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Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies

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Resumo:To improve the biocompatibility and bioactivity of biodegradable iron-based materials, nanostructured surfaces formed by metal oxides offer a promising strategy for surface functionalization. To explore this potential, iron oxide nanotubes were synthesized on pure iron (Fe) using an anodic oxidation process (50 Vâ 30 min, using an ethylene glycol solution containing 0.3% NH4F and 3% H2O, at a speed of 100 rpm). A nanotube layer composed mainly of α-Fe2O3 with diameters between 60 and 70 nm was obtained. The effect of the Fe-oxide nanotube layer on cell viability and morphology was evaluated by in vitro studies using a human osteosarcoma cell line (SaOs-2 cells). The results showed that the presence of this layer did not harm the viability or morphology of the cells. Furthermore, cells cultured on anodized surfaces showed higher metabolic activity than those on non-anodized surfaces. This research suggests that growing a layer of Fe oxide nanotubes on pure Fe is a promising method for functionalizing and improving the cytocompatibility of iron substrates. This opens up new opportunities for biomedical applications, including the development of cardiovascular stents or osteosynthesis implants.
Autores principais:Rangel, Rita de Cássia Reis
Outros Autores:Rangel, André Luiz Reis; Silva, Kerolene Barboza da; Escada, Ana Lúcia do Amaral; Chaves, Javier Andres Munoz; Maia, F. Raquel; Pina, Sandra Cristina Almeida; Reis, R. L.; Oliveira, Joaquim M.; Alves, Ana Paula Rosifini
Assunto:Biodegradable biomaterials Biodegradable metal Surface modification
Ano:2024
País:Portugal
Tipo de documento:artigo
Tipo de acesso:acesso aberto
Instituição associada:Universidade do Minho
Idioma:inglês
Origem:RepositóriUM - Universidade do Minho
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author Rangel, Rita de Cássia Reis
author2 Rangel, André Luiz Reis
Silva, Kerolene Barboza da
Escada, Ana Lúcia do Amaral
Chaves, Javier Andres Munoz
Maia, F. Raquel
Pina, Sandra Cristina Almeida
Reis, R. L.
Oliveira, Joaquim M.
Alves, Ana Paula Rosifini
author2_role author
author
author
author
author
author
author
author
author
author_facet Rangel, Rita de Cássia Reis
Rangel, André Luiz Reis
Silva, Kerolene Barboza da
Escada, Ana Lúcia do Amaral
Chaves, Javier Andres Munoz
Maia, F. Raquel
Pina, Sandra Cristina Almeida
Reis, R. L.
Oliveira, Joaquim M.
Alves, Ana Paula Rosifini
author_role author
contributor_name_str_mv Universidade do Minho
country_str PT
creators_json_txt [{\"Person.name\":\"Rangel, Rita de Cássia Reis\"},{\"Person.name\":\"Rangel, André Luiz Reis\"},{\"Person.name\":\"Silva, Kerolene Barboza da\"},{\"Person.name\":\"Escada, Ana Lúcia do Amaral\"},{\"Person.name\":\"Chaves, Javier Andres Munoz\"},{\"Person.name\":\"Maia, F. Raquel\"},{\"Person.name\":\"Pina, Sandra Cristina Almeida\"},{\"Person.name\":\"Reis, R. L.\"},{\"Person.name\":\"Oliveira, Joaquim M.\"},{\"Person.name\":\"Alves, Ana Paula Rosifini\"}]
datacite.contributors.contributor.contributorName.fl_str_mv Universidade do Minho
datacite.creators.creator.creatorName.fl_str_mv Rangel, Rita de Cássia Reis
Rangel, André Luiz Reis
Silva, Kerolene Barboza da
Escada, Ana Lúcia do Amaral
Chaves, Javier Andres Munoz
Maia, F. Raquel
Pina, Sandra Cristina Almeida
Reis, R. L.
Oliveira, Joaquim M.
Alves, Ana Paula Rosifini
datacite.date.Accepted.fl_str_mv 2024-07-01T00:00:00Z
datacite.date.available.fl_str_mv 2024-07-26T15:19:06Z
datacite.date.embargoed.fl_str_mv 2024-07-26T15:19:06Z
datacite.rights.fl_str_mv http://purl.org/coar/access_right/c_abf2
datacite.subjects.subject.fl_str_mv Biodegradable biomaterials
Biodegradable metal
Surface modification
datacite.titles.title.fl_str_mv Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
dc.contributor.none.fl_str_mv Universidade do Minho
dc.creator.none.fl_str_mv Rangel, Rita de Cássia Reis
Rangel, André Luiz Reis
Silva, Kerolene Barboza da
Escada, Ana Lúcia do Amaral
Chaves, Javier Andres Munoz
Maia, F. Raquel
Pina, Sandra Cristina Almeida
Reis, R. L.
Oliveira, Joaquim M.
Alves, Ana Paula Rosifini
dc.date.Accepted.fl_str_mv 2024-07-01T00:00:00Z
dc.date.available.fl_str_mv 2024-07-26T15:19:06Z
dc.date.embargoed.fl_str_mv 2024-07-26T15:19:06Z
dc.format.none.fl_str_mv application/pdf
dc.identifier.none.fl_str_mv https://hdl.handle.net/1822/92623
dc.language.none.fl_str_mv eng
dc.publisher.none.fl_str_mv MDPI
dc.rights.none.fl_str_mv http://purl.org/coar/access_right/c_abf2
dc.subject.none.fl_str_mv Biodegradable biomaterials
Biodegradable metal
Surface modification
dc.title.fl_str_mv Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
dc.type.none.fl_str_mv http://purl.org/coar/resource_type/c_6501
description To improve the biocompatibility and bioactivity of biodegradable iron-based materials, nanostructured surfaces formed by metal oxides offer a promising strategy for surface functionalization. To explore this potential, iron oxide nanotubes were synthesized on pure iron (Fe) using an anodic oxidation process (50 Vâ 30 min, using an ethylene glycol solution containing 0.3% NH4F and 3% H2O, at a speed of 100 rpm). A nanotube layer composed mainly of α-Fe2O3 with diameters between 60 and 70 nm was obtained. The effect of the Fe-oxide nanotube layer on cell viability and morphology was evaluated by in vitro studies using a human osteosarcoma cell line (SaOs-2 cells). The results showed that the presence of this layer did not harm the viability or morphology of the cells. Furthermore, cells cultured on anodized surfaces showed higher metabolic activity than those on non-anodized surfaces. This research suggests that growing a layer of Fe oxide nanotubes on pure Fe is a promising method for functionalizing and improving the cytocompatibility of iron substrates. This opens up new opportunities for biomedical applications, including the development of cardiovascular stents or osteosynthesis implants.
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eu_rights_str_mv openAccess
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id rum_4e090e49a282cd5d7330010758405591
identifier.url.fl_str_mv https://hdl.handle.net/1822/92623
instacron_str repositorium
institution Universidade do Minho
instname_str Universidade do Minho
language eng
network_acronym_str rum
network_name_str RepositóriUM - Universidade do Minho
oai_identifier_str oai:repositorium.uminho.pt:1822/92623
organization_str_mv urn:organizationAcronym:repositorium
person_str_mv Rangel, Rita de Cássia Reis
Rangel, André Luiz Reis
Silva, Kerolene Barboza da
Escada, Ana Lúcia do Amaral
Chaves, Javier Andres Munoz
Maia, F. Raquel
Pina, Sandra Cristina Almeida
Reis, R. L.
Oliveira, Joaquim M.
Alves, Ana Paula Rosifini
publishDate 2024
publisher.none.fl_str_mv MDPI
reponame_str RepositóriUM - Universidade do Minho
repository_id_str urn:repositoryAcronym:rum
service_str_mv urn:repositoryAcronym:rum
spelling engMDPIporTo improve the biocompatibility and bioactivity of biodegradable iron-based materials, nanostructured surfaces formed by metal oxides offer a promising strategy for surface functionalization. To explore this potential, iron oxide nanotubes were synthesized on pure iron (Fe) using an anodic oxidation process (50 Vâ 30 min, using an ethylene glycol solution containing 0.3% NH4F and 3% H2O, at a speed of 100 rpm). A nanotube layer composed mainly of α-Fe2O3 with diameters between 60 and 70 nm was obtained. The effect of the Fe-oxide nanotube layer on cell viability and morphology was evaluated by in vitro studies using a human osteosarcoma cell line (SaOs-2 cells). The results showed that the presence of this layer did not harm the viability or morphology of the cells. Furthermore, cells cultured on anodized surfaces showed higher metabolic activity than those on non-anodized surfaces. This research suggests that growing a layer of Fe oxide nanotubes on pure Fe is a promising method for functionalizing and improving the cytocompatibility of iron substrates. This opens up new opportunities for biomedical applications, including the development of cardiovascular stents or osteosynthesis implants.application/pdfporCharacterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studiesRangel, Rita de Cássia ReisRangel, André Luiz ReisSilva, Kerolene Barboza daEscada, Ana Lúcia do AmaralChaves, Javier Andres MunozMaia, F. RaquelPina, Sandra Cristina AlmeidaReis, R. L.Oliveira, Joaquim M.Alves, Ana Paula RosifiniHostingInstitutionOrganizationalUniversidade do Minhoe-mailmailto:repositorium@usdb.uminho.ptrepositorium@usdb.uminho.ptISSNIsPartOf1996-1944DOIIsPartOf10.3390/ma171536272024-07-26T15:19:06Z2024-072024-072024-07-25T16:30:05Z2024-07-01T00:00:00ZHandlehttps://hdl.handle.net/1822/92623http://purl.org/coar/access_right/c_abf2open accessBiodegradable biomaterialsBiodegradable metalSurface modification6122338 bytesliteraturehttp://purl.org/coar/resource_type/c_6501journal articlehttp://purl.org/coar/access_right/c_abf2application/pdffulltexthttps://prod-dspace.uminho.pt/bitstreams/4c6be76a-a9cd-45d1-9cb0-81f937797978/download
spellingShingle Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
Rangel, Rita de Cássia Reis
Biodegradable biomaterials
Biodegradable metal
Surface modification
status SINGLETON
subject.fl_str_mv Biodegradable biomaterials
Biodegradable metal
Surface modification
title Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
title_full Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
title_fullStr Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
title_full_unstemmed Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
title_short Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
title_sort Characterization of iron oxide nanotubes obtained by anodic oxidation for biomedical applications—In vitro studies
topic Biodegradable biomaterials
Biodegradable metal
Surface modification
topic_facet Biodegradable biomaterials
Biodegradable metal
Surface modification
url https://hdl.handle.net/1822/92623
visible 1