumulation of limonene and camphor by the insect was detected. The findings contribute to the knowledge of the ecological interactions between the two species.
Autores principais:Fernandes, Fátima
Outros Autores:Pereira, David M.; Pinho, P. Guedes de; Valentão, Patrícia; Pereira, J.A.; Bento, Albino; Andrade, Paula B.
Assunto:Brassica oleracea L. var. acephala Kale Pieris brassicae Volatile compounds HS-SPME GC/IT-MS
Ano:2009
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso restrito
Instituição associada:Instituto Politécnico de Bragança
Idioma:inglês
Origem:Biblioteca Digital do IPB
Descrição
Resumo:The influence of Pieris brassicae feeding on kale was monitored, by evaluating its effect on the volatiles released by the plant through time. This is the first study applying headspace solid-phase microextraction (HS-SPME) and gas chromatography/ion trap-mass spectrometry to an isolated insect, as most studies analyse the insect–plant system as a whole, being unable to evaluate the contribution of the insect itself. Substantial differences were noticed between the volatiles composition of kale before and after the insect’s attack. More than 60 compounds were found, including terpenes, lipoxygenase pathway by-products, ketones, norisoprenoids, etc. After insect attack, l-camphor, sabinene and a-thujene were found and limonene and eucalyptol suffered a noticeable increase. A considerable rise in (Z)-3-hexenyl acetate was also observed. In vivo accumulation of limonene and camphor by the insect was detected. The findings contribute to the knowledge of the ecological interactions between the two species.