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Catalytic wet air oxidation of low molecular weight carboxylic acids using a carbon supported platinum catalyst

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Detalhes bibliográficos
Resumo:Aqueous solutions of low molecular weight carboxylic acids, such as acetic, propionic and butyric acids, were treated by catalytic wet air oxidation (CWAO) using a carbon supported platinum catalyst. Oxidation in the presence of the catalyst, in a stirred reactor, was carried out at 200 C and 6.9 bar of oxygen partial pressure, with conversions (after 2 h) ranging from 59.4 to 75%, and selectivities to gaseous products of up to 100%. Initial rates for conversion varied from 184 (butyric acid) to 260 mmol h−1 g−1 Pt (propionic acid). The activation energy for butyric acid conversion was found to be 56.7 kJ mol−1.
Autores principais:Gomes, Helder
Outros Autores:Figueiredo, José; Faria, Joaquim
Assunto:Catalytic wet air oxidation (CWAO) Carbon supported platinum catalyst Carboxylic acids (low molecular weight)
Ano:2000
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso restrito
Instituição associada:Instituto Politécnico de Bragança
Idioma:inglês
Origem:Biblioteca Digital do IPB
Descrição
Resumo:Aqueous solutions of low molecular weight carboxylic acids, such as acetic, propionic and butyric acids, were treated by catalytic wet air oxidation (CWAO) using a carbon supported platinum catalyst. Oxidation in the presence of the catalyst, in a stirred reactor, was carried out at 200 C and 6.9 bar of oxygen partial pressure, with conversions (after 2 h) ranging from 59.4 to 75%, and selectivities to gaseous products of up to 100%. Initial rates for conversion varied from 184 (butyric acid) to 260 mmol h−1 g−1 Pt (propionic acid). The activation energy for butyric acid conversion was found to be 56.7 kJ mol−1.